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| 混配配合物[Zn(CF3COO)2(C7H6NS)2]的合成、晶体结构及表征 | |
| 引用本文： | 马卫兴,钱保华,李善忠,王建,许兴友,陆路德,宋海斌.混配配合物[Zn(CF3COO)2(C7H6NS)2]的合成、晶体结构及表征[J].无机化学学报,2006,22(10):1925-1928. |
| 作者姓名： | 马卫兴 钱保华 李善忠 王建 许兴友 陆路德 宋海斌 |
| 作者单位： | 1. 江苏省海洋生物技术重点建设实验室,淮海工学院,连云港,222005;淮海工学院化学工程系,连云港,222005 2. 淮海工学院化学工程系,连云港,222005;南京理工大学材料化学实验室,南京,210094 3. 南京理工大学材料化学实验室,南京,210094 4. 南开大学化学学院,天津,300071 |
| 基金项目： | 江苏省自然科学基金;江苏省高校自然科学基金;江苏省海洋生物技术重点建设实验室研究基金;淮海工学院校科研和教改项目 |
| 摘 要： | A mixed complex Zn(CF3COO)2(C7H6NS)2] was synthesized based on the reaction of Zn(CF3COO)2 and 2-aminobenzothiazol (C7H6NS) in methanol. The structure of the complex was characterized by elemental analysis, IR, 1H NMR and thermal analysis. The crystal structure of the complex was determined by X-ray single crystal diffraction. The crystal belongs to monoclinic system with space group C2/c, a=3.174 3(9) nm, b=1.010 0(3) nm, c=1.723 1(5) nm, β=118.841(4)°, V=4.839(2) nm3; Dc=1.625 g·cm-3; Z=8; F(000)=2 368; μ=1.266 mm-1. CCDC: 600233. |
| 关 键 词： | Zn(Ⅱ)配合物 谱学表征 晶体结构 |
| 文章编号： | 1001-4861(2006)10-1925-04 |
| 收稿时间： | 2006-03-13 |
| 修稿时间： | 2006-08-31 |
Synthesis, Crystal Structure and Spectral Characterization of the Complex [Zn(CF3COO)2(C7H6NS)2] |
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| MA Wei-Xing,QIAN Bao-Hu,LI Shan-Zhong,WANG Jian,XU Xing-You,LU Lu-De and SONG Hai-Bin.Synthesis, Crystal Structure and Spectral Characterization of the Complex [Zn(CF3COO)2(C7H6NS)2][J].Chinese Journal of Inorganic Chemistry,2006,22(10):1925-1928. | |
| Authors: | MA Wei-Xing QIAN Bao-Hu LI Shan-Zhong WANG Jian XU Xing-You LU Lu-De and SONG Hai-Bin |
| Affiliation: | Jiangsu Provincial Key Laboratory of Ocean Biotechnology, Huaihai Institute of Technology, Lianyungang, Jiangsu 222005;Dept. of Chemical Technology, Huaihai Institute of Technology, Lianyungang, Jiangsu 222005,Dept. of Chemical Technology, Huaihai Institute of Technology, Lianyungang, Jiangsu 222005;Materials Chemistry Laboratory, Nanjing University of Science & Technology, Nanjing 210094,Dept. of Chemical Technology, Huaihai Institute of Technology, Lianyungang, Jiangsu 222005;Materials Chemistry Laboratory, Nanjing University of Science & Technology, Nanjing 210094,Dept. of Chemical Technology, Huaihai Institute of Technology, Lianyungang, Jiangsu 222005;Materials Chemistry Laboratory, Nanjing University of Science & Technology, Nanjing 210094,Dept. of Chemical Technology, Huaihai Institute of Technology, Lianyungang, Jiangsu 222005;Materials Chemistry Laboratory, Nanjing University of Science & Technology, Nanjing 210094,Materials Chemistry Laboratory, Nanjing University of Science & Technology, Nanjing 210094 and College of Chemistry, Nankai University, Tianjin 300071 |
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