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1.
N. Balchev D. Kovacheva V. Lovchinov K. Konstantinov K. Petrov 《Journal of Superconductivity》1993,6(1):49-54
The preparation conditions, phase composition, and superconducting properties of Bi-Pb-Sr-Ca-Cu oxide materials from different nominal compositions have been investigated. Nearly single-phase samples from Bi2Pb0.4Sr2Ca3Cu4O
y
, as well as from the proposed compositions Bi1.8Pb0.4Sr2Ca3Cu4O
y
and Bi1.8Pb0.4Sr2Ca2.5Cu3.5O
y
were obtained by a solid-state reaction in air. Samples with the third nominal composition showed the best superconducting properties (T
on=111 K and zero resistance atT
0=103 K). A possible mechanism for the 2223 phase formation in the three investigated compositions has been discussed. 相似文献
2.
V. V. Tcherdyntsev S. D. Kaloshkin A. I. Salimon E. A. Leonova I. A. Tomilin J. Eckert F. Schurack V. D. Rogozin S. P. Pisarev Yu. P. Trykov 《Materials and Manufacturing Processes》2002,17(6):825-841
Al-Cu-Fe alloys were prepared from elemental powders in a high-energy planetary ball mill. A sequence of solid state reactions resulting in quasicrystal (QC) phase formation takes place during heating of the as-milled powder. These reactions were studied by both differential scanning calorimetry and x-ray diffraction methods. Mechanically alloyed powders were consolidated by cold and hot pressing, as well as by explosive compaction. After annealing at sufficiently high temperatures, the consolidated samples are single-phase QC, except the ones consolidated by explosion. The high reactivity of the as-milled alloys causes the appearance of high porosity of the consolidated samples after the annealing. 相似文献
3.
In this paper, a new approach for powder cold compaction simulations is presented. A density-dependent plastic model within
the framework of finite strain multiplicative hyperelastoplasticity is used to describe the highly nonlinear material behaviour;
the Coulomb dry friction model is used to capture friction effects at die-powder contact; and an Arbitrary Lagrangian–Eulerian
(ALE) formulation is used to avoid the (usual) excessive distortion of Lagrangian meshes caused by large mass fluxes. Several
representative examples, involving structured and unstructured meshes are simulated. The results obtained agree with the experimental
data and other numerical results reported in the literature. It is shown that, contrary to other Lagrangian and adaptive h-remeshing approaches recently reported for this type of problems, the present approach verifies the mass conservation principle
with very low relative errors (less than 1% in all ALE examples and exactly in the pure Lagrangian examples). Moreover, thanks
to the use of an ALE formulation and in contrast with other simulations, the presented density distributions do not present
spurious oscillations.
Received: 20 March 2002 / Accepted: 15 October 2002
The partial financial support of the Ministerio de Ciencia y Tecnología (grant number DPI 2001-2204) is gratefully acknowledged. 相似文献
4.
5.
J. Clausen L. Damkilde L. Andersen 《International journal for numerical methods in engineering》2006,66(6):1036-1059
A new return method for implicit integration of linear isotropic yield criteria is presented. The basic idea is to perform all the manipulations in the principal stress space and thereby achieve very simple formulae for calculating the plastic corrector stresses, based on the constant gradient of such criteria. The return formulae are in closed form and no iteration is required. The method accounts for three types of stress return: return to a single yield plane, to a discontinuity line at the intersection of two yield planes and to a discontinuity point at the intersection between three or more yield planes. The infinitesimal and the consistent elastoplastic constitutive matrix are calculated for each type of stress return, as are the conditions to ascertain which type of return is required. The method is exemplified with the Mohr–Coulomb yield criterion. Copyright © 2005 John Wiley & Sons, Ltd. 相似文献
6.
Stirman Shannon Wiltsey; DeRubeis Robert J.; Crits-Christoph Paul; Brody Pamela E. 《Canadian Metallurgical Quarterly》2003,71(6):963
To determine the extent to which published randomized controlled trials (RCTs) of psychotherapy can be generalized to a sample of community outpatients, the authors used a method of matching information obtained from outpatient charts to inclusion and exclusion criteria from published RCT studies. They found that 80% of the patients in their sample who had diagnoses represented in the RCT literature were judged eligible for at least 1 published RCT; however, 58% of the patients had primary diagnoses such as adjustment disorder or dysthymia, which were not represented in the existing psychotherapy outcome literature. The most common reasons that patients in their sample did not match with published RCTs for psychotherapy are listed, and the implications of these findings for research and practice are discussed. (PsycINFO Database Record (c) 2010 APA, all rights reserved) 相似文献
7.
Miguel Eduardo L. Felismino Paul A. Helm Chelsea M. Rochman 《Journal of Great Lakes research》2021,47(1):180-189
Microplastics (plastic particles <5 mm in size) have been reported in ecosystems worldwide and have been shown to cause adverse negative impacts on organisms. This study provides the first report of microplastics and other anthropogenic microparticles in the surface waters and sediments of Lake Simcoe in Ontario, Canada, a popular recreational and fishing lake. Surface waters (low volume grabs and manta trawls) and sediments were sampled from eight sites to determine microparticle abundances and character (size, morphology, material identity). Concentrations ranged from 0 to 0.7 particles/L in surface water grab samples, 0.4–1.3 particles/m3 in manta trawl samples, and 8.3–1070 particles/kg in sediment samples. Spectroscopic analysis confirmed that 72% of particles were anthropogenic, with 64% unambiguously identified as microplastics. However, confirmed microplastic concentrations were approximately 6–7 times lower than unadjusted counts in sediments, demonstrating the importance of verifying and adjusting reported values. Fibers were only quantified and characterized in surface water grab samples and sediments, and were the most common morphology, accounting for 82% and 89% of anthropogenic particles, respectively. Fragments were most common in manta trawl samples (75%, excluding fibers) and consisted predominantly of polyethylene (41%) and polypropylene (22%). The influence of proximity to urban centers and prevailing winds on the distribution of microplastics was apparent in surface water manta trawls. Microplastics and other anthropogenic microparticles are present in Lake Simcoe but at lower abundances than at locations impacted by larger population centers in other large freshwater lakes such as Lakes Ontario and Erie of the Great Lakes. 相似文献
8.
Abstract. Consider an AR(1) process given by X t =γ+ø X t + Z t ≥ 1. where 0 ≤γ, 0 ≤ø 1 are unknown parameters and the innovations Z t , ≥ 1, are independently and identically distributed positive random variables. We propose estimates of (γø) which are obtained as the solution to a linear programming problem and establish their strong consistency. When the Z t s have the exponential distribution. our estimate becomes the conditional maximum likelihood estimate given X 0 . Under the assumption of regular variation of the innovation distribution at its left and right endpoints (assumed to be 0 and ∝ respectively), we establish asymptotic limit laws for the estimates. Consistent estimators for a class of moving-average processes with heavy-tailed innovation distribution are also presented. 相似文献
9.
Mariem Nafti Chiraz Hannachi Jaber Hsaini Béchir Hamrouni Habib Nouaïgui 《分离科学与技术》2020,55(15):2772-2778
ABSTRACT A new approach of cloud point extraction CPE procedure is optimized for hexavalent chromium determination in airborne dusts. Triton X-114 is used as a surfactant and 1-(2-pyridylazo)-2-naphthol as a specific complexing agent for the trivalent chromium’s removal from the aqueous phase to isolate hexavalent chromium compounds. The parameters influencing the extraction protocol (pH, surfactant concentration, and temperature are optimized. The obtained detection and quantification limits are 0.1 and 0.4 μg/L, respectively. The linearity is verified, with a regression coefficient close to 0.999 and the extraction recovery exceeds 99%. The method was successfully applied to analyze airborne samples collected from workplaces. 相似文献
10.
钱永江 《延边大学学报(自然科学版)》2009,35(3):207-210
讨论了缺失数据在随机补充方式下均值的估计,证明了估计的相合性和渐进正态性,并给出了经验似然比统计量的渐进分布. 相似文献