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经痛消颗粒中芍药苷含量测定
引用本文:马春芬,张红瑞. 经痛消颗粒中芍药苷含量测定[J]. 上海中医药杂志, 2002, 36(10): 42-43
作者姓名:马春芬  张红瑞
作者单位:河南中医学院,河南,郑州,450003
摘    要:为建立经痛消颗粒中芍药苷含量测定方法,以薄层色谱-比色法,采用薄层色谱法将复方制剂经痛消颗粒中的芍药苷与其他成分分离,然后用紫外分光光度法测定其含量。结果:能消除其他成分的背景干扰,芍药苷平均回收率为98.74%,RSD为1.41%。在一定浓度范围内线性良好,提示薄层色谱-比色法可用作该制剂的定量分析。

关 键 词:经痛消颗粒 芍药苷 薄层色谱-比色法 含量测定
文章编号:1007-1334(2002)10-0042-02

Assessment of Paeoniae Saponin in "Jingtongxiao Granule"
He'nan College of Traditional Chinese Medicine MA Chun fen ZHANG Hong rui. Assessment of Paeoniae Saponin in "Jingtongxiao Granule"[J]. Shanghai Journal of Traditional Chinese Medicine, 2002, 36(10): 42-43
Authors:He'nan College of Traditional Chinese Medicine MA Chun fen ZHANG Hong rui
Affiliation:He'nan College of Traditional Chinese Medicine 450003MA Chun fen ZHANG Hong rui
Abstract:To measure the paeoniae saponin in "Jingtongxiao Granule",thin layer chromatography (TLC) was used to separate paeoniae saponin from other ingredients;then ultraviolet spectrophotometry was performed to measure the paeoniae saponin.Results:This method can eliminate the disturbance of other ingredients;the average recovery rate was 98 74% and RSD was 1 43%,with good linear relationship.It is suggested that this method can be used as quantitative analysis for paeoniae saponin
Keywords:Jingtongxiao Granule"  ,paeoniae saponin,thin layer chromatography(TLC)
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