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超临界CO_2萃取-气相色谱质谱法测定斑点叉尾鮰肌肉中的脂肪酸 总被引:1,自引:0,他引:1
采用超临界CO2萃取工艺、气相色谱-电子电离质谱(GC-EI-MS)法,建立了斑点叉尾鮰肌肉中脂肪酸的定性与定量分析方法。在CO2流速为30 L/h、温度45℃、压力25 MPa、时间100 min条件下进行超临界CO2萃取,所得油脂皂化10 min,采用三氟化硼法进行甲酯化衍生20 min,经HP-Innowax毛细管柱分离,电子电离质谱检测,以全扫描模式定性分析,选择离子扫描模式定量分析,饱和脂肪酸、单不饱和脂肪酸、双不饱和脂肪酸、多不饱和脂肪酸的定量离子分别为m/z74,55,67和79。14种脂肪酸甲酯的检出限和定量限分别在2.2~20μg/L和7.4~60μg/L之间;平均回收率为90.0%~111.2%,相对标准偏差为2.0%~5.9%。本方法灵敏度高、重复性好,可用于测定斑点叉尾鮰肌肉样品的脂肪酸。 相似文献
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利用相干渡越辐射(CTR)测量短和超短电子束团长度是国际上束测领域新发展的频域测量技术.文中理论分析和数值计算了北京自由电子激光装置的皮秒级的射频电子束团序列产生的CTR,当辐射波长在长于束长(4ps)时,渡越辐射发生相干增强效应;与非相干渡越辐射相比,当λ≥2πσz时,增强的倍数约等于束团中粒子的数目(108);CTR从亚毫米波到毫米波段呈宽带连续谱特性;渡越辐射能量主要集中在轴线附近,宏脉冲辐射能量高达几毫焦.设计采用偏振型束团长度测量系统,利用CTR自相关技术,实验测量该束团序列的纵向长度,并藉助傅里叶变换光谱法,推求束团电子分布. 相似文献
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With the development of free electron laser (FEL) and the international linear collider (ILC), the electron bunch length is getting smaller and smaller. The traveling-wave transverse RF deflecting structure is an important part of the RF deflecting method for bunch length measurement and phase space diagnostics. The operation mode in RF deflector is the ``TM11-like' mode. Since the TM11-like mode in this structure has a pair of degenerate dipole modes, two additional holes are provided on either side of each iris to stabilize the mode. The simulation and optimization have been done. A prototype has been fabricated and tested. The cold test results have been compared with the simulations of the first three modes. 相似文献
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Peking University is developing a 1.3 GHz superconducting accelerating section highpower THz freeelectron laser for the China Academy of Engineering Physics(CAEP). A compact fast/slow tuner has been developed by the Institute of High Energy Physics(IHEP) for the accelerating section to control Lorentz detuning, compensate for beam loading effect, microphonics and liquid helium pressure fluctuations. The tuner design, warm test and cold test of the first prototype are presented, which has a guiding significance for the manufacture of the formal tuner and cryomodule assembly. 相似文献
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