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红橘油中脂肪酸组成的 GC-MS分析
引用本文:李英,刘志红,刘丽.红橘油中脂肪酸组成的 GC-MS分析[J].分析测试学报,2001,20(5):81-82.
作者姓名:李英  刘志红  刘丽
作者单位:深圳出入境检验检疫局工业品检测技术中心
摘    要:用正己烷溶解达川和万县产的两种红橘油,将样品皂化和甲酯化后,以毛细管柱DB-WAX作为分离柱,用气相色谱-质谱法测定其中的脂肪酸组成,两种红橘油的主要脂肪酸成分有明显的差别,两者的不饱和脂肪酸相对含量分别为92.1%及76.7%。

关 键 词:红橘油  脂肪酸  气相色谱-质谱法  GC-MS  分析  植物香料
文章编号:1004-4957(2001)05-0081-02
修稿时间:2000年10月26

Analysis of Fatty Acids in Tangerine Oil by GC-MS
LI Ying,LIU Zhi _ hong,LIU Li.Analysis of Fatty Acids in Tangerine Oil by GC-MS[J].Journal of Instrumental Analysis,2001,20(5):81-82.
Authors:LI Ying  LIU Zhi _ hong  LIU Li
Abstract:Two tangerine oil samples from different places of production were dissolved in hexane. The fatty acids of them were saponified and methylated in KOH-CH3OH solution, then separated in capillary DB _ WAX column and identified by GC-MS. Their relative contents were quantified by normalizing method of area. There are distinct differences of main fatty acid components between the two. The relative content of unsaturated acids in tangerine oil was 92.1% for the oil from Dachuan and 76.7% for the oil from Wanxian.
Keywords:Tangerine oil  Fatty acid  GC-MS
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