| 烷基胺插层层状化合物LiNbWO_6纳米复合材料的研究 |
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| 引用本文： | 汪胜,刘超,张晓波,童志伟. 烷基胺插层层状化合物LiNbWO_6纳米复合材料的研究[J]. 淮海工学院学报, 2010, 19(2): 41-44 |
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| 作者姓名： | 汪胜 刘超 张晓波 童志伟 |
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| 作者单位： | 汪胜,刘超(南京工业大学材料科学与工程学院,江苏,南京,210009;淮海工学院化学工程学院,江苏,连云港,222005);张晓波(淮海工学院化学工程学院,江苏,连云港,222005;江苏省海洋资源开发研究院,江苏,连云港,222001);童志伟(淮海工学院化学工程学院,江苏,连云港,222005;江苏省海洋资源开发研究院,江苏,连云港,222001;日本科学与技术振兴机构,日本崎玉县,川口市,332-0012) |
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| 基金项目： | 国家自然科学基金资助项目，江苏省高等学校大学生实践创新训练计划资助项目 |
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| 摘 要： | LiNbWO6作为一种无机层状化合物,是制备有机-无机物纳米复合材料的优良基体。使用高温固相方法合成LiNbWO6,并用直接插入法分别将正丙胺、正丁胺、正己胺、正辛胺插入HNbWO6层间制备了烷基胺的插层复合材料,并用SEM,XRD等方法进行了表征,同时研究了层间距的增加与烷基胺中碳原子数目之间的关系。
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| 关 键 词： | LiNbWO6 烷基胺 纳米复合材料 插层反应 |
Synthesis and Characterization of Nanocomposite Material Alkylamine Intercalated into Layered Compound LiNbWO6 |
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| WANG Sheng,LIU Chao,ZHANG Xiao-bo,TONG Zhi-wei. Synthesis and Characterization of Nanocomposite Material Alkylamine Intercalated into Layered Compound LiNbWO6[J]. Journal of Huaihai Institute of Technology:Natural Sciences Edition, 2010, 19(2): 41-44 |
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| Authors: | WANG Sheng LIU Chao ZHANG Xiao-bo TONG Zhi-wei |
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| Affiliation: | 1.School of Materials Science ＆ Engineering,Nanjing University of Technology,Nanjing 210009,China; 2. School of Chemical Engineering,Huaihai Institute of Technology,Lianyungang 222005,China; 3. Jiangsu Marine Resources Development Research Institute,Lianyungang 222001,China; 4. Japan Science and Technology Agency,Kawaguchi-shi 332-0012,Japan) |
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| Abstract: | LiNbWO6 is a well-defined layered inorganic material and an excellent base to prepare organic-inorganic nanocomposites. In this paper,LiNbWO6 microcrystalline were prepared by means of high temperature solid state synthesis method,and then n-propylamine,n-butylamine,n-hexylamine and n-octylamine were directly intercalated into the HNbWO6 layers to fabricate alkylamine nanocomposite by the guest-guest ion exchange method. The structure and the morphology of the nanocompostive were characterized by scanning electronic microscopy （SEM） and X-ray diffraction （XRD）. Moreover,the relation of the interlayer distance of intercalates and the number of carbon atoms in alkylamine was investigated systematically. |
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| Keywords: | LiNbWO6 |
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