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Polymer networks in which poly(propylene imine) dendrimers (Astramol?) are connected to each other by linear polytetrahydrofuran (polyTHF) segments, were prepared by two methods. The first method was a one‐step procedure in which bifunctionally living polyTHF, obtained by initiation of the THF polymerization with trifluoromethane sulfonic anhydride (triflic anhydride), was reacted with an amino‐dendrimer. This reaction was very fast but did not allow formation of the end products. The second method was a two‐step procedure. In a first step, living polyTHF, prepared with acryloyloxybutyl triflate as initiator, was grafted on an amino‐dendrimer, to form a star‐like, acrylate‐terminated polyTHF multi‐macromonomer with the dendrimer as core. In a second step, networks were obtained by Michael addition between the acrylate end‐groups and unreacted amino‐groups of the dendrimer. This cross‐linking reaction occurred spontaneously upon heating of the solution of the multi‐macromonomer with gelation times varying from a few minutes to a few hours, depending on the temperature and the composition of the prepolymers. With this method it was possible to prepare networks in the form of coatings or films. © 2003 Society of Chemical Industry 相似文献
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报导一种模糊逻辑控制系统的建模与优化方法。以此方法设计的模糊逻辑控制器,用于双波长稳频CO2激光器的控制得到令人满意的结果。 相似文献
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Panagiotis N. Zarros Myung J. Lee Tarek N. Saadawi 《Journal of Network and Systems Management》1994,2(4):361-382
In this paper, an algorithm to determine the set of packets generated continuously and periodically from different participants that are arriving at a node either for mixing at the master of a conference, or for simply playing back at a regular participant of a conference, is proposed. The essence of the algorithm is to estimate the expected packet arrival time (or reference time) for each participant. With the reference time at hand, the maximum jitter and the optimum waiting time for a mixer to wait packets from all participants can be determined. An enhancement to improve synchronization which deals with the estimation of the time offsets between the individual periods of the sources and the period of the receiver is also presented. The error of the proposed algorithm is enumerated by the Chernoff bound and demonstrated by simulation and is shown to be acceptable in practical application. The algorithm can also be employed when traffic sources operate with different periods. 相似文献
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阐述了城域光网络(MON)技术的出现背景、定义、技术方案和特点,以及与现有城域基础设施的比较,突出说明了其应用上的竞争优势。最后介绍了MON的现状和前景展望。 相似文献
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标签粘贴机是一种可自动进行标签打印和粘贴的设备装置,在工业自动化生产中有着广泛的应用.介绍了一种采用单台微机进行控制的全自动标签粘贴机的工作原理及各部分组成,以及使用过程中对其进行设置和调整的方法.该标签粘贴机已实际应用于华飞彩色显示系统有限公司29英寸彩色显像管生产线的屏网组装工序,取得了良好的效果. 相似文献
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