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采用溶胶凝胶法,以蔗糖和正硅酸乙酯(TEOS)为原料,草酸为TEOS水解的催化剂,制备均相碳化硅前驱体,在氩气氛和高温条件下(1 350~1 600 ℃)将碳化硅先驱体进行碳热还原,制备出高比表面积的SiC。考察了水/TEOS物质的量的比、碳/硅物质的量的比及镍盐等因素对碳化硅比表面积的影响。结果表明,当nwater/nTEOS=7.5,nC/nSi=4时,适宜的镍催化剂(nNi/nTEOS=0.005),凝胶形成的时间最短,镍盐的加入可使碳热还原温度降低200 ℃。 相似文献
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The level structure in neutron-deficient nucleus 91Ru was investigated via the 58Ni(36Ar,2 plnγ)Ru reaction at a beam energy of 111 MeV.Charged particles,neutrons,and y-rays were emitted in this reaction and detected by the DIAMANT CsI ball,Neutron Wall,and the EXOGAM Ge clover array,respectively.In addition to the previously reported levels in 91Ru,new low-to-medium spin states were observed.Angular correlation and linear polarization measurements were performed to unambiguously determine spins and parities of the excited states in 91 Ru.The low-spin states of 91 Ru exhibit a scheme of multi-quasiparticle excitations,which is very similar to that of the neighboring N=47 isotone.These excitations have been interpreted in terms of the shell model.The calculations performed in the configuration space(p3/2,f5/2,p1/2,g9/2)reproduce the experimental excitation energies reasonably well,supporting the interpretation of the newly assigned positive-parity states in terms of the three quasiparticle configurationsπ(g9/2)^-2v(g9/2^-1 and v(g9/2)^-3. 相似文献
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High-spin states in nucleus 139Pm have been studied using the reaction 116Cd(27Al,4n)139Pm.Two dipole cascades have been found.Spin and parity assignments were based on the Directional Correlation of Oriented Nuclei(DCO) ratios and systematic behavior in neighboring odd-proton nuclei.The level structures of 139Pm are compared with those of the N =78 isotone 141Eu in which two dipole bands have been confirmed as magnetic rotational bands.The close similarity between them suggests that the dipole bands in 139... 相似文献
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265Bh(Z=107)同位素的首次观测 总被引:1,自引:0,他引:1
在兰州的重离子加速器上用26Mg离子束轰击243Am靶,产生了新同位素265Bh.通过观测新同位素265Bh和它的已知子核261Db和257Lr之间的α衰变的关联,实现了对新核素的鉴别.实验中使用了一套新建立的具有数个探测器对的转轮收集探测系统.将该系统用于特殊的母–子核搜索模式,从而大大减少了本底.共测得了8个265Bh的α衰变关联事件;同时4个已知核264Bh的衰变关联事件也被鉴别出来.实验测得265Bh的α衰变能量为(9.24±0.05)MeV,半衰期为0.94+0.70–0.31s. 相似文献
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应用E-GOS(E-Gamma Over Spin)曲线方法研究了A≈110质量区奇A核结构随角动量增加的演化, 发现随着角动量的增加原子核的激发特性从振动逐渐演化为转动。 The E-GOS(E-Gamma Over Spin)curves were used to investigate the structure evolution in the odd A nuclei around A≈110 as a function of spin. The result shows that there is a clear transition from vibration to rotation while increasing spin. 相似文献
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利用在束γ谱学方法,通过反应144Sm(28Si,1p3n)169Re研究了169Re的激发态能级结构.实验进行了X-γ符合、γ-γ符合、DCO系数和带内B(M1)/B(E2)比率测量.基于这些测量,建立了组态为π9/2-[514]的强耦合带和组态为π1/2-[541]的退耦合带.通过比较169Re的转动带与邻近奇质子核已知转动带的结构和B(M1)/B(E2)比率,指定了169Re转动带的组态.实验观测到π9/2-[514]和π1/2-[541]转动带的中子AB带交叉的转动频率分别为0.23和0.27MeV.着重讨论了169Re转动带的中子AB带交叉频率、转动角动量顺排和旋称劈列等,并讨论了奇ARe核转动带结构的系统性 相似文献