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Sintering and grain growth of nano-crystalline undoped ZnO has been studied in detail over a wide range of temperature and holding time. Below 800 °C, sintering of over 70% theoretical density is not observed, irrespective of particle size. At 900 °C for 6 h, the nano-crystalline sample sinters to 99% of theoretical density whereas the density for as received sample is 93% of theoretical density. However, at 1300 °C or higher, the densification is found to be much faster and after a few hours becomes independent of holding time. Grain growth studies reveal a similar feature of attaining saturation over holding time. The average saturated grain size is found to be ∼1.5 and ∼2.2 μm at 800 and 900 °C, respectively, while at 1300 °C or higher, it is in between 12 and 13 μm. 相似文献
3.
Animesh Chakrabarti Man Mohan Sharma 《Journal of the American Oil Chemists' Society》1992,69(12):1251-1253
Anhydrous esterification of myristic acid with propylene was carried out in the temperature range of 110–145°C and pressure
from 190–195 psig in the presence of Amberlyst-15 (cation exchange resin) and Filtrol-24 (acid-treated clay) as catalysts.
The product ester, isopropyl myristate finds use in cosmetic and topical medicinal preparations where good absorption through
the skin is desired. Filtrol-24 is the catalyst of choice, and the recommended operating temperature is 130°C with a pressure
of 190 psig. 相似文献
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Semi1 and semi2 interpenetrating polymer networks (IPNs) of PVC and in situ formed PMMA have been synthesized using diallyl phthalate and ethylene glycol dimethacrylate as the crosslinkers of PVC and PMMA, respectively. These two types of IPNs have been compared w.r.t their physical, mechanical, and thermal properties and an endeavor has been made to find a correlation of these properties with the morphology generated in these systems. The semi1 IPNs displayed a decrease in their mechanical parameters and the physical properties as well, while in contrast, the semi2 IPNs exhibited a marginal increase in the corresponding values after an initial drop upto about 15% of crosslinked PMMA incorporation when compared to the crosslinked PVC in the case of semi1 IPN and linear PVC in the case of semi2 IPN. The various samples of semi1 and semi2 IPNs showed a two‐stage degradation typical of PVC, while confirming the increased stability with the samples having higher percentages of PMMA. The influence of crosslinking of the major matrix in semi1 IPN was almost counterbalanced by the influence of crosslinking in the dispersed PMMA phase in the case of semi2 IPN. The softening characteristics as detected by the extent of penetration of the probe, as has been detected by thermomechanical analysis, are in conformity with their mechanicals. © 2005 Wiley Periodicals, Inc. J Appl Polym Sci 97: 1725–1735, 2005 相似文献
7.
Coarse frequency offset estimate and tracking of residual frequency offset are two crucial stages for frequency synchronization in OFDM based WLAN systems. An improved frequency offset estimation scheme is proposed for tracking residual offset. The estimation scheme is dependent on the position of an OFDM symbol in a frame. 相似文献
8.
Bhattacharya D Saha S Basu S Chakravarty S Chakravarty A Banerjee D Chakrabarti A 《Proteomics. Clinical applications》2010,4(5):480-488
Purpose: In (hemoglobin, Hb) HbEβ‐thalassemia, HbE (β‐26 Glu→Lys) interacts with β‐thalassemia to produce clinical manifestation of varying severity. This is the first proteomic effort to study changes in protein levels of erythrocytes isolated from HbEβ‐thalassemic patients compared to normal. Experimental design: We have used 2‐DE and MALDI‐MS/MS‐based techniques to investigate the differential proteome profiling of membrane and Hb‐depleted fraction of cytosolic proteins of erythrocytes isolated from the peripheral blood samples of HbEβ‐thalassemia patients and normal volunteers. Results: Our study showed that redox regulators such as peroxiredoxin 2, Cu‐Zn superoxide dismutase and thioredoxin and chaperones such as α‐hemoglobin stabilizing protein and HSP‐70 were upregulated in HbEβ‐thalassemia. We have also observed larger amounts of membrane associated globin chains and indications of disruption of spectrin‐based junctional complex in the membrane skeleton of HbEβ‐thalassemic erythrocytes upon detection of low molecular weight fragments of β‐spectrin and decrease in β‐actin and dematin content. Conclusion and clinical relevance: We have observed interesting changes in the proteomic levels of redox regulators and chaperons in the thalassemic hemolysates and have observed strong correlation or association of the extent of such proteomic changes with HbE levels. This could be important in understanding the role of HbE in disease progression and pathophysiology. 相似文献
9.
Chakrabarti A Naik V Dechoudhury S Bandyopadhyay A Mondal M Pandey HK Roy TK Sanyal D Bhowmick D 《The Review of scientific instruments》2007,78(4):043303
A 33.7 MHz heavy-ion radio frequency quadrupole (RFQ) linear accelerator has been designed, built, and tested. It is a four-rod-type RFQ designed for acceleration of 1.38 keVu, qA> or =116 ions to about 29 keVu. Transmission efficiencies of about 85% and 80% have been measured for the unanalyzed and analyzed beams, respectively, of oxygen ((16)O(2+), (16)O(3+), (16)O(4+)), nitrogen ((14)N(3+), (14)N(4+)), and argon ((40)Ar(4+)). The system design and measurements along with results of beam acceleration test will be presented. 相似文献
10.
Dimensionality Reduction for Fast Similarity Search in Large Time Series Databases 总被引:36,自引:3,他引:33
Eamonn Keogh Kaushik Chakrabarti Michael Pazzani Sharad Mehrotra 《Knowledge and Information Systems》2001,3(3):263-286
The problem of similarity search in large time series databases has attracted much attention recently. It is a non-trivial
problem because of the inherent high dimensionality of the data. The most promising solutions involve first performing dimensionality
reduction on the data, and then indexing the reduced data with a spatial access method. Three major dimensionality reduction
techniques have been proposed: Singular Value Decomposition (SVD), the Discrete Fourier transform (DFT), and more recently
the Discrete Wavelet Transform (DWT). In this work we introduce a new dimensionality reduction technique which we call Piecewise
Aggregate Approximation (PAA). We theoretically and empirically compare it to the other techniques and demonstrate its superiority.
In addition to being competitive with or faster than the other methods, our approach has numerous other advantages. It is
simple to understand and to implement, it allows more flexible distance measures, including weighted Euclidean queries, and
the index can be built in linear time.
Received 16 May 2000 / Revised 18 December 2000 / Accepted in revised form 2 January 2001 相似文献