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1.
A novel series of temperature‐sensitive poly[(N‐isopropylacrylamide)‐co‐(ethyl methacrylate)] (p(NIPAM‐co‐EMA)) microgels was prepared by the surfactant‐free radical polymerization of N‐isopropylacrylamide (NIPAM) with ethyl methacrylate (EMA). The shape, size dispersity and volume‐phase transition behavior of the microgels were investigated by transmission electron microscopy (TEM), ultraviolet–visible (UV–Vis) spectroscopy, dynamic light scattering (DLS) and differential scanning calorimetry (DSC). The transmission electron micrographs and DLS results showed that microgels with narrow distributions were prepared. It was shown from UV–Vis, DLS and DSC measurements that the volume‐phase transition temperature (VPTT) of the p(NIPAM‐co‐EMA) microgels decreased with increasing incorporation of EMA, but the temperature‐sensitivity was impaired when more EMA was incorporated, causing the volume‐phase transition of the microgels to become more continuous. It is noteworthy that incorporation of moderate amounts of EMA could not only lower the VPTT but also enhance the temperature‐sensitivity of the microgels. The reason for this phenomenon could be attributed to changes in the complicated interactions between the various molecules. Copyright © 2004 Society of Chemical Industry 相似文献
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本文研究了浸胶工艺对Nomex蜂窝性能的影响,分析探讨了提高Nomex蜂窝性能及外观质量的途径。研究结果表明:采取新的浸胶工艺制作的Nomex蜂窝,各项性能全面达到法国宇航材料标准。 相似文献
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Jihao Wang Yufen Han Zhiyang Xu Xiaozhen Yang Seeram Ramakrishna Yong Liu 《大分子材料与工程》2021,306(4):2000724
Polymer systems have typical multiscale characteristics, both in space and time. The mesoscopic properties of polymers are difficult to describe through traditional experimental approaches. Dissipative particle dynamics (DPD) is a simulation method used for solving mesoscale problems of complex fluids and soft matter. The mesoscopic properties of polymer systems, such as conformation, dynamics, and transport properties, have been studied extensively using DPD. This paper briefly summarizes the application of DPD to research involving microchannel flow, electrospinning, free-radical polymerization, polymer self-assembly processes, polymer electrolyte fuel cells, and biomedical materials. The main features and possible development avenues of DPD are described as well. 相似文献
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Xiaozhen Yang 《Polymer》2004,45(12):4241-4248
The conformational distribution change of amorphous poly(lactic acid) (PLA) induced by deformation has been studied using Raman spectroscopy. Spectroscopic features associated with the rotational isomeric states (ttt, ttg′, tg′t, tg′g′) have been established experimentally and supported by normal coordinate analysis. Deformation induced a significant increase in the most favorable tg′t conformation. Based on the relative intensities of Raman-active skeletal modes, a quantitative method has been developed that can be used to elucidate structural changes in a variety of deformed polymer samples. For biaxially oriented PLA films, the overall tg′t conformation increased from the 76% in undeformed sample to a value as high as 92%. The change in conformational distribution in the amorphous phase follows a different trend (76-88%) as compared to the increase in sample crystallinity (0-43%). A large change in amorphous chain conformation occurred at relatively low draw ratios. In contrast, the large change in the degree of crystallinity occurred at higher draw ratios. 相似文献
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文章针对无线传感器网络技术在环境监测中的应用,研究并开发了基于无线传感器网络的电力信息机房监测系统,系统采用CC2530芯片及温度、湿度、烟雾、漏水传感器、UPS监控设备等,基于ZigBee网络,实现了机房中重要环境参数的采集,并通过服务器端的B/S系统将数据分析与存储,便于用户在远程查看,实现了机房的远程监测。 相似文献
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CRH380BL高速动车组转向架技术含量高,结构复杂,需要高效率、高质量的检修与维护手段。文章综合应用虚拟现实、多媒体和仿真技术,设计开发了动车组转向架检修虚拟仿真支持系统。它提供一个可视化的多媒体信息平台,可支持新的培训模式,使培训人员在虚拟环境中快速掌握检修技能,以交互方式浏览转向架各组成部件的三维模型,了解转向架的技术信息、结构特点、模块配置、各级修程信息及产品装配过程。该文介绍了转向架结构特点,详细描述了系统的结构、功能以及关键技术。 相似文献
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Support crushing and water inrush when mining under an unconsolidated confined aquifer in the Qidong Coal Mine was prevented by roof pre-blasting. The mechanism and applicable conditions for this method have been studied. The results show that when an overburden structure that may cause support crushing and a water inrush accident exists the weakening of the primary key stratum, which thereby reduces its weighting step, roof pre-blasting is both feasible and effective. If the position of the primary key stratum can be moved upward to exceed 10 times the mining height the possibility of support crushing and water inrush disaster caused by key stratum compound breakage will be lowered. The overburden structure of the number 7121 working face was considered during the design of a technical proposal involving roof pre-blasting. After comprehensively analyzing the applicability of roof pre-blasting the resulting design prevented support crushing and water inrush disasters from happening at the number 7121 working face and laid a solid foundation for mining safely. 相似文献
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根据大量国内外网站可用性相关理论,从内容、外观和导航等3方面,对B2C网站可用性给予消费者购买意愿的影响进行了分析,通过建立B2C网站可用性对消费者购买意愿影响的模型,结合对调研数据进行统计分析,旨在找出对消费者购买意愿影响较大的B2C网站可用性因素,不但为网站设计人员设计出高可用性B2C网站提供参考,从而吸引更多消费者. 相似文献