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1.
Gopalu Karunakaran Govindhan Maduraiveeran Evgeny Kolesnikov Suresh Kannan Balasingam Lysov Dmitry Viktorovich Igor Ilinyh Mikhail V. Gorshenkov Manickam Sasidharan Denis Kuznetsov Manab Kundu 《JOM Journal of the Minerals, Metals and Materials Society》2018,70(8):1416-1422
We have synthesized NiCo2O4 nanoparticles (NCO NPs) using an ascorbic acid-assisted co-precipitation method for the first time. When NCO NPs are used as an anode material for lithium-ion batteries, the cell exhibits superior lithium storage properties, such as high capacity (700 mA h g?1 after 300 cycles at 200 mA g?1), excellent rate capabilities (applied current density range 100–1200 mA g?1), and impressive cycling stability (at 1200 mA g?1 up to 650 cycles). The enhanced electrochemical properties of NCO NPs are due to the nanometer dimensions which not only offers a smooth charge-transport pathway and short diffusion paths of the lithium ions but also adequate spaces for volume expansion during Li storage. Hence, this eco-friendly synthesis approach will provide a new strategy for the synthesis of various nanostructured metal oxide compounds, for energy conversion and storage systems applications. 相似文献
2.
Dhineshbabu Nattanmai Raman Karunakaran Gopalu Suriyaprabha Rangaraj Manivasakan Palanisamy Rajendran Venkatachalam 《纳微快报(英文)》2014,6(1):46-54
Nano-Micro Letters - Magnesia (MgO) nanoparticles were produced from magnesite ore (MgCO3) using ball mill. The crystalline size, morphology and specific SSA were characterized by X-ray diffraction... 相似文献
3.
P. Karunakaran C. Jegadheesan P. Dhanapal P. Sengottuvel 《Russian Journal of Non-Ferrous Metals》2014,55(3):247-253
X-ray diffraction, thermogravimetric analysis, scanning electron microscopy and energy-dispersive spectroscopy studies were performed with molding sand and sugar industry fly ash to evaluate and compare their physical properties. We noted that several physical properties of sugar industry fly ash and molding sand were similar. We then tested the permeability, green compression strength and dry compression strength of various compositions of sugar industry fly ash and bentonite to explore their potential as an alternative to molding sand, thereby reducing the dependency on the latter, as well as to suggest an effective way for disposal of fly ash from sugar industry. We also found that quality aluminium castings could be produced using fly ash, which effectively replaced 24% of molding sand in the foundry, thereby reducing the cost of production and increasing the surface finish of castings. 相似文献
4.
Emergence of Gold‐Mesoporous Silica Hybrid Nanotheranostics: Dox‐Encoded,Folate Targeted Chemotherapy with Modulation of SERS Fingerprinting for Apoptosis Toward Tumor Eradication 下载免费PDF全文
Adukkadan N. Ramya Manu M. Joseph Santhi Maniganda Varsha Karunakaran Sreelekha T. T. Kaustabh Kumar Maiti 《Small (Weinheim an der Bergstrasse, Germany)》2017,13(31)
Strategically fabricated theranostic nanocarrier delivery system is an unmet need in personalized medicine. Herein, this study reports a versatile folate receptor (FR) targeted nanoenvelope delivery system (TNEDS) fabricated with gold core silica shell followed by chitosan–folic acid conjugate surface functionalization by for precise loading of doxorubicin (Dox), resembled as Au@SiO2‐Dox‐CS‐FA. TNEDS possesses up to 90% Dox loading efficiency and internalized through endocytosis pathway leading to pH and redox‐sensitive release kinetics. The superior FR‐targeted cytotoxicity is evaluated by the nanocarrier in comparison with US Food and Drug Administration (FDA)‐approved liposomal Dox conjugate, Lipodox. Moreover, TNEDS exhibits theranostic features through caspase‐mediated apoptosis and envisages high surface plasmon resonance enabling the nanoconstruct as a promising surface enhanced Raman scattering (SERS) nanotag. Minuscule changes in the biochemical components inside cells exerted by the TNEDS along with the Dox release are evaluated explicitly in a time‐dependent fashion using bimodal SERS/fluorescence nanoprobe. Finally, TNEDS displays superior antitumor response in FR‐positive ascites as well as solid tumor syngraft mouse models. Therefore, this futuristic TNEDS is expected to be a potential alternative as a clinically relevant theranostic nanomedicine to effectively combat neoplasia. 相似文献
5.
A benzimidazole-based receptor 2-(4-fluorophenyl)-1-phenyl-1H-benzo[d]imidazole [FPPBI] has been designed, synthesized and characterized by 1H NMR, 13C NMR, mass and single crystal XRD. Absorption, emission, lifetime and cyclic voltammetry have been made to deduce the interaction between FPPBI and ZnO nanocrystals. FPPBI act as a new host for ZnO nanocrystals that enhance its luminescence. The apparent binding constant has been obtained. Adsorption of the FPPBI on ZnO nanocrystals lowers the HOMO energy level of the FPPBI. The strong adsorption of the FPPBI on the surface of ZnO nanocrystals is likely due to the chemical affinity of the nitrogen atom of the FPPBI to the zinc ion on the surface of nanocrystals. 相似文献
6.
7.
Balakumaresan Ragupathy Manivannan Karunakaran 《International journal of imaging systems and technology》2021,31(1):379-390
This article develops a methodology for meningioma brain tumor detection process using fuzzy logic based enhancement and co‐active adaptive neuro fuzzy inference system and U‐Net convolutional neural network classification methods. The proposed meningioma tumor detection process consists of the following stages as, enhancement, feature extraction, and classifications. The enhancement of the source brain image is done using fuzzy logic and then dual tree‐complex wavelet transform is applied to this enhanced image at different levels of scale. The features are computed from the decomposed sub band images and these features are further classified using CANFIS classification method which identifies the meningioma brain image from nonmeningioma brain image. The performance of the proposed meningioma brain tumor detection and segmentation system is analyzed in terms of sensitivity, specificity, segmentation accuracy, and Dice coefficient index with detection rate. 相似文献
8.
K. P. Karunakaran Saurabh Agrawal Pankaj D. Vengurlekar Onkar S. Sahasrabudhe Vishal Pushpa Ronald H. Ely 《IIE Transactions》2005,37(4):291-302
Rapid Prototyping (RP) is a technology based on a “divide-and-conquer” strategy that enables automatic physical realization of a design without any special tooling. However, existing RP processes suffer from staircase defects since they are all based on 2.5-axis kinematics. To minimize the error due to staircase defects parts are normally built from very thin layers typically with thickness values of 0.010 to 0.300 mm. Therefore, hundreds of layers are required to produce a typical object making RP a slow and costly process. To overcome these limitations, a new RP process called Segmented Object Manufacturing (SOM) is proposed in this paper. SOM makes use of three-axis kinematics in conjunction with a novel slicing method. Slicing in SOM is based on certain visibility-based considerations and is independent of the part accuracy. Since only a few thick layers are used in the SOM technique, a part can be produced faster and cheaper with an accuracy comparable to that of CNC machining. 相似文献
9.
Govindan Suresh Kumar Gopalu Karunakaran Easwaradas Kreedapathy Girija Evgeny Kolesnikov Nguyen Van Minh Mikhail V. Gorshenkov Denis Kuznetsov 《Ceramics International》2018,44(10):11257-11264
We report the rapid microwave-assisted hydrothermal synthesis of mesoporous hydroxyapatite (HAp) nanocrystals with controlled size, morphology, and surface area using various organic modifiers as regulators. The products were analyzed for their crystalline nature, phase purity, morphology, particle size and pore size distribution. Results indicated that ascorbic acid, cetyltrimethyl ammonium bromide (CTAB) and polyvinylpyrrolidone (PVP) play an important role to obtain needle like, rod like and fiber like mesoporous HAp nanocrystals with different specific surface area by controlling growth habit of HAp along c-axis. In addition, the prepared samples were B-type carbonated HAp similar to bone minerals. Therefore, the present approach can be a promising way to obtain precursor for making tissue engineering scaffolds, drug/protein delivery carriers and bone fillers with tunable characteristics. 相似文献
10.
Here we present a high-resolution chromosomal spectral map derived from synchrotron-based soft X-ray spectromicroscopy applied to quinoa species. The label-free characterization of quinoa metaphase chromosomes shows that it consists of organized substructures of DNA-protein complex. The analysis of spectra of chromosomes using the scanning transmission X-ray microscope (STXM) and its superposition of the pattern with the atomic force microscopy (AFM) and scanning electron microscopy (SEM) images proves that it is possible to precisely locate the gene loci and the DNA packaging inside the chromosomes. STXM has been successfully used to distinguish and quantify the DNA and protein components inside the quinoa chromosomes by visualizing the interphase at up to 30-nm spatial resolution. Our study represents the successful attempt of non-intrusive interrogation and integrating imaging techniques of chromosomes using synchrotron STXM and AFM techniques. The methodology developed for 3-D imaging of chromosomes with chemical specificity and temporal resolution will allow the nanoscale imaging tools to emerge from scientific research and development into broad practical applications such as gene loci tools and biomarker libraries. 相似文献