降低成品油二次物流运输成本的思考

介绍了传统成品油进货和管理模式存在的诸如成品油物流以行政区划、中问环节多、信息化程度不高、运输路线未优化造成物流成本提高等问题。提出要降低成品油二次物流运输成本，当务之急是加强成品油物流的信息化建设；调整管理模式，打破行政区域界限，开展经济辐射半径内的库站物流配送；引进竞争机制，打破运输垄断，一、二次物流结合，大、小车型搭配，提高运营效率；做好运杂费全面预算、核算及运行费用的过程控制。     

游梁式抽油机二次平衡分析

为解决游梁式抽油机能耗大、效率低的问题，设计了二次平衡装置。这种装置通过是挂在抽油机后端的平衡重的平衡作用，降低一次平衡曲柄轴净扭矩的两个峰值，达到减少能耗提高效率的目的。对抽油机的二次平衡作了较详尽的理论分析，给出了实行二次平衡后曲柄轴净扭矩的计算公式和安装二次平衡装置前后曲柄轴净扭矩曲线图。在大庆油田两口井上进行的现场试验结果表明，安装二次平衡装置后，两口井年节约电费分别为0.25万元和1．17万元，经济效益明显。     

超细Fe3O4粒子表面包覆酞菁钴性质研究

本文研究了合成载氧体的金属有机化学液相淀积法制造工艺，所得产物经ＴＥＭ、ＸＰＳ、Ｍｏｓｓ－ｂａｕｅｒ谱和Ｂ－Ｈ仪等手段，研究了它的结构和磁性能。实验表明，酞青钴以薄层形式包覆在Ｆｅ＿３Ｏ＿４的表面，封闭了Ｆｅ＿３Ｏ＿４的表面孔洞，稳定了Ｆｅ＿３Ｏ＿４的物相，增强了磁性能。     

高氯酸为催化剂乙酰化法测定伯醇或仲醇

提出了以主氯酸为催化剂，分析纯乙酸乙酯为介质，乙酸化法测定伯、仲醇的实验条件，实现了对经典方法的改进，简化了操作程序。     

8Li次级束的产生

在北京串列加速器次级束流线上通过2 H(7Li,8Li) 1H逆运动学反应产生了用于核天体物理研究的8Li次级束。准直后的次级束纯度达到 80 %以上 ,对于 44MeV的7Li强度约为 3 0s- 1·pnA- 1,可以用来进行逆几何转移反应的实验测量。     

过氧化甲乙酮合成研究

论述了过氧化甲乙酮的合成方法，用阳离子交换树脂催化剂代替传统的无机酸催化剂。考察了离子交换树脂用量、反应温度对反应产率、活性氧含量的影响及溶剂对产品稳定性的影响。     

转炉炼钢静态模型的初步探讨

根据转炉炼钢的物理化学反应机理，从质量平衡和能量平衡的计算出发，通过小参数变动，导出了增量式静态模型中矿石方程和供氧方程的系数。所得结论与新日铁资料基本相符。同时，还进行了炉料和产物的计算，分析了改变废钢比对生产的影响。     

An attempt to compare the performance of bioscrubbers and biotrickling filters for degradation of ethyl acetate in gas streams

This study presents a comparison of the efficiency of a bioscrubber and a biotrickling filter (BTF) for the removal of ethyl acetate (EA) vapour from a waste gas stream, under the same operating conditions. The maximum EA elimination capacity achieved in the bioscrubber was 550 g m^?3 h^?1 with removal efficiency higher than 96%. For higher EA loadings the bioscrubber was oxygen limited, which caused incomplete EA biodegradation. When pure oxygen was fed to the bioscrubber at a rate of 0.02 L min^?1, the bioscrubber recovered and could treat higher EA loadings without any oxygen limitation. The BTF achieved EA elimination capacity of 600 g m^?3 h^?1 with removal efficiency higher than 97% and the dissolved oxygen concentration remained substantially higher than in the bioscrubber. However, severe channelling and blockage of the spray nozzle occurred due to the excessive biomass growth. Overall, the bioscrubber system was easier to operate and control than the BTF, while an enhancement of the oxygen mass transfer in the bioscrubber could potentially increase its performance by up to three times. Copyright © 2005 Society of Chemical Industry     

Comparison of mass transfer efficiency in horizontal rotating packed beds and rotating biological contactors

In this study, the mass transfer efficiencies of a novel horizontal rotating packed (h‐RPB) bed and the conventional disc‐type rotating biological contactor (RBC) were studied at four speeds and seven submergences. Pall rings of two different sizes (25, 38 mm), superintalox saddles and a wiremesh spiral bundle were used as packings in the h‐RPB. Volumetric gas–liquid mass transfer coefficients were determined by unsteady state absorption of atmospheric oxygen in de‐aerated water. Power consumption per unit liquid volume has been found for all geometries tested. The oxygen transfer efficiency values for the h‐RPB were found to be 2–5 kg kWh^?1 and for the disc RBC were found to be 1–2 kg kWh^?1. The performance of the h‐RPB was also compared with other gas–liquid contactors such as surface aerators. The study proves that the h‐RPB is a energy efficient alternative to conventional contactors. Copyright © 2005 Society of Chemical Industry     

飞行时间二次离子质谱--强有力的表面、界面和薄膜分析手段

二次离子质谱（Secondary ion mass spectrometry，简称SIMS）是一种对表面灵敏的质谱技术，建立在表面各种类型带正、负电荷原子或分子发射的基础上。用飞行时间（Time of flight，简称TOF）仪器对这些二次离子进行质量分析，能确保并行质量登录、高质量范围、高流通率下的高分辨和精确质量测定这些优异性能。配合细聚焦扫描一次离子束，可在优于1nm的高深度分辨和优于50nm的横向分辨本领下，实现对表面优于单层ppm(百万分之一）量级的极高检测灵敏度。当今TOF－SIMS已发展为一种成熟且完善的表面分析技术。极高的灵敏度，再加上即使对大分子及不易挥发性分子都独具的敏感性，使它成为很多高技术领域不可缺少的分析手段，这些领域包括微电子学、化学和材料科学以至纳米技术和生命科学等。本文简述了TOF－SIMS的原理、仪器及其多方面的应用和展望。