| 碲化铜(Cu2-xTe)纳米管的可控合成与性能表征 |
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| 引用本文： | 潘飞,李晓燕,刘磊,郑业和,蒋利民,陈春年.碲化铜(Cu2-xTe)纳米管的可控合成与性能表征[J].安徽化工,2011,37(5):29-32. |
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| 作者姓名： | 潘飞 李晓燕 刘磊 郑业和 蒋利民 陈春年 |
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| 作者单位： | 合肥工业大学化学工程学院,安徽合肥,230009;合肥工业大学化学工程学院,安徽合肥,230009;合肥工业大学化学工程学院,安徽合肥,230009;合肥工业大学化学工程学院,安徽合肥,230009;合肥工业大学化学工程学院,安徽合肥,230009;合肥工业大学化学工程学院,安徽合肥,230009 |
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| 基金项目： | 合肥工业大学2010-2011年学生创新基金资助项目(XS2010029) |
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| 摘 要： | 介绍了采用溶剂热辅助牺牲模板法在混合溶剂中实现碲化铜（Cu2-xTe）纳米管的可控合成。在乙二醇∶丙三醇为1∶2（体积）的混合溶剂中,以铜纳米线作为牺牲模板与低温下制备的碲负离子进行反应,制得了直径约为100~200nm的碲化铜纳米管。实验过程中活性碲负离子的低温制取、铜纳米线的制备以及混合溶剂的比例是纳米管均匀生长的重要影响因素。最后对制得的碲化铜纳米管进行了X射线衍射（XRD）、透射电子显微镜（TEM）和紫外可见光谱（UV）等分析和表征。
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| 关 键 词： | 碲化铜 纳米管 可控合成 电化学性质 |
Controlled Synthesis and Characterization of Copper Telluride(Cu_(2-x)Te) Nanotubes |
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| PAN Fei,LI Xiao-yan,LIU Lei,ZHENG Ye-he,JIANG Li-min,CHEN Chun-nian.Controlled Synthesis and Characterization of Copper Telluride(Cu_(2-x)Te) Nanotubes[J].Anhui Chemical Industry,2011,37(5):29-32. |
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| Authors: | PAN Fei LI Xiao-yan LIU Lei ZHENG Ye-he JIANG Li-min CHEN Chun-nian |
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| Affiliation: | PAN Fei,LI Xiao-yan,LIU Lei,ZHENG Ye-he,JIANG Li-min,CHEN Chun-nian(School of Chemical Engineering,Hefei University of Technology,Hefei 230009,China) |
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| Abstract: | This paper had described that the controlled synthesis of copper telluride(Cu2-xTe) nanotubes was achieved by the use of assisted Solvothermal Template Sacrificed method in mixed solvents.In the mixed solvents of ethylene glycol and glycerol,the copper nanowires which have been used as sacrificial templates reacted with the low-temperature prepared telluride anions.A lot of copper telluride nanotubes which have diameter of about 100~200nm were obtained.In process of experiment,chemical active telluride anio... |
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| Keywords: | Copper Telluride nanotubes controlled synthesis electrochemical properties |
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