Observation of the morphology of thin films of solid helium deposited from the fluid onto sapphire

Thin layers of solid helium were grown on sapphire single-crystal substrates at pressures from about 500 bar to 9 kbar. Grain boundaries can be observed in these layer crystals. The morphology of the grains depends on the crystal modification. In the hcp phase (below about 1.13 kbar) a system of parallel bands is observed, probably due to slip and twinning. In the fcc phase (above 1.13 kbar) a polygonal structure similar to a helium froth is found. Melting of this froth in the fcc phase shows grain boundary melting; fluid helium is wetting the fcc grains. Grain boundaries in the hcp phase are, in contrast, not wetted by fluid helium. Near the triple point at 1.13 kbar and 15.0 K one can deposit both crystalline phases side by side. In such structures, the transition fcc hcp⁴He can be observed during isothermal holding. The transition proceeds by the parallel motion of low-energy grain boundaries.