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油井水泥降失水剂AS的合成与性能评价
引用本文:王广英,张金生,李丽华,杨波勇.油井水泥降失水剂AS的合成与性能评价[J].辽宁石油化工大学学报,2012(2):38-42.
作者姓名:王广英  张金生  李丽华  杨波勇
作者单位:辽宁石油化工大学化学与材料科学学院;辽宁石油化工大学石油化工学院
摘    要:采用自由基聚合法,以2-丙烯酰胺基-2- 甲基丙磺酸(AMPS)和丙烯酰胺(AM)为原料合成共聚物,再与木质素磺酸钠复配,合成了降失水剂 AS.通过正交试验优选合成条件,并对降失水剂AS进行了全面的性能评价.评价结果表明:降失水剂AS具有较好的耐热性和耐盐性,在150℃下,降失水剂AS在饱和盐水中的API滤失量(API...

关 键 词:降失水剂  耐温  耐盐  固井

Synthesis and Evaluation of AS Fluid Loss Additive for Cement Slurry
WANG Guang-ying,ZHANG Jin-sheng,LI Li-hua,YANG Bo-yong.Synthesis and Evaluation of AS Fluid Loss Additive for Cement Slurry[J].Journal of Liaoning University of Petroleum & Chemical Technology,2012(2):38-42.
Authors:WANG Guang-ying  ZHANG Jin-sheng  LI Li-hua  YANG Bo-yong
Affiliation:1(1.School of Chemistry and Material Science,Liaoning Shihua University,Fushun Liaoning 113001,P.R.China;2.School of Petrochemical Engineering,Liaoning Shihua University,Fushun Liaoning 113001,P.R.China)Received 29 November 2011;revised 29 December 2011;accepted 6 March 2012
Abstract:The AS fluid loss additive was formulated with sodium lignosulfonate and the copolymers obtained by radical polymerization with AMPS and AM as raw material.Orthogonal tests were designed for optimizing the synthetic process of the fluid loss additive AS,and the performance of this fluid loss additive was systematically evaluated.API filtration in saturated salt solution at 150 ℃ is 96 mL;API filtration can be controlled within 50 mL when adding AS between 3% and 8%(weight percentage) at 120 ℃;Meanwhile AS has good compatibility with other additives.Sodium bicarbonate was used to adjust the PH and discharge oxygen of device used in the synthesis process.No nitrogen was needed as protective gas,which simplified the synthesis process.The sodium lignosulfonate derives from the wastewater of paper mill,so it not only reduces the cost but also protects the environment.
Keywords:Fluid loss additive  Heat resistance  Salt resistance  Well cementation
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