| HPLC法测定复方消脂胶囊中人参皂苷Rg_1、Re、Rb_1及三七皂苷R_1的含量 |
| |
| 引用本文： | 郑继标,陈丽莲. HPLC法测定复方消脂胶囊中人参皂苷Rg_1、Re、Rb_1及三七皂苷R_1的含量[J]. 亚太传统医药, 2011, 7(11): 29-32 |
| |
| 作者姓名： | 郑继标 陈丽莲 |
| |
| 作者单位： | 湛江市妇幼保健院,广东湛江,524037 |
| |
| 摘 要： | 目的:建立复方消脂胶囊中人参皂苷Rg1、Re、Rb1及三七皂苷R1含量的分析方法。方法:采用高效液相色谱法,色谱柱:Phenomenex Luna C18(2)(4.6mm×250mm,5μm);流动相:以乙腈为流动相A,以水为流动相B;柱温:27℃(70min时降为20℃);检测波长:203nm;流速:1.0mL.min-1。结果:三七中人参皂苷Rg1线性范围为1.88～11.28μg/mL,回收率为100.26%,RSD为1.56%;人参皂苷Re线性范围为0.294～1.764μg/mL,回收率为100.68%,RSD为0.64%;人参皂苷Rb1线性范围为1.76～10.56μg/mL,回收率为100.53%,RSD为0.58%;三七皂苷R1线性范围为0.376～2.256μg/mL,回收率为99.21%,RSD为1.38%。人参皂苷Rg1、Re、Rb1及三七皂苷R1四种成分均达到良好分离,在测定范围内线性良好,回收率均在99%～101%之间。结论:所建立的含量测定方法简便可行、重复性好,可用于复方消脂胶囊的质量监控。
|
| 关 键 词： | 高效液相色谱法 复方消脂胶囊 三七皂苷R1 人参皂苷Re 人参皂苷Rg1 人参皂苷Rb1 |
Determination of Ginsenoside Rg1, Re, Rb1 and Notoginsenoside R1 in Fufang Xiaozhi Capsule by HPLC |
| |
| Zheng Jibiao,Chen Lilian. Determination of Ginsenoside Rg1, Re, Rb1 and Notoginsenoside R1 in Fufang Xiaozhi Capsule by HPLC[J]. Asia-Pacific Traditional Medicine, 2011, 7(11): 29-32 |
| |
| Authors: | Zheng Jibiao Chen Lilian |
| |
| Affiliation: | Zheng Jibiao,Chen Lilian(Maternity and child care centers,Guangdong 524037,China) |
| |
| Abstract: | Objective:To establish a method for simultaneous determining ginsenoside Rg1,Re,Rb1 and notoginsenoside R1 in Fufang Xiaozhi Capsule.Methods:The effective components in Fufang Xiaozhi Capsule were determined by HPLC.Results:The resolution and the linearity were fine.The average recoveries of ginsenoside Rg1,Re,Rb1 and notoginsenoside R1 were 100.26%,(RSD 1.56%),100.68%,(RSD 0.64%),100.53%,(RSD0.58%) and 99.21%,(RSD 1.38%) separately.Conclusion:The quantitative method for determinating the ingredients of Fuf... |
| |
| Keywords: | HPLC Fufang Xiaozhi Capsule Ginsenoside Rg1 Ginsenoside Re Ginsenoside Rb1 Notoginsenoside R1 |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
|
