基于晶体塑性学的铁素体不锈钢表面起皱有限元分析

针对成形过程中铁素体不锈钢薄带存在的表面起皱问题,基于晶体塑性学建立了有限元仿真模型并通过一系列实验进行了相关验证分析,模拟计算了不同晶粒大小的铁素体不锈钢薄带在20%延伸率下的起皱高度。经研究发现,铁素体不锈钢表面的起皱现象主要源于晶粒的滚动与滑移变形。在成形过程中,大尺度晶粒所形成的具有特定取向(如{001}<110>)的晶粒簇易于产生较大的塑性变形,与周边晶粒产生的塑性变形形成差异,导致严重的表面起皱现象,结果表明铁素体不锈钢在成形过程中的起皱高度与材料的平均晶粒尺寸基本呈正相关。研究结果可为表面质量良好的铁素体不锈钢薄带轧制工艺制定提供理论参考。     

Influence of thermo hydrogen treatment on hot deformation behavior of Ti600 alloy

Hot compressive deformation of Ti600 alloy after thermo hydrogen treatment (THT) was carried out within hydrogen content range of 0-0.5%, temperature range of 760-920 ℃ and strain rate range of 0.01-10 s-1. The flow stress of Ti600 alloy after THT was obtained under hot deformation condition, and the influence of hydrogen on work-hardening rate (S*), strain energy density (U*), and deformation activation energy (Q) was analysed. The results show that the flow stress of Ti600 alloy decreases remarkably with the increase of hydrogen when the hydrogen content is less than 0.3%. Both S* and U* decrease with the increase of hydrogen when the hydrogen content is less than 0.3%, and when the hydrogen content is more than 0.3%, S* and U* increase with hydrogen addition. The value of Q decreases with the increase of strain at the same hydrogen content. The addition of small quantity of hydrogen leads to an increase of Q at small strain values, and when the strain reaches 0.6, the value of Q decreases gradually with the increase of hydrogen. When the hydrogen content is within the range of 0.1%-0.3%, the flow stress of Ti600 alloy is decreased when being deformed at the temperature range of 760-920 ℃.     

焊接热输入和焊后热处理对搅拌摩擦焊2024-T3铝合金焊核区硬度的影响

在不同焊接热输入条件下对2024-T3铝合金进行搅拌摩擦焊接,并利用透射电镜、差热分析和维氏硬度测试对焊核区的组织和硬度进行分析检测。研究表明,焊核区的硬度受到焊接热输入的影响。在高焊接热输入条件下,焊接速度的提升有利于提升焊核区硬度。而在低焊接热输入条件下,焊核区硬度随着旋转速度的增加而增加。焊后热处理导致组织过时效,焊核区硬度降低。相比于其他参数下获得的焊核区,旋转速度为500 r/min,焊接速度为100 mm/min条件下获得的焊核区拥有较高的抗过时效性能,硬度下降仅为3.8%,而其他焊核区的硬度下降超过10%。焊核区硬度主要受到强化相形态的影响。     

玻璃基LSCO/PZT/LSCO电容器的制备和铁电性能

采用磁控溅射法制备La0.5Sr0.5CoO3(LSCO)薄膜、sol-gel法制备Pb(Zr0.4Ti0.6)O3(PZT)薄膜,在玻璃和Ti-Al/Si衬底上构架了LSCO/PZT/LSCO电容器,研究了衬底对LSCO/PZT/LSCO电容器结构和铁电性能的影响。研究发现:虽然生长在两种衬底上的PZT薄膜均为钙钛矿结构多晶薄膜,但是,生长在玻璃衬底上的LSCO/PZT/LSCO电容器具有更好的铁电性能。玻璃基LSCO/PZT/LSCO电容器的剩余极化强度(Pr)为28×10–6C/cm2,矫顽电压(Vc)为0.96V;而硅基LSCO/PZT/LSCO电容器的Pr为25×10–6C/cm2,Vc为1.05V。     

Research of the influence of thermohydrogen treatment on microstructural evolution and hardness of Ti600 alloy

研究了热氢处理对Ti600合金组织演变和硬度的影响. 结果表明: 热氢处理后,在Ti600合金中析出具有四方结构的硅化物粒子S3(0.357% H)和六方结构的硅化物粒子S1(0.497% H). 在氢的质量分数为0.357%和0.497%的试样中均发现有面心立方(fcc)的氢化物, 并且随着氢含量的提高氢化物表现出明显细化的趋势.Ti600合金的硬度随着氢含量的提高而提高, 其主要原因是氢化物、硅化物粒子以及晶格缺陷的存在.     

激光微区等离子体光谱测定铁电薄膜材料组份的元素比率

本文在常压空气环境下,以单脉冲YAG激光作为激发源,通过辅助电极激发,获得了铁电薄膜样品上不同位置处的等离子体发射光谱.利用最小二乘法对铁电薄膜样品中Co、Sr和La的光谱数据进行处理,得到了元素谱线辐射强度比和原子个数比之间的线性因子Kij,并利用线性因子Kij计算了铁电薄膜上不同位置处的元素比率.结果表明,激光微区等离子体光谱法可以用于测定亚微米薄膜材料中的元素比率.     

热氢处理对Ti600合金的组织演变和硬度的影响

研究了热氢处理对Ti600合金组织演变和硬度的影响.结果表明:热氢处理后,在Ti600合金中析出具有四方结构的硅化物粒子S3(0.357%H)和六方结构的硅化物粒子S1(0.497%H).在氢的质量分数为0.357%和0.497%的试样中均发现有面心立方(fcc)的氢化物,并且随着氢含量的提高氢化物表现出明显细化的趋势.Ti600合金的硬度随着氢含量的提高而提高,其主要原因是氢化物、硅化物粒子以及晶格缺陷的存在.     

Influence of hydrogenation on microstructures and microhardness of Ti6A14V alloy

The microstructures of Ti6A14V alloy after hydrogenation were investigated by optical microscopy（OM）, X-ray diffraction（XRD） and transmission electron microscopy（TEM）. The influence of hydrogenation on the hardness of α and β phases was analysed by microhardness testing. The influence of hydrogenation on alloying elements diffusion was studied by electron probe microanalysis（EPMA）. The microstructural observation reveals that hydride δ （FCC structure） as well as large number of dislocations precipitate in the specimens with 0.278% and 0.514% hydrogen, and a lot of twins are found in the specimen with 0.514% hydrogen, simultaneously. The result of microhardness testing shows that the hardness of a and β phases increases synchronously with the increase of hydrogen and the hardness increment of β is larger than that of a. According to analysis of EPMA, the diffusion ability of alloy elements Al and V increases after hydrogenation. It is considered that hydrogen solution strengthening and V element diffusion are the main factors causing the hardness of a phase increase with the increase of hydrogen, and the formation of δ hydrides, lattice defects, hydrogen solution strengthening and Al element diffusion jointly cause the hardness of β phase increase with the increasing hydrogen.     

新复方降压胶囊对高血压病疗效观察1

目的 观察新复方降压胶囊对高血压病的疗效。方法 经2 wk洗脱期后的高血压病人随机分为3 组:卡托普利组:卡托普利12.5 ~ 25 mg, 每日3 次;尼群地平组:尼群地平5 ~ 10 mg, 每日3 次;新复方降压胶囊组:1 ~ 2 粒, 每日3 次;疗程8 wk。观察治疗前后24 h动态血压、生化指标和不良反应。结果 新复方降压胶囊组24 h动态血压明显优于其它两组, 而生化指标和不良反应无明显差异。结论 新复方降压胶囊具有较好的降压作用。     

保温时间对SPS烧结硬质合金和高强度钢粘结的影响

使用放电等离子烧结技术(SPS)制备硬质合金和高强度钢的复合材料,研究了在烧结过程中保温时间(5,10,15和20 min)对复合材料的显微组织和形成相以及力学性能的影响.研究表明,随着保温时间的增加,烧结质量越来越好,粘结界面光滑连续,没有出现明显的裂纹和分层;XRD检测结果显示:当保温时间为5 min时,复合材料的...