Microscopical studies of water/flour systems

Summary Wheat flour particles sprinkled on a water surface form strands which are visible in the light microscope. These strands form aggregates by means of mechanical forces which show viscoelastic behaviour. Amino acid analysis of both the protein strands and the aggregates formed shows that they consist of gluten protein. The formation of the protein strands occurs at the air/water interface and results from the action of a protein film which spreads around the flour particles.

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Mikroskopische Untersuchungen von Mehl/Wasser-Systemen

Zusammenfassung Weizenmehlpartikel, die auf Wasser gestreut werden, bilden lichtmikroskopisch sichtbare Stränge aus. Durch mechanische Beanspruchung lassen sich these Stränge zu Aggregaten zusammenfassen, die visco-elastisches Verhalten zeigen. Die Aminosäureanalyse sowohl der Proteinstrange wie auch der daraus gebildeten Aggregate zeigt, daß es sich dabei um Kleberprotein handelt. Die Proteinfäden entstehen an der Wasser-Luft-Grenzflache als Folge eines spreitenden Proteinfilms, der sich um die Mehlpartikel herum ausbreitet.

     

High-performance liquid chromatography of reduced glutenin: amino acid composition of fractions and components

Reduced glutenin is separated by gel permeation high-performance liquid chromatography into three major and five minor fractions, which significantly differ in their amino acid compositions. By reversed-phase high performance liquid chromatography, about 20 glutenin components are obtained. These can be classified into three groups according to their amino acid compositions: a hydrophilic group with relatively high values of Glx and Phe, a more hydrophobic group with a high content of Gly, and a strongly hydrophobic group with higher values of Val and Leu. Groups 1, 2 and 3 contain middle-, high- and low-molecular-weight (MMW-, HMW-, LMW-) subunits respectively.     

Sicherheitstechnische Maßnahmen bei der thermischen Abluftreinigung

Safety measures in thermal waste air purification units . Safety problems may arise in thermal waste air purification units from the occasional explosive nature of the exhaust gases, which may cause a flashback into the production plant. This must be avoided by the installation of safety devices that arrest a flashback. The number of such safety devices is determined by the probability of formation of explosive waste air, according to the zone classification of the explosion-protection guide. The principal explosion arrestor devices installed between combustion chamber and production plant are liquid submersion systems, detonation barriers, and dynamic flashback-free inlets into the combustion chamber, all of which must be operated under instrumental surveillance. This report presents a state-of-the-art summary of all suitable procedures and safety devices permitting safe design of systems for thermal air cleaning problems encountered in practice.     

Model reactions on roast aroma formation

Summary From model roastings of mixtures containing serine, threonine and sucrose about 350 volatile compounds were separated and identified by GC/MS. Among them there were more than 100 monocyclic furans, 13 furanones and 8 bicyclic furans, the mass spectra and retention indices of which are recorded. The most important mass spectrometric fragmentation pathways are described. Spectra obtained from roasting coffee under identical conditions are compared with the spectra from model roastings.

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Modell-Reaktionen zur Röstaroma-BildungII. Die massenspektrometrische Identifizierung von Furanen und Furanonen aus der Reaktion von Serin und Threonin mit Saccharose unter den Bedingungen der Kaffeeröstung

Zusammenfassung Aus Modellröstungen von Gemischen aus Serin, Threonin und Saccharose unter den Bedingungen der Kaffeeröstung wurden etwa 350 flüchtige Verbindungen mittels GC/MS getrennt und identifiziert. Unter ihnen befanden sich über 100 monocyclische Furane und 13 Furanone sowie 8 bicyclische Furane, deren Massenspektren und Retentions-indices angegeben werden. Die wichtigsten massenspektrometrischen Fragmentierungswege werden beschrieben. -Die aus einer gleich behandelten Röstung von Rohkaffee erhaltenen Spektren werden mit denen der Modellröstungen verglichen.

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Dissertation Gloria Bochmann, TU Berlin 1984     

Isothermic growth of one spherulite around circular obstacles in a polypropylene foil

Growth of one spherulite within a thin foil of polypropylene around one circular obstacle or around combinations of circular obstacles is investigated. For each obstacle there exists a region of shadow, seen from the nucleus of the spherulite, which influences the growth of the spherulite. Within any region of shadow the growth fronts are evolvents of the obstacle's boundary, because the spherulite grows isotropically. When two growth fronts belonging to one spherulite meet each other inside the shadow, an intrinsic grain boundary is formed for each obstacle. Additionally, growth of one spherulite around a rectangular obstacle and a spherical obstacle is investigated.     

Zu einem Phänomen der Lochkorrosionsbegrenzung bei hochlegierten Sonderedelstählen und NiCrMo-Legierungen in Chloridlösungen

On a phenomenon of the limitation of pitting corrosion at high alloyed special stainless steels and NiCrMo-alloys in chloride solutions Testing the pitting corrosion resistance of high alloyed special stainless steels and NiCrMo-alloys in chloride solutions there was observed a limitation of the pitting corrosion range toward more positive potentials. Above this limitation, the so-called pitting corrosion limitation potential, the pit initiation by all means is prevented, but the growth of pits which had been initiated before in the pitting corrosion range not necessarily comes to a stop. Therefore current density-potential curves which are obtained by downward polarization after an initial potential jump into the transpassive region and chronopotentiostatic tests are more suitable to investigate this phenomenon than cyclic polarization measurements and potentiostatic alteration tests. There is indicated a dependence of this phenomenon on temperature. The phenomenon of a limitation of the pitting corrosion range toward more positive potentials has been found until now at alloy 926, alloy 31, alloy 28, alloy 59 and alloy C-276.     

方便显示器升级的复合型VGA编码器／解码器

较老式的计算机系统通过4根75Ω同轴电缆把RGB(三原色)视频和复合同步信号输送到150英尺外的RGB彩色监视器。如需升级,用于替换的VGA视频卡可直接驱动VGA监视器的内部端接部件带来的75Ω负载。但是,VGA标准使用单独的水平和垂直正向同步信号。向原始电缆添加一根额外的同轴电缆来承载单独的同步信号,这是一种困难并且成本很高的建议。一个明显的解决方案就是把单独的同步信号组合到一种复合格式中。图1中的组合器电路很简单,成本很低,并且可用随时供货的备件来迅速组装。     

Proteine des Bienenhonigs

Zusammenfassung Die Isolierung der Saccharase (E.C. 3.2.1.20) aus den Proteinkonzentraten von Raps-, Tannen- und Zuckerfütterungshonig wird beschrieben. Die Abtrennung von anderen Enzymen, insbesondere von saurer Phosphatase gelingt durch hydrophobe Wechselwirkungschromatographie, von inerten Proteinen durch Gelfiltration. Im Zusammenhang damit wird das Verhalten des Enzyms bei der Chromatographie an Anionenaustauschern, an Hydroxylapatit und an immobilisiertem Weizenkeimlectin untersucht. Dabei ergab sich am Lectin-Gel eine Trennung in zwei multiple Formen.Die Saccharase aus allen drei Honigsorten verhielt sich einheitlich, woraus zu schließen ist, daß sie ausschließlich von der Biene stammt. Ihre Molekül masse wurde gelchromatographisch zu 57000 ermittelt.

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The proteins of honeyVIII. Honey sucrase, isolation, chromatographic behaviour and properties

Summary The isolation of the honey sucrase (E.C. 3.2.1.20) from rape- and fir-honey as well as from honey obtained after sugar feeding is described. The separation from other honey enzymes especially from acid phosphatase succeded by reversed phase chromatography. Separation of other, non-active proteins was accomplished by gel permeation chromatography. The behaviour of the honey sucrase upon chromatography on anion exchangers, on hydroxylapatite and wheat germ lectin was investigated. No differences were found between the sucrases of the three honeys.The molecular weight was determined at 57 000. By affinity chromatography with wheat germ lectin the enzyme could be separated into two multiple forms.