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推拉式小车法制备单层硒化钨薄膜
引用本文:曹元广,于佳鑫.推拉式小车法制备单层硒化钨薄膜[J].光学仪器,2020,42(4):88-94.
作者姓名:曹元广  于佳鑫
作者单位:上海理工大学 光电信息与计算机工程学院,上海 200093
基金项目:国家自然科学基金(NSFC11604210)
摘    要:为了提升单层硒化钨(WSe2)薄膜的制备质量,在传统化学气相沉积(CVD)法制备的基础上进行改进,通过引入推拉式小车来制备单层WSe2薄膜,从而构造出可以调控沉积区域、精确控制生长时间,并可实现快速降温的生长方式。采用光学显微镜和原子力显微镜来表征制备材料的尺寸、荧光强度、形貌结构等特性,证明了利用推拉式小车法可成功制备出高质量的单层WSe2薄膜。推拉式小车法可以稳定制备大面积、高质量、单层的WSe2薄膜,为其在信息、能源、生物等前沿领域的应用提供参考。

关 键 词:单层WSe2薄膜  化学气相沉积法  高质量  推拉式小车
收稿时间:2019/12/3 0:00:00

Preparation of monolayer tungsten selenide film by trolley based chemical vapor deposition method
CAO Yuanguang,YU Jiaxin.Preparation of monolayer tungsten selenide film by trolley based chemical vapor deposition method[J].Optical Instruments,2020,42(4):88-94.
Authors:CAO Yuanguang  YU Jiaxin
Affiliation:School of Optical-Electrical and Computer Engineering, University of Shanghai for Science and Technology, Shanghai, 200093, China
Abstract:In order to improve the preparation quality of monolayer (ML) tungsten selenide (WSe2). We improve the traditional chemical vapor deposition (CVD) method. ML WSe2 film is prepared by introducing a trolley to construct a growth method that can regulate the deposition area, precisely control the growth time, and achieve rapid temperature reduction. Optical microscope and atomic force microscope are used to characterize the size, fluorescence intensity and morphology of the prepared materials, which proved that a high-quality ML WSe2 film is successfully prepared by the push-pull trolley method. The large-area, high-quality, single-layer WSe2 film can be stably prepared by the trolley based method, which provides an important basis for its future application in the information, energy, and biology frontier fields.
Keywords:monolayer WSe2 film  chemical vapor deposition  high quality  trolley
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