邻—(4—乙基苯甲酰基)苯甲酸的研究

本文阐述了通过Friedel-Crafts反应合成邻-(4-乙基苯甲酰基)苯甲酸的方法.研究了影响产物质量的因素,提出了适宜的工艺条件.     

Fe－Cu包埋团簇的制备及其微观结构的研究

基于溅射－气体－聚集（ＳＧＡ）形成团簇的原理，提出了蒸发－气体－聚集（ＥＧＡ）共沉积方法，并在方华膜载网上成功地制备了Ｆｅ－Ｃｕ纳米磁性包理团簇样品。ＴＥＭ／ＥＤ分析表明，样品中Ｆｅ团簇被Ｃｕ原子所包裹，形成了以Ｆｅ团簇为芯，Ｃｕ膜为壳的良好的芯－壳式包埋结构。当衬底温度由２５℃变化到２００℃时，样品形貌由弥散状过渡到集团状，直至形成大的块状；其结构也相应的由Ｆｅ－Ｃｕ多晶共存变化为一种不规则的单晶形态。     

国外化工数据编篡进展简介

介绍了美国ＤＩＰＰＲ、德国ＤＥＴＨＥＲＭ和日本ＮＩＳＴ的组织情况和编篡工作，从此得到启示，以求加速我国化工物性数据编篡工作的发展。     

基于单片机和线阵CMOS的激光三角测距传感器设计与实现

介绍一种基于STM32单片机和线阵CMOS传感器的激光三角测距传感器的系统实现。包括原理电路部分以及算法程序部分的设计与实现。     

Preparation of treelike and rodlike carboxymethylated nanocellulose and their effect on carboxymethyl cellulose films

In this work, carboxymethyl cellulose (CMC) with low substitution degree, followed by different posttreatments, was applied to prepare treelike CMC nanofibrils (CMCNFs) and rodlike CMC nanocrystals (CMCNCs), and their performance in CMC composite film was evaluated simultaneously. From transmission electron microscopy results, it was found that the treelike CMCNCFs exhibited a lager aspect ratio compared to the rodlike CMCNCs. As for reinforcing CMC film, 4 wt% was the best adding amount, at this time, the tensile strength of CMC/CMCNFs and CMC/CMCNCs composite films was increased by 72.1% and 47.3%, respectively. Moreover, adding these nanofillers to CMC also could enhance the thermal stability of composite films slightly, while the transmittance of composite films was reduced at the same time. In addition, CMC/CMCNFs film was designed as a packaging box to determine its performance. Therefore, this study could reveal the differences of properties for composites with different types of nanocellulose and provide a foundation for further application of nanocellulose.     

成型砂轮截面曲线光顺处理的近似双圆弧插补法及误差估算

在解决成型砂轮截面曲线的光顺处理问题时，作者提出了一种新的曲线数字化处理方法——近似双圆弧插补法，简化了计算过程。为了估算该方法的误差，本文模拟曲线反求的过程进行了仿真计算，计算结果表明：若曲线反求时测量点的间距取为0．1mm左右，则对所讨论的实例而言，处理结果对原曲线的最大偏离为0．552μm，这样的误差对数控加工影响很小，而且整个处理过程所花费的时间不足1分钟，因此，该方法能满足数控加工的要求。     

Research on graphite powders used for HTR-PM fuel elements

Different batches of natural graphite powders and electrographite powders were characterized by impurity, degree of graphitization, particle size distribution, specific surface area, and shape characteristics. The graphite balls consist of proper mix-ratio of natural graphite, electrographite and phenolic resin were manufactured and characterized by thermal conductivity, anisotropy of thermal expansion, crush strength, and drop strength. Results show that some types of graphite powders possess very high purity, degree of graphitization, and sound size distribution and apparent density, which can serve for matrix graphite of HTR-PM. The graphite balls manufactured with reasonable mix-ratio of graphite powders and process method show very good properties. It is indicated that the properties of graphite balls can meet the design criterion of HTR-PM. We can provide a powerful candidate material for the future manufacture of HTR-PM fuel elements.     

基于分区电价的跨区电力调度双层优化模型

为充分利用跨区调度资源,提出一种基于分区电价的跨区电力调度双层优化模型。采用等效发电成本曲线对区域内部的煤电机组出力进行建模,采用一种基于整数规划的机会约束方法对风电和光伏出力进行建模。建立与分级调度模式相适应的双层优化模型,作为上级调度机构的上层模型以区域间送受电量为决策变量,以区域间送受电量价值最大化为目标,下层模型实现区域内部的经济调度。根据卡罗需-库恩-塔克(KKT)条件将双层模型转化为单层模型进行求解。算例结果验证了所提模型的有效性。所提模型在送电区域和受电区域之间维持一定的电价差异,通过传输较少的电量缓解受电区域的电力供需矛盾。     

考虑电池储能老化和需求侧响应的交直流混合配电网动态重构方法

现有的电池储能模型一方面认为电池的充放电功率和效率为固定不变的,另一方面有关电池储能的充放电过程对循环老化的影响缺少考虑,这与电池单元本体的非线性等效电路模型相违背。因此,考虑电池储能的循环老化成本、需求侧响应,提出了交直流混合配电网动态重构方法。通过对实际电池储能的充放电功率的运行区域进行采样,在凸包络的采样点集合中将非理想状态下的电池储能模型重构为线性模型。在此基础上,分别建立了基于累积吞吐电量和放电深度的循环老化成本模型,构建了综合成本最小化的交直流混合配电网动态重构模型。并采用混合整数二阶锥规划方法求解。在改进的33节点算例上仿真验证了所提基于放电深度的循环老化成本模型的经济性,分析了交直流混合配电网重构方法经济性的影响因素。     

用．NET开发导温系数测试装置的测控与仿真软件

采用瞬态热流法测定导温系数的方法具有装置结构简单、测试时间短和误差小等优点。但由于需要在线采集数据,因此必须开发专门的软件。经过分析对比,采用．NET技术开发本系统软件具有较好的优越性。该软件基于控件与类库的设计,实现了实时数据通信、数据采集、数据存储、图形显示、数据处理、实验仿真、数据输出等功能。系统的运行结果表明,该系统稳定性高、误差小、操作方便,有一定的应用价值。