| 氯甲基-乙氧基-二甲基硅烷的合成研究 |
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| 引用本文： | 陈献军. 氯甲基-乙氧基-二甲基硅烷的合成研究[J]. 精细化工中间体, 2013, 43(3): 54-56 |
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| 作者姓名： | 陈献军 |
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| 作者单位： | 天铁集团崇利制钢有限公司,河北涉县,056400 |
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| 摘 要： | 研究了以乙醇和氯甲基二甲基氯硅烷为原料合成氯甲基-乙氧基-二甲基硅烷的实验方法。探讨了反应溶剂、反应温度和氯化氢去除方式等影响因素,得出了适宜的反应条件:反应溶剂为石油醚,反应温度65℃,用尿素做缚酸剂去除氯化氢,收率92%,产物纯度98%。
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| 关 键 词： | 氯甲基-乙氧基-二甲基硅烷 氯甲基二甲基氯硅烷 乙醇 |
Synthesis of Chloromethyl-ethoxy-dimethylsilane |
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| CHEN Xian-jun. Synthesis of Chloromethyl-ethoxy-dimethylsilane[J]. Fine Chemical Intermediates, 2013, 43(3): 54-56 |
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| Authors: | CHEN Xian-jun |
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| Affiliation: | CHEN Xian-jun(Chongli Steel Co.,Ltd.,Tiantie Group,Shexian 056400,China) |
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| Abstract: | Chloromethyl dimethylchlorosilane was synthesized by the reaction of chloromethyl ethoxy dimethylsilane with ethanol and the reaction conditions were optimized.The target product was obtained in 92% yield（purity 98%） while the reaction was conducted in petroleum ether at 65℃ using urea as the acid-binding agent. |
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| Keywords: | chloromethyl-ethoxy-dimethylsilane chloromethyl-dimethylchlorosilane ethanol |
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