热处理工艺对Cu-Fe-P合金显微硬度及导电率的影响

自行设计了一种Cu Fe P系合金 ,研究了固溶温度、时效温度以及时效时间对该合金显微硬度和导电率的变化规律。结果表明 ,该合金的最佳固溶处理工艺为 90 0℃× 70min ,并在 4 0 0℃× 2h时效条件下具有较好的综合性能 ,显微硬度可达到 10 6 4HV0 1,导电率可达 82 3%IACS。试验结果还表明 ,在 4 0 0℃、5 0 0℃下时效 ,随着时间的延长合金显微硬度会出现两个峰值。     

Magnetic and mechanical properties of FeSi alloys with high Si content

The chemical vapor（CVD） deposition-diffusion method was applied to prepare FeSi alloys with high silicon content up to 6.5%. In spite of various deposition and post-annealing, the sample remains α-Fe bcc structure. The cross section of the composition was analyzed to evaluate the Si content and distribution before and after annealing. The results show that the soft magnetic properties are improved by increasing the silicon content. For the samples containing about 6.5% Si, the coercivity decreases to 60 from 237.3 A/m of the original. It is also obtained that, in addition to the Si content, Si distribution has a large influence on the core loss due to the effect of resistivity. The micro-hardnesses were also evaluated along the cross-section after various annealings.     

M2高速钢强脉冲离子束表面改性及其耐磨耐蚀性

针对陶瓷梯度涂层性能优良,在大气氛围下等离子喷涂制备涂层会受到空气氧化这一情况,在可控气氛（Ar气）中采用等离子喷涂的方法制取了NiCrBSi/Al₂O₃的梯度涂层,并且与大气条件下制取的NiCrBSi/Al₂O₃的梯度涂层进行对比.借助扫描电子显微镜（SEM）、x 射线衍射仪（XRD）对涂层的组织分布、相结构进行分析.结果表明：在Ar气和大气中梯度涂层的组织内部都没有明显的界面,实现了组织的连续变化;在Ar气中制取的梯度涂层的组织更加致密,被氧化的程度更低,质量更好.     

TiN/Cr/Al2O3 and TiN/Al2O3 hybrid coatings structure features and properties resulting from combined treatment

New experimental results are presented on the structure and the elemental and phase composition of hybrid coatings, which were deposited on a substrate of AISI 321 stainless steel using a combination of plasma-detonation, vacuum-arc and subsequent High-Current Electron Beam (HCEB) treatment. We found that an increase in energy density intensified mass transfer processes and resulted in changes in aluminum oxide phase composition (γ → α and β → α). Also we observed the formation of a nanocrystalline structure in Al₂O₃ coatings. Electron beam treatment of a hybrid coating surface induced higher adhesion, decreased the intensity of surface wear and increased corrosion resistance in a sulphuric acid solution. The corrosion resistance of the coatings was studied in several electrolytic solutions (0.5 M H₂SO₄, 1 M HCl, 0.75 M NaCl) using electrochemical techniques. In most cases the corrosion resistance was improved, except those in NaCl solutions. The nano-hardness of the protecting coating was 13 GPa before electron beam melting and 9 GPa after it (as a result of TiN and Al₂O₃ sub-layers mixing).     

Friction stir welding of AZ31 magnesium alloy

Friction stir welding (FSW) is an new solid-phase joining technology which has more advantages over fusion welding methods in welding of aluminum and other non-ferrous metals. The effects of welding parameters on mechanical properties and microstructure during friction stir welding of AZ31 magnesium alloy were studied in this paper. Microstructures and mechanical properties of the joints were investigated by means of optical microscopy, scanning electric microscopy ( SEM ) , micro-hardness analysis, and tensile test. Experimental results show that the magnesium alloy can be successfully welded by FSW method, and the ultimate tensile strength (UTS) of FSW joint reaches up to 90 percent of base metal. The microstructures of welded joints exhibit the variation from dynamically recrystallized fine grains to greatly deformed grains. Hardness in nugget zone was found lower than the base metal but not too obvious.     

Investigation of process parameters influence in abrasive water jet cutting of D2 steel

In the present experimental study, abrasive water jet (AWJ) cutting tests were conducted on D2 steel by different jet impingement angles and abrasive mesh sizes. The experimental data was statistically analyzed using the simos–grey relational method and ANOVA test. In addition, the outcome of influencing cutting parameters, namely jet pressure, jet impingement angle, and abrasive mesh size on the different response parameters, namely, the jet penetration, material removal rate, taper ratio, roughness, and topography, were studied. Micro-hardness test and surface morphology analysis were employed to examine the D2 cut surfaces at different AWJ cutting conditions. The chemical element study was performed to determine the abrasive particle contamination in the AWJ kerf wall cut surfaces. The ANOVA test result indicated the jet pressure and jet impingement angle as the influencing process parameters affecting the various performance characteristics of AWJ cutting. The overall AWJ cutting performance of the D2 steel has been improved through proper identification of the optimal process parameter settings, namely jet pressure 225?MPa, abrasive mesh size #100, and jet impingement angle 70° by the simos–grey relational analysis.     

Effect of heat treatment on the mechanical properties of FeCoZrWB bulk metallic glass

A Fe61Co10Zr5W4B20 bulk metallic glass (BMG) with a diameter of 2 mm was prepared by using copper mould suction casting. The X-ray diffraction (XRD), differential scanning calorimetry (DSC), micro-hardness and compression tests were adopted to investigate the structure, thermal stability, especially, the effect of heat treatment on the micro-hardness and compression strength of this BMG. The BMG exhibits micro-hardness of about 1 207 Hv and compression fracture strength of about 1 707.6 MPa. After being annealed below the onset of crystallization temperature, the micro-hardness almost keeps constant. But after being annealed above the peak of crystallization temperature, the micro-hardness increases firstly and then declines gradually with the elongation of annealing time. However, annealed for the same period of time, the micro-hardness will increase with the rise of annealing temperature, while the compression fracture strength will apparently decrease.     

Research on the inwall shot blasting of the S30432 high-pressure boiler tube

Inwall shot blasting is a method of improving the surface hardness and high temperature oxidation resistance of the S30432 high-pressure boiler tube.The differences on residual stress,sub-grain size,micro-hardness and structure between the S30432 inwall shot-blasting tube produced by Baosteel with six technological process parameters and the imported super 304H were studied systematically by contrast test research.It has been demonstrated that the S30432 obtains a higher residual stress,a deeper distributed layer and a better sub-grain size of the inwall field shot-blasting layer;the martensite content of the shot-blasting surface was low;and micro-hardness and structure refinement were better.After 2000 h' oxidation test under the 650℃/26MPa steam condition,steam oxidation resistance of the Baosteel steel tube shot-blasting surface was higher,the oxide layer was thinner,and was well combined with bulk material.     

Ti6Al4V钛合金表面蓝色微弧氧化膜的制备及性能

利用微弧氧化技术在Ti6Al4V钛合金表面制备出蓝色微弧氧化膜。对微弧氧化膜的微观形貌和元素组成进行了分析,并对微弧氧化膜的显微硬度进行了测试。结果表明:微弧氧化膜表面光整,呈均匀深蓝色,其主要由Ti、Mn、O和C四种元素组成,还含有少量的V、Al和Si元素;微弧氧化膜的表面粗糙度约为0.159μm,与钛合金的表面粗糙度相近;微弧氧化膜的显微硬度为5 437.4 MPa,显著高于钛合金的显微硬度。     

激光表面熔凝处理对30Cr2Ni4MoV转子钢高温水腐蚀性能的影响

进行了三种强度级别的30Cr2Ni4MoV钢的激光表面熔凝处理,用电化学极化曲线和高温应力腐蚀试验考察了其耐腐蚀性能。研究表明:激光熔凝处理后在30Cr2Ni4MoV表面形成了约10~20μm的致密马氏体硬化层和压应力状态,基材状态对激光熔凝硬化层的性能无明显影响,但激光功率增大会导致表面熔凝层硬度水平降低;激光表面熔凝处理使腐蚀电位左移,腐蚀电流密度减小,抗腐蚀性能明显增强。