| 薄层扫描法测定益气维血颗粒中黄芪甲苷的含量 |
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| 引用本文： | 陶移文,张文峰. 薄层扫描法测定益气维血颗粒中黄芪甲苷的含量[J]. 海南医学院学报, 2010, 16(12): 1549-1550,1557 |
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| 作者姓名： | 陶移文 张文峰 |
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| 作者单位： | 1. 广州医学院,广东,广州,510182
2. 回音必集团海南制药有限公司,海南,海口,570311 |
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| 基金项目： | 广州医学院博士启动项目 |
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| 摘 要： | 目的:建立益气维血颗粒中黄芪甲苷含量测定的薄层扫描法。方法:采用双波长薄层扫描法测定本品中黄芪甲苷的含量。结果:黄芪甲苷0.255~4.590μg范围内,呈良好的线性关系,r=0.998 1,平均回收率98.43%,RSD为2.28%(n=6)。结论:本法简单、准确、重现性好,适用于益气维血颗粒中黄芪甲苷的含量测定。
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| 关 键 词： | 益气维血颗粒 黄芪甲苷 薄层扫描 |
Determination of astragaloside in Yiqiweixue granules by TLC-scanning |
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| TAO Yi-wen,ZHANG Wen-feng. Determination of astragaloside in Yiqiweixue granules by TLC-scanning[J]. Journal of Hainan Medical College, 2010, 16(12): 1549-1550,1557 |
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| Authors: | TAO Yi-wen ZHANG Wen-feng |
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| Affiliation: | 1.Guangzhou Medical College,Guangzhou 510082,China;2.Hainan Huiyinbi Pharmaceutical CO.,LTD,Haikou 570311,China) |
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| Abstract: | Objective：To establish a TLC-scanning method for determination of astragaloside in Yiqiweixue granules.Methods：Dual wavelength TLC-scanning was used to detect the concentration of astragaloside in the tested Yiqiweixue granules.Results：A good linearity was shown at the concentration of 0.255 to 4.590 μg of astragaloside（r= 0.998 1）,the average recovery was 98.64% and the RSD was 2.28%.Conclusion：The method is simple,accurate,reliable,and can be used for determination of astragaloside in Yiqiweixue granules. |
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| Keywords: | Yiqiweixue granules Astragaloside TLC-scanning |
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