Pressure infiltration of sol/gel processed short fibre ceramic matrix composites

Using pressure infiltration short fibre-reinforced ceramic matrix composites with uniform and dense microstructure can be made. Based upon this processing technique, composites composed of silica sol, alumina particles, and alumina short fibres were fabricated. The related processing parameters studied in this work include infiltration rate, fibre volume fraction Vf, particle size, and infiltrate viscosity. An optimal infiltration rate was 4 mm min-1, at which rate the composite with Vf of 8.1% and particle size of 3 m has the highest green density. An equilibrium between particle packing strength and applied load must be obtained during the infiltration to obtain high green density and composite strength. The influence of fibre volume fraction and particle size on composite green density is in a synergistic manner because it involves particle–fibre interactions, fibre–fibre interactions, and sedimentation. Furthermore, the increase of sol viscosity results in more sedimentation in the infiltrate and lower composite green density. The fracture toughness of composites is 38% higher than that of monolithic alumina. © 1998 Chapman & Hall