预处理工艺对硬质合金与金刚石膜间粘结力的影响

在两种经不同预处理的硬质合金YG8基底上，采用微波等离子体化学气相沉积法，在微波功率2kW，压强4.0kPa和6.5kPa，CH4和H2流量分别为1.6cm/s和100.0cm/s的条件下生长金刚石薄膜。利用X射线衍射检测了金刚石薄膜是否存在，用拉曼光谱分析了薄膜的质量，用金相显微镜观察了薄膜的洛氏硬度压痕，标定并比较了不同预处理工艺膜与基底的结合力。实验结果表明，不同的预处理方法对于粘结力的影响不大，最主要的因素是钴含量的多少。     

Rheological and drug‐release behaviour of a scleroglucan gel matrix at different drug loadings

The aim of this study was to investigate the drug‐loading effects on release and mechanical properties of a scleroglucan gel, with the intention of considering them in delivery systems formulations. The rheological and kinetic properties of a 2 % w/w scleroglucan gel matrix loaded with 0, 0.02, 0.04, 0.06, 0.2 and 0.4 % w/w of theophylline (Th, used as a model drug) were investigated. Rheological measurements were performed in a controlled‐stress rotational‐shear rheometer under isothermal conditions. For theophylline release from the gel a flat Franz cell was used and the kinetic parameters were derived applying a semi‐empirical power law. The influence of scleroglucan molar weight on kinetic and rheological behaviour was also studied. Results suggest two possible effects of drug loading on the gel network: in the 0.04–0.06 % w/w Th range a plasticizing effect and in the 0.2–0.4 % w/w Th range a rigidization effect. In the first range mentioned, the changes in the gel structural properties tested by means of rheological measurements are coincident with changes in drug‐release kinetics. Copyright © 2005 Society of Chemical Industry     

Dynamic response and behavior of reinforced concrete slabs under impact loading

Reinforced concrete slabs are among the most common structural elements. In spite of the large number of slabs designed and built, the effect of their details on their behavior under impact loads are not always appreciated or properly taken into account. This experimental study was aimed at understanding the dynamic behavior of structural concrete slabs under impact loading to improve the state of the art of protective design. This study investigated the effects of different types of slab reinforcements and the applied impact loads on the dynamic response and behavior of reinforced concrete slabs.     

Behaviors of concrete-filled steel tubular members subjected to combined loading

The present study is an investigation on the behaviors of concrete-filled thin-walled steel tubular members subjected to combined loading, such as compression and torsion, bending and torsion, compression, bending and torsion. ABAQUS software is used in this paper for the finite element analysis (FEA). A comparison of results calculated using this modeling shows generally good agreement with test results. The FEA modeling is then used to investigate the influence of important parameters that determine the ultimate strength of the composite members under combined loading, such as compression and torsion, bending and torsion, compression, bending and torsion. The parametric studies provide information for the development of formulae for calculating the ultimate strength of the composite members subjected to combined loading.     

Equipment for Testing Sheet Structural Materials under Biaxial Tension. Part 2. Testing by Biaxial Loading in the Plane of the Sheet

We analyze specific features of the design of equipment used for mechanical testing of sheet structural materials under the conditions of biaxial static, cyclic, or dynamic loading. We propose original solutions of the problems related to the fatigue testing of crosslike specimens performed without using complex hydraulic systems and their dynamic testing carried out by using very simple testing machines for uniaxial tension–compression.     

Analytical Calculation of Large-Scale Deflection of Pulse-Loaded Elliptic Plates

Large deflections of pulse-loaded elliptic and round plates made of hardenable elastoplastic materials are investigated analytically using an energy-based approach. Formulas that are convenient for engineering design have been derived.     

结构陶瓷的高温疲劳强度衰减理论

提出了陶瓷材料疲劳强度衰减理论并由此导出了各种疲劳关系式。建立了疲劳基本方程ｄσ＿ｒ／ｄ＿ｉ＝一Ａσ（ｔ）￣ｎｔ￣（－ｍ），得出了疲劳寿命公式Ｔ＝Ｍ（σ＿０－σ）／Ａσ￣ｎ（静疲劳时Ｍ＝１，连续增载疲劳时Ｍ＝ｎ＋１，循环疲劳时Ｍ＝（ｎ＋１）／（１＋Ｒ＋Ｒ￣２＋……＋Ｒ￣ｎ），逐级加载时，并导出不同疲劳方式下疲劳寿命间的关系。同时，用多种Ｓｉ＿３Ｎ＿４材料在高温中作了论证试验，结果与理论一致。     

连续式超临界流体萃取进卸料装置

概括了超临界流体萃取技术和包括连续式操作在内的超临界流体萃取装置的研究现状 ,提出了一种通过球形进、卸料器完成固相物料超临界流体萃取连续化进卸料的装置 ,介绍了该装置的结构和工作原理 ,给出装置中各主要部件的计算方法。     

Strength of Metals at High Strain Rates

Results of metal testing in impact tension–compression and indentation are analyzed. As the analysis of these data demonstrates, the strength of metals increases greatly with strain rates and at moderate indentation rates. At high indentation rates, a decrease in the specific energy (per unit volume of a displaced material) necessary for the formation of a conical cavity was observed. The account of the effects of viscosity, temperature increase upon plastic deformation and its localization can be used to explain the above phenomena.