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| 吹扫捕集气质联用法测定水中吡啶 | |
| 引用本文： | 秦明友,张新申,康莉,黄璐.吹扫捕集气质联用法测定水中吡啶[J].皮革科学与工程,2012,22(4):69-71. |
| 作者姓名： | 秦明友 张新申 康莉 黄璐 |
| 作者单位： | 1. 四川大学制革清洁技术国家工程实验室,四川成都 6100652;四川省泸州市环境保护监测站,四川泸州 646000 2. 四川大学制革清洁技术国家工程实验室,四川成都,6100652 3. 四川省泸县第一中学泸县 646124 4. 四川省泸州市环境保护监测站,四川泸州,646000 |
| 基金项目： | 国家高技术研究发展计划(863计划)资助项目 |
| 摘 要： | 建立了吹扫捕集气质联用法测定水中吡啶的方法,优化了吹扫条件,用自动进标样的方法绘制工作曲线,方法的检出限为0.08μg/L,相对标准偏差在1.5%～5.1%之间,方法用于地表水、生活污水和化工废水中吡啶的测定,进行了加标回收实验,回收率在82.5%～102.5%之间。 |
| 关 键 词： | 吡啶 吹扫捕集 气相色谱/质谱 水 |
Determination of Pyridine in Water by Gas Chromatography/mass Spectrometry Coupled with Purge and Trap |
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| QIN Ming-you , ZHANG Xing-shen , KANG Li , HUANG Lu.Determination of Pyridine in Water by Gas Chromatography/mass Spectrometry Coupled with Purge and Trap[J].Leather Science and Engineering,2012,22(4):69-71. | |
| Authors: | QIN Ming-you ZHANG Xing-shen KANG Li HUANG Lu |
| Affiliation: | 1.National Engineering Laboratory for Clean Technology of Leather Manufacture;Sichuan University; Chengdu 610065;2.Luzhou Environmental Protection Monitoring Station,Luzhou Sichuan 646000; 3.No.1 Middle School of Luxian City 646124) |
| Abstract: | A method was established to determine pyridine in water by purge and trap coupled with gas chromatography/mass spectrometry.The purge and trap condition was optimized.The calibration curve was made by auto sampler.The detection limits of pyridine was 0.08 μg/L.The RSD of the method was 1.5%-5.1%,The method was applied to the analysis in surface water and domestic sewage and industrial waste water.The average recovery of the samples were 82.5%-102.5%. |
| Keywords: | pyridine gas chromatography/mass Spectrometry purge and trap water |
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