Effects of hydrothermal temperatures on properties of magnetic titanate nanotubes |
| |
Authors: | XIA Shu-mei XU Chang-song DU Yan-yan ZHANG Mi-lin |
| |
Affiliation: | [1]College of Material Science and Chemical Engineering, Harbin Engineering University, Harbin 150001, China [2]College of power and energy Engineering, Harbin Engineering University, Harbin 150001, China |
| |
Abstract: | NiFe2O4 dopeded with magnetic titanate nanotubes(MTNT)were prepared by a hydrothermal method using magnetic nanoparticles TiO2/SiO2/NiFe2O4 as the precursor.The effects of hydrothermal temperatures on their composition,morphologies and magnetic properties of products were characterized by transmission electron microscopy(TEM),scanning electron microscopy(SEM),X-ray diffraction(XRD),vibration sample magnetometer(VSM)and energy dispersive X-ray spectroscopy(EDS).The results show that the hydrothermal temperature has a significant impact on the morphology of the products.The MTNT is synthesized in the temperature range of 120-160 ℃ and the inner diameter of MTNT is about 3-10 nm,the wall thickness 4-12nm and the length 100-200 nm.The components of MTNT are Na0.8H12Ti3O7 and a little of anatase TiO2 and NiFe2O4.The ferrimagnetisms and magnetic hysteresis phenomena are shown in the prepared MTNT.The hydrothermal temperature has no clear effect on the magnetic properties in the range of 120-180 ℃.The visiblelight photo-catalytic activity of the products decreases as the temperature increases.The decolorization of methylene blue is 94.6% by the MTNT obtained at 120 ℃ and the recovery rate of MTNT is more than 95 percent.The MTNT has excellent photocatalytic activity and is easy to recovery. |
| |
Keywords: | magnetic titanate nanotubes hydrothennal method doping |
本文献已被 CNKI 维普 万方数据 等数据库收录! |
| 点击此处可从《哈尔滨工业大学学报(英文版)》浏览原始摘要信息 |
|
点击此处可从《哈尔滨工业大学学报(英文版)》下载全文 |