Condensation polymerization of pyrogallol and benzaldehyde

Novolac-type polycondensation of benzaldehyde (B) and pyrogallol (P) has been carried out at 60°C, 75°C and 90°C and at B/P mole ratios of 1.5 and 3.0 using phosphoric acid as catalyst. The reaction follows a 2nd order rate law. By using GC consumption data of benzaldehyde and pyrogallol, kinetic parameters such as the overall rate constants, activation energies (E_a) and logA values are investigated. The activation energies for 1.5 and 3.0 B/P mole ratios are found as 62.3 kJ mol^?1 and 56.4 kJ mol^?1, respectively. The molecular weights of the resins determined by measuring intrinsic viscosities (25°C, THF) are in the range of 0.03 to 0.07 dL g^?1 at various temperatures and B/P mole ratios.     

Convolutional solutions of partial difference equations

A significant part of the theory of one-dimensional linear shift-invariant systems is based on the concept of weighting function (or impulse response): the output is the convolution of the weighting function with the input. This paper introduces the concept of linear translation-invariant systems and uses this notion in studying impulse response, z-transforms, and transfer functions for multidimensional systems.     

基于移动Agent技术的QoS保障机制

介绍了移动Agent的基本特性。移动Agent可在异构的网络各个节点间自由地移动,它能感知网络的状态,监控系统并与其他Agent进行交互。IETF的IS模型采用了RSVP(ResourcereSerVationProtocol)协议对系统资源进行预留,从而达到一定程度上保障所需QoS的目的。QoS保障机制将移动agent技术与RSVP协议结合起来,通过资源预留和agent动态移动的实现可以达到更好地改善QoS的目的。     

The hydration phase and pore structure formation in the blends of sulfoaluminate-belite cement with Portland cement

Sulfoaluminate-belite (SAB) cements are an attractive class of low-energy cements from the viewpoint of saving energy and releasing less CO₂ into the atmosphere during their production. Their hydraulic activity, however, does not match that of the ordinary Portland cement (PC) and needs improvement before they can be used on their own. However, SAB cements when blended with PC have the potential to be used effectively in traditional applications as shown by this study. Mortars made with blends of SAB cements and PC, and a cement-to-sand ratio of 1:3 by weight and a water-to-cement ratio of 0.5, indicate a superior protection against corrosion of steel to those made with blends of PC and blast-furnace slag (BFSPC). The prepared mortars were stored at 20 °C for 90 days under either a 60% relative humidity (RH)-dry air, or 100% RH-wet air conditions. With further improvement in the SAB cement quality through better understanding of their characteristics, a genuine competition between SAB/PC and BFSPC can be expected in practice.     

Testability-analysis driven test-generation of analogue cores

A new definition of the testability transfer factor for circuit components that provides better sensitivity with respect to parametric deviations is presented. New equations for the testability measures in a mixed-signal core are given. Testability analysis is used for test-pattern generation and for consideration of inserting wrapper cells. The simulation results show the effectiveness of the approach.     

Graft copolymerization of different mixtures of acrylic monomers on amylopectin. Swelling behavior

Hydroxylic and nonhydroxylic acrylates—methyl acrylate (MA), ethyl acrylate (EA), butylacrylate (BA), hydroxypropyl methacrylate (HPMA), ethylenglycol dimethacrylate (EGDMA), and mixtures of HPMA–MA, HPMA–EA, HPMA–BA in a 50/50 feed composition—were grafted onto amylopectin with different amounts of crosslinking agent, EGDMA. Percent of total conversion, percent crude grafting, and influence of pH in water content were studied. In this sense it was only at pH 10 when a real variation in the water content could be seen. It was also proved that the highest values were obtained when one of the comonomers was EGDMA with a 34 mol% of the initial feed composition. © 1994 John Wiley & Sons, Inc.     

Sphere Lower Bound for Rotated Lattice Constellations in Fading Channels

We study the error probability performance of rotated lattice constellations in frequency-flat Nakagami-m block-fading channels. In particular, we use the sphere lower bound on the underlying infinite lattice as a performance benchmark. We show that the sphere lower bound has full diversity. We observe that optimally rotated lattices with largest known minimum product distance perform very close to the lower bound, while the ensemble of random rotations is shown to lack diversity and perform far from it.     

Influence of deposition parameters on hole mobility in polymorphous silicon

Time-of-flight transient photoconductivity measurements reveal a monotonic increase with the deposition pressure in the hole mobility in polymorphous silicon for samples deposited under hydrogen dilution. With helium dilution, a maximum mobility that matches the highest value from H-dilution samples is measured at the intermediate pressure of 1.4 Torr. The deposition rate of those samples is twice the rate for the H-dilution ones. For the samples with the best hole mobilities, the valence-band tail is comparable to the one of standard hydrogenated amorphous silicon.     

Phase method for monitoring the permittivity of different media

A nondestructive method was developed for rapidly monitoring the permittivities of solid, liquid, and gaseous materials, based on measuring the phase difference of signals passing along two transmission lines and comparing the parameters of the “standard” and “investigated” media. The design of a volume-integral microwave transducer is considered together with its operating principle and its range of application. Translated from Izmeritel'naya Tekhnika, No. 4, pp. 53–55, April, 1996.