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Microwave-assisted synthesis and optical property of CdMoO4 nanoparticles
Authors:Anukorn Phuruangrat  Nuengruethai Ekthammathat  Somchai Thongtem
Affiliation:a Department of Materials Science and Technology, Faculty of Science, Prince of Songkla University, Hat Yai, Songkhla 90112, Thailand
b Department of Chemistry, Faculty of Science, Chiang Mai University, Chiang Mai 50200, Thailand
c Department of Physics and Materials Science, Faculty of Science, Chiang Mai University, Chiang Mai 50200, Thailand
Abstract:Microwave-assisted synthesis is a novel method used to synthesize CdMoO4 nanoparticles in propylene glycol. The effects of reaction time and microwave power on phase, morphologies, and optical properties of CdMoO4 nanoparticles were studied, using X-ray diffraction (XRD), Raman spectroscopy, Fourier transform infrared spectroscopy (FTIR), transmission electron microscopy (TEM), and UV-visible spectroscopy. The present analyses proved that these crystalline powders were scheelite-type tetragonal structured CdMoO4, with the crystallite size of 14-20 nm, and 4.51-4.73 eV band gaps, controlled by the synthetic conditions.
Keywords:A  Semiconductors  C  Electron microscopy  C  Raman spectroscopy  C  X-ray diffraction  D  Optical properties
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