A Multi-Stage Secure IoT Authentication Protocol

The Internet of Things (IoT) is a network of heterogeneous and smart devices that can make decisions without human intervention. It can connect millions of devices across the universe. Their ability to collect information, perform analysis, and even come to meaningful conclusions without human capital intervention matters. Such circumstances require stringent security measures and, in particular, the extent of authentication. Systems applied in the IoT paradigm point out high-interest levels since enormous damage will occur if a malicious, wrongly authenticated device finds its way into the IoT system. This research provides a clear and updated view of the trends in the IoT authentication area. Among the issues covered include a series of authentication protocols that have remained research gaps in various studies. This study applies a comparative evaluation of authentication protocols, including their strengths and weaknesses. Thus, it forms the foundation in the IoT authentication field of study. In that direction, a multi authentication architecture that involves secured means is proposed for protocol authentication. Informal analysis can affect the security of the protocols. Burrows-Abadi-Needham (BAN) logic provides proof of the attainment of mutual authentication. NS3 simulator tool is used to compare the performance of the proposed protocol to verify the formal security offered by the BAN logic.     

Anomalous high-frequency oscillations in a field emission tube and their significance in pulsed field emission

Relaxation oscillations occur when a capacitor is inserted in series with a field emission tube, a DC high-voltage power supply, and a ballast resistor. The waveform of these oscillations is highly reproducible with a dominant frequency of 200 MHz and a decay time of 20 ns. The peak current as high as 320 mA has been observed although the tungsten emitter is only rated for 10 microA. We have shown that these oscillations are due to a displacement current, charging of the anode-tip capacitance, and are not of a field emission origin. We conclude that the effects of displacement current should be considered in measurements of field emission with microsecond pulses, where high-current densities can be observed.     

Microencapsulation of Oils: A Comprehensive Review of Benefits,Techniques, and Applications

Microencapsulation is a process of building a functional barrier between the core and wall material to avoid chemical and physical reactions and to maintain the biological, functional, and physicochemical properties of core materials. Microencapsulation of marine, vegetable, and essential oils has been conducted and commercialized by employing different methods including emulsification, spray‐drying, coaxial electrospray system, freeze‐drying, coacervation, in situ polymerization, melt‐extrusion, supercritical fluid technology, and fluidized‐bed‐coating. Spray‐drying and coacervation are the most commonly used techniques for the microencapsulation of oils. The choice of an appropriate microencapsulation technique and wall material depends upon the end use of the product and the processing conditions involved. Microencapsulation has the ability to enhance the oxidative stability, thermostability, shelf‐life, and biological activity of oils. In addition, it can also be helpful in controlling the volatility and release properties of essential oils. Microencapsulated marine, vegetable, and essential oils have found broad applications in various fields. This review describes the recognized benefits and functional properties of various oils, microencapsulation techniques, and application of encapsulated oils in various food, pharmaceutical, and even textile products. Moreover, this review may provide information to researchers working in the field of food, pharmacy, agronomy, engineering, and nutrition who are interested in microencapsulation of oils.     

One Step Synthesis of NiO Nanoparticles via Solid-State Thermal Decomposition at Low-Temperature of Novel Aqua(2,9-dimethyl-1,10-phenanthroline)NiCl2 Complex

[NiCl₂(C₁₄H₁₂N₂)(H₂O)] complex has been synthesized from nickel chloride hexahydrate (NiCl₂·6H₂O) and 2,9-dimethyl-1,10-phenanthroline (dmphen) as N,N-bidentate ligand. The synthesized complex was characterized by elemental analysis, infrared (IR) spectroscopy, ultraviolet-visible (UV-vis) spectroscopy and differential thermal/thermogravimetric analysis (TG/DTA). The complex was further confirmed by single crystal X-ray diffraction (XRD) as triclinic with space group P-1. The desired complex, subjected to thermal decomposition at low temperature of 400 ºC in an open atmosphere, revealed a novel and facile synthesis of pure NiO nanoparticles with uniform spherical particle; the structure of the NiO nanoparticles product was elucidated on the basis of Fourier transform infrared (FT-IR), UV-vis spectroscopy, TG/DTA, XRD, scanning electron microscopy (SEM), energy-dispersive X-ray spectrometry (EDXS) and transmission electron microscopy (TEM).     

A fast method for the determination of the efficiency coefficient of bare CR-39 detector

A fast and simple method for the determination of the efficiency coefficient (η) of bare CR-39 detector is presented and discussed. The efficiency coefficient of bare CR-39 detector is then calculated by different ways and the obtained values are found to be comparable to each other. The average value of η of bare CR-39 is found to be 0.20 ± 0.01 tracks cm⁻² day⁻¹ per Bq m⁻³.     

A compact CMOS DC-DC buck converter based on a novel complement value leaping PWM technique

A very compact ultra-low power DC-DC buck converter is presented. The proposed buck converter employs a novel complement value leaping pulse-width modulation (PWM) technique to realize the desired DC mean-value for various loads. Incorporating just two counters with a simple digital controller to load the repeatedly complemented value of the 4bit up/down counter as the initial value of the least significant bits of the 5bit up counter, a PWM pulse is created to manage the charge/recharge period. The realized PWM signal maintains the same desired output voltage mean value for any load resistance between 80 and 140 Ω. The switching frequency is 160 kHz, and the overall power consumption is 26.9 nW, while the efficiency is 93.4% for current range of 1.7 to 3 mA. The performance of the proposed converter is validated by Cadence post-layout simulations utilizing TSMC180nm CMOS technology for 1-V supply voltage providing the output voltage mean value of 0.24 V.     

Nitrogen-doped graphene-supported zinc sulfide nanorods as efficient Pt-free for visible-light photocatalytic hydrogen production

Nitrogen-doped graphene-ZnS composite (NG-ZnS) was synthesized by thermal treatment of graphene-ZnS composite (G-ZnS) in NH₃ medium. In the second step, the as-synthesized samples were deposited on indium tin oxide glass (ITO) by electrophoretic deposition for photocatalytic hydrogen evolution reaction. The as-prepared NG-ZnS-modified ITO electrode displayed excellent photocatalytic activity, rapid transient photocurrent response, superior stability and high recyclability compared to the pure ZnS and G-ZnS-modified ITO electrode due to the synergy between the photocatalytic activity of ZnS nanorods and the large surface area and high conductivity of N-graphene.