| 乌梅人丹质量标准的研究 |
| |
| 引用本文： | 毛秀红,王柯,季申. 乌梅人丹质量标准的研究[J]. 中成药, 2005, 27(8): 896-899 |
| |
| 作者姓名： | 毛秀红 王柯 季申 |
| |
| 作者单位： | 上海市药品检验所,上海,200233 |
| |
| 摘 要： | 目的:建立乌梅人丹的质量标准;方法:对制剂中乌梅用薄层色谱法进行定性鉴别,同时采用气相色谱法测定制剂中薄荷脑含量以及采用高效液相色谱法测定制剂中甘草酸铵的含量.结果:平均回收率分别为103.5%、100.3%,RSD分别为0.76%(n=6)和1.03%(n=6).薄层图谱斑点清晰,空白无干扰.结论:方法简便、准确、重现性好,可有效控制该制剂的质量.
|
| 关 键 词： | 乌梅人丹 鉴别 薄荷脑 气相色谱法 甘草酸铵 高效液相色谱法 含量测定 |
| 文章编号： | 1001-1528（2005）08-0896-03 |
| 收稿时间： | 2004-04-30 |
| 修稿时间： | 2004-04-30 |
Quality standard of Wumeirendan |
| |
| MAO Xiu-hong,WANG Ke,JI Shen. Quality standard of Wumeirendan[J]. Chinese Traditional Patent Medicine, 2005, 27(8): 896-899 |
| |
| Authors: | MAO Xiu-hong WANG Ke JI Shen |
| |
| Abstract: | AIM: To establish the quality standard of Wumeirendan (Fructus Mume, Radix et Rhizoma Glycyrrhizae, Mentholm, etc.) METHODS: Fructus Mume was identified by TLC. Menthol was determined by GC, Ammonium glycyrrhiziate was determined by HPLC. RESULTS: The average recoveries were 103.5% and 100.3%, RSD were 0.76% and 1.03%. The TLC sports developed were fairly clear, and the blank test showed no interference. CONCLUSION:The method developed is simple and accurate with good reproducibility, and the method can be used for quality control of Wumeirendan. |
| |
| Keywords: | Wmeirendan identification menthol GC ammonium glycyrrhiziate HPLC determination |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
|
