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测定食盐碘含量及其影响因素研究
引用本文:额尔登桑,耐登,柴志波. 测定食盐碘含量及其影响因素研究[J]. 食品研究与开发, 2012, 33(2): 126-130
作者姓名:额尔登桑  耐登  柴志波
作者单位:内蒙古师范大学化学与环境科学学院,内蒙古呼和浩特,010022
基金项目:内蒙古自治区科技计划项目资助(20080502)
摘    要:用碘离子选择性电极测定食盐中碘含量并对影响因素进行探讨。在Na2SO3作还原剂,双盐桥甘汞电极作参比电极的条件下,引入表面活性剂,使碘离子的浓度在2.0×10-7mol/L~1.0×10-2mol/L范围内的对数与响应电位值呈良好的线性关系。试验结果显示:碘盐中的碘含量为27.22 mg/kg,均达到国家标准,同时讨论温度、时间等对碘含量的影响。碘的回收率在94.99%~106.3%之间,相对标准偏差RSD≤3.23%。

关 键 词:离子选择性电极  食盐  影响因素  碘损失

Research on Temperature Effect and Determination of Iodine Content in Iodacted Salt
E Erdengsang , NAI Deng , CHAI Zhi-bo. Research on Temperature Effect and Determination of Iodine Content in Iodacted Salt[J]. Food Research and Developent, 2012, 33(2): 126-130
Authors:E Erdengsang    NAI Deng    CHAI Zhi-bo
Affiliation:(Chemistry & Environment Science College,Inner Mongolia Normal University,Huhhot 010022,Inner Mongolia,China)
Abstract:Determinate the Iodine in table salt by Iodine Ion-selective electrode and then discusse about it’s influence factors.Take Na2SO3 as a reductant,in the double salt bridge GanGong for the reference electrode sitnatoin,inducted surfactant,that makes the iodine ion concentration within 2.0×10-7 mol/L-1.0×10-2 mol/L the scope of the logarithmic and response potential value was good linear relationship.The results showed that: the iodine content in Table Salt is 27.22 mg/kg,all had reached national standards.At the same time discussed the influence about the temperature,time and so on.The recovery are between 94.99 %-106.30 %,The relative standard deviation(RSD) is not more than 3.23 %.
Keywords:ion-selective electrode  table salt  effective factors  the loss of iodine
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