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Carbon spheres with size of 50–300 nm were synthesized via a solvent-thermal reaction with calcium carbide and chloroform
as reactants in a sealed autoclave. The morphologies and microstructures of carbon spheres before and after high temperature
treatment (HTT) were characterized by X-ray diffractometry (XRD), scanning electronic microscopy (SEM), energy diffraction
spectroscopy (EDS), and transmission electron microscopy (TEM). The formation mechanism of carbon spheres was discussed. The
results indicate that the carbon spheres convert to hollow polyhedron through HTT. Carbon spheres are composed of entangled
and curve graphitic layers with short range order similar to cotton structure, and carbon polyhedron with dimension of 50–250
nm and shell thickness of 15–30 nm. The change of solid spheres to hollow polyhedron with branches gives a new evidence for
formation mechanism of hollow carbon spheres. 相似文献
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利用浸渍炉内残留或废弃的呋喃树脂,采用温压成形技术制备高电阻率炭材料。研究了粘结剂质量分数对材料性能(密度、电阻率、石墨化度)的影响,用扫描电镜观察了材料断口的微观形貌。结果表明,采用30%的酚醛树脂做粘结剂时,材料的综合性能最优,其平均密度为1.47g.cm-3,电阻率为224μΩ.m;制品中加入粘结剂时,石墨化度明显增加,为37.5%;试样断口扫描电镜照片表明粘结剂的质量分数为30%时,材料致密,孔隙细小且分布均匀,没有明显裂纹。 相似文献
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粉末冶金技术在中国的应用获得快速发展。系统介绍了粉末冶金摩擦材料在飞机刹车、坦克制动、离合器片、风电制动器主轴、高速列车制动闸片等领域的国内外应用现状,并对粉末冶金摩擦材料的原材料提出了具体要求,以期对粉末冶金技术的进一步发展提供参考。 相似文献
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摩擦过程中的温度场和热应力分布状况是摩擦学研究领域的一个重要课题.基于炭/炭复合材料制动盘湿式制动试验,将制动过程中的摩擦生热等效为瞬时移动面热源,按传动学理论计算制动盘与冷却润滑油的对流传热系数,建立三维循环对称有限元模型,运用有限元软件ANSYS分析制动盘的温度分布,给出典型时刻的温度场分布云图及温度升高引起的热应力场.利用有限元分析刹车制动过程的温度场,可为摩擦材料的研制及制动盘的设计提供有效的参考. 相似文献
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C/C-SiC composites with SiC island distribution were prepared via a new processing route. The fabrication process mainly included
silicon infiltration by ultrasonic vibration, chemical vapor deposition (CVD), siliconizing, liquid phase impregnation and
carbonization. The wear and friction properties were tested by an MM-1000 wet friction machine. The results show that SiC
phases are mainly distributed between carbon fibers and pyrocarbons as well as among the pryocarbons. The dynamic friction
coefficient of the composites decreases gradually from 0.126 to 0.088 with the increase of the surface pressure from 0.5 to
2.5 MPa at the same rotary speed. Furthermore, under the constant surface pressure, the dynamic friction coefficient increases
from 0.114 to 0.126 with the increase of the rotary speed from 1 500 to 2 500 r/min. However, the coefficient decreases to
0.104 when the rotary speed exceeds 4 500 r/min. During the friction process, the friction coefficient of C/C-SiC composite
is between 0.088 and 0.126, and the wear value is zero after 300 times brake testing.
Foundation item: Project(2006CB600901) supported by the Major State Basic Research and Development Program of China; Project(0991015) supported
by Guangxi Science Found, China; Project(200808MS083) supported by Guangxi Education Department Found 相似文献
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