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痕量硫示波极谱的测定
引用本文:钱俊青.痕量硫示波极谱的测定[J].食品与生物技术学报,2001,20(2):177-180.
作者姓名:钱俊青
作者单位:浙江工业大学生物环境工程学院,
摘    要:选择硼砂溶液为测定介质,以抗坏血酸(Vc)除去介质中的氧,研究了示波极谱测定痕量硫的方法,并初步探讨了其机理.硫浓度在1.0×10

关 键 词:  痕量  示波极谱  水样
文章编号:1009-038X(2001)02-0177-04
修稿时间:2000年3月24日

The Determination of Visigraph Polarography for Trace Sulphur
QIAN Jun,qing.The Determination of Visigraph Polarography for Trace Sulphur[J].Journal of Food Science and Biotechnology,2001,20(2):177-180.
Authors:QIAN Jun  qing
Abstract:In this paper, the alkalinity borax solution of pH 10 was selected for medium of determination. To eliminate the oxygen in the medium by Vitamin C, the method of determination of trace sulphur with visigiph polargraphy was studied by the test, and mechanism of method was preliminarily explored. There is good linearity that the concentration of sulphur was between 1.0×10-5~1.0×10-7 mol/L. Limit of detection was 5.0×10-8 mol/L. The relative standard deviation of method was 0.49%. The disturbance of usual metal ion can be eliminated with the suitable shelter. The results might get satisfied that method was applied to determin various water specimens.
Keywords:sulphur  trace  visigraph polarography  water specimen
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