A simple technique to minimize heat damage to specimens during thermal polymerization of LR White in plastic and gelatin capsules

London Resin (LR) White is a commonly used resin for embedding specimens to be used for immuno- and/or cytochemical studies. In some instances, due to either the properties of the specimen or the availability of various reagents and equipment, it becomes necessary and/or more convenient to polymerize LR White using heat rather than chemical accelerators or UV light. It is known, however, that heat can reduce or even eliminate the anti genicity of the tissue being embedded. It is therefore desirable to polymerize specimens at the lowest temperature possible and to remove the specimens from the oven as soon as polymerization is complete. We have developed a technique that provides a visual marker that allows the exothermic polymerization of LR White to be monitored, thus minimizing the amount of time a specimen must stay in the oven while excluding oxygen from capsules of polymerizing LR White.     

注塑件熔接缝结构,性能评价及影响因素

文章介绍了熔接缝形成的原因，接缝类型，接缝外观和断口形态特征以及接缝性能评价方法。分析了接缝类型，塑料材料性质，工艺参数和其它因素对接缝性能的影响。     

丙烯酸树脂涂料的近期进展

介绍了丙烯酸树脂涂料的国内外发展的概况及其性能和应用.提出了我国发展丙烯酸树脂涂料的建议。     

瓦楞纸板用抗水淀粉胶配方及性能研究

简要分析了玉米淀粉胶的组成及对其质量的影响，重点对粘合剂的防水性进行了研究，叙述了瓦楞纸板用抗水粘合剂的配制及工艺过程，并与常规方法制备的粘合剂进行了性能比较，测定了抗水时间，得出了瓦楞纸板用抗水粘合剂的最佳配制比例。     

Quilone试剂改性脲醛树脂——新型防水涂料的制备

叙述了Quilone试剂的合成,改性脲醛树脂的原理、实验方法、改性后脲醛树脂的抗水性、抗渗透性、耐化学药品性及其影响因素。     

Near-wall porosity characteristics of fixed beds packed with wood chips

Packed beds of fuel wood chips are commonly found in thermal conversion processes such as combustion or gasification. Wood chips in particular are mostly used as fuel for small-scale domestic heating boilers but also for commercial-scale combustion units. The characterization of spatial voidage distribution inside the wood chip beds is of great importance for flow and reactor modelling. This study focuses on the radial porosity variations of cylindrical beds of three different types of commercially available wood chips including chips classified as G30 size class. The conventional technique of consolidating packed beds with a resin was chosen as the experimental procedure. The radial voidage distribution in different cylindrical beds is determined by image analysis of sections of the solidified packings. Additionally, a packing of monosized spheres was investigated in order to assess the selected procedure in comparison with widely available literature data for spheres. The results are discussed and summarized in a mathematical expression correlating the radial voidage distribution depending on average wood chip size, packing core porosity and dimensionless distance from the tube wall.     

4F0.06AC树脂吹塑薄膜技术的探讨

在加工应用试验的基础上。探讨了加工温度、吹胀比、超想线高度及设备对４Ｆ０．０６ＡＣ薄膜适宜的加工条件。     

脲醛呋喃树脂中氮含量的测定

脲醛呋喃树脂中的含氮量,一般采用克氏定氮法,方法繁琐,费时较长,不利于快速分析的要求,本文利用气相色谱法对脲醛呋喃树脂中的氮含量进行分析测定,并建立了测定方法.方法简捷、快速、重现性好,加标回收率在100.8～109.0之间,准确度较高,可很好的满足工业生产中快速分析的要求.     

覆膜砂工艺参数优化的研究

通过对覆膜全过程的分析和优化实验，确定影响覆膜砂性能的工艺因素主要有：原砂的加热温度、加入树脂后的混砂时间、加入固化剂的混砂时间等，为了获得最佳的工艺参数，对各个工艺参数进行了正交实验。实验结果表明：为获得较高的热态抗拉强度，可以选用砂温180℃，加树脂后的混砂时间为100S，加固化剂后的混制时间为40S，加硬脂酸钙后的混制时间为30S；为获得较好的常温抗拉强度，可以选用砂温180℃，加树脂后的混砂时间为80s，加固化剂后的混制时间为30s，加硬脂酸钙后的混制时间为20s。     

树脂砂型离心铸管表面粘砂缺陷的研究

研究了树脂砂型离心铸管表面质量及影响因素。结果表明，覆膜砂粒反和砂层厚反对铸件表面质量有显著影响。砂的粒度细时不易粘砂且铸件表面粗糙度高，而砂层厚度越薄表面质量越差，故至少需４ｍｍ厚的砂层。砂中加氧化铁粉时对防止粘砂不起作用，但砂层表面涂刷涂料时防止粘砂效果非常明显。