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Esteve-Turrillas FA Armenta S Moros J Garrigues S Pastor A de la Guardia M 《Journal of chromatography. A》2005,1065(2):321-325
A non-destructive, fast and environmentally friendly procedure has been developed for cocaine determination in euro bank notes. Cocaine was extracted with 15 ml methanol by vortex agitation during 5 min. The extract was evaporated and reconstituted in 0.5 ml methanol. GC-MS-MS analysis was performed using as precursor ion m/z 182.2, with an excitation energy voltage of 1.60 eV, being the product ions measured m/z 150.2 and 82.0. A limit of detection of 0.15 ng per note and a repeatability of 6%, established from the relative standard deviation, of a 1 ng ml(-1) level, were achieved. Recoveries of 101+/-2 and 98+/-3% were obtained for samples spiked with 100 and 10 microg respectively. Results show that all the euro bank notes measured (16 samples) were contaminated with cocaine in the range between 1.25 and 889 microg. Two different contamination levels, high level (150-889 microg) and low one (1.25-77 microg) were found and it could be related with the direct or indirect contact with the drug. 相似文献
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Ray Nichol Jim Robinson 《International Journal of Mathematical Education in Science & Technology》2013,44(4):495-504
After the invasion and occupation of their land by Europeans, Indigenous Australians were expected to benefit from a Western education system based on that of the dominant Europeans. Gradually educators realized that Aboriginal children learn differently and that Indigenous culture and pedagogy has validity and strength. Of course, educators also need to be acutely aware of the diversity of Indigenous cultures in Australia and that there is not a monolithic sense of Aboriginal identity or Aboriginal pedagogy. Dispossession and alienation, poor health and few employment opportunities must also affect educational interest, attendance, application and performance. In this paper the characteristics of Indigenous learners are examined and pedagogical strategies to assist in both students' learning and teachers' delivery are explored. The message conveyed in this paper has particular relevance for teaching mathematics to Aboriginal learners. It is also of considerable value in teaching mathematics to nonAboriginal students, in Australia and elsewhere. 相似文献
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王永刚 龚靖School of Civil Engineering Mechanics Xi'an Jiaotong University Xi'an P.R.China Department of Civil Engineering Northeast China Institute of Electric Power Jilin P.R.China 张景绘School of Civil Engineering Mechanics Xi'an Jiaotong University Xi'an P.R.China 《应用数学和力学(英文版)》2004,(8)
IntroductionThestudiedobjectintheclassicstructuredynamicsisthepassivestructureswhicharechangedintoactivestructurewhencontroldevicesorsmartmaterialsareintroducedintoandthecontrolfunctionisapplied .Anactivestructureisgenerallycalledactivesystem .Asforthedefinitionofactivestructure ,itistheconceptofworthydiscussion[1].Thedefinitionshouldbebecomingrigorouswiththestudyontheactivestructuraldynamics.Withincertaincategoryofactivestructuresinpaper (Ⅰ ) [2 ],someattributesaboutthemodesoflinearactivest… 相似文献
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We provide analytic pricing formulas for Fixed and Floating Range Accrual Notes within the multifactor Wishart affine framework which extends significantly the standard affine model. Using estimates for three short rate models, two of which are based on the Wishart process whilst the third one belongs to the standard affine framework, we price these structured products using the FFT methodology. Thanks to the Wishart tractability the hedge ratios are also easily computed. As the models are estimated on the same dataset, our results illustrate how the fit discrepancies (meaning differences in the likelihood functions) between models translate in terms of derivatives pricing errors, and we show that the models can produce different price evolutions for the Range Accrual Notes. The differences can be substantial and underline the importance of model risk both from a static and a dynamic perspective. These results are confirmed by an analysis performed at the hedge ratios level. 相似文献
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本文从定义信用违约联结票券出发,介绍了JarrowandTurnbul(1995)违约强度模型。然后在该模型的基础上,针对不同的公司,假设违约时间独立同服从指数分布且与利率期间结构独立,分别就t=0与0 相似文献
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ZHENG ShiJun 《分析论及其应用》2004,20(3)
Schr(o)dinger operator is a central subject in the mathematical study of quantum mechanics.Consider the Schrodinger operator H = -△ V on R, where △ = d2/dx2 and the potential function V is real valued. In Fourier analysis, it is well-known that a square integrable function admits an expansion with exponentials as eigenfunctions of -△. A natural conjecture is that an L2 function admits a similar expansion in terms of "eigenfunctions" of H, a perturbation of the Laplacian (see [7], Ch. Ⅺ and the notes), under certain condition on V. 相似文献
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界定了笔记覆盖率的概念,对高中生化学课堂笔记覆盖率与学业成绩、记笔记习惯与学业成绩以及合成变量与学业成绩的相关性进行了检测,并依据检测的结果,提出了帮助学生做好课堂笔记以提升学习能力的教学建议。 相似文献
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