| 2，4－二硝基－6－氰苯胺的合成研究 |
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| 引用本文： | 朱惠祥,笪远峰,张启兴. 2，4－二硝基－6－氰苯胺的合成研究[J]. 江苏化工, 1994, 0(4) |
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| 作者姓名： | 朱惠祥 笪远峰 张启兴 |
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| 作者单位： | 南京大学化学化工学院，镇江医学院，南京金陵化工厂 |
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| 摘 要： | 以水杨酸为原料，经硝化、酰卤化、氨化等三步反应，得到重要的染料中间体２，４－二硝基－６－氰苯胺，总收率７０．５％。
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| 关 键 词： | 染料中间体，水杨酸，硝化，酰胺，氨解 |
Synthesis of 2, 4-dinitro- 6-Cyanoaniline |
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| Zhu Huixiang Da Yuanfeng. Synthesis of 2, 4-dinitro- 6-Cyanoaniline[J]. Jiangsu Chemical Industry, 1994, 0(4) |
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| Authors: | Zhu Huixiang Da Yuanfeng |
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| Affiliation: | (4)Zhu Huixiang (College of Chemistry and Chemical Technology,Nanjing University,210008 )Da Yuanfeng (Zhengjiang Medical College,212008 ) |
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| Abstract: | Dinitro-6-cyanoaniline is an important azo-dye intermediate. It was synthesized by nitration of salycylic acid followed by acyl-halogenation and amination.The overall yield was 70. 5%. |
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| Keywords: | s: dye intermediate salycylic acid nitration amide amination |
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