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Deprotection of cyclic acetals and oxidative desilylation of trimethylsilyl ethers into the corresponding carbonyl compounds with -picolinium chlorochromate (-PCC) under nonaqueous conditions at room temperature is described. Oxidation of aldehydes to carboxylic acids was not observed in any case. 相似文献
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Sarafraz M. M. Tian Zhe Tlili I. Kazi Sabeena Goodarzi Marjan 《Journal of Thermal Analysis and Calorimetry》2020,139(4):2435-2445
Journal of Thermal Analysis and Calorimetry - In the present study, a set of experiments were accomplished to appraise the thermal performance and heat transfer of n-pentane-acetone and... 相似文献
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A. Mobinikhaledi N. Foroughifar F. Goodarzi 《Phosphorus, sulfur, and silicon and the related elements》2013,188(3):507-512
Thiazolo 3 a–c and oxothialo 5 a–b pyrimidine compounds were synthesized by a simple one-pot condensation reaction of the pyrimidine derivative i 1a and 1,2-dibromoethane i 2 or 2-bromopropanoic acid 4 . In a similar way the thiazepinopyrimidine compounds 7 (a–b) were synthesized by reaction of 1b and 1,4-dichlorobutane 6 in dimethylformamide under reflux condition. The yields of products following recrystallization were of the order of 60–80%. 相似文献
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Giwa S. O. Sharifpur M. Goodarzi M. Alsulami H. Meyer J. P. 《Journal of Thermal Analysis and Calorimetry》2021,143(6):4149-4167
Journal of Thermal Analysis and Calorimetry - Recently, the suspension of hybrid nanoparticles in conventional fluids has been investigated as a technique for improving the thermophysical... 相似文献
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Waqas Hassan Farooq Umar Khan Shan Ali Alshehri Hashim M. Goodarzi Marjan 《Journal of Thermal Analysis and Calorimetry》2021,145(4):2033-2044
Journal of Thermal Analysis and Calorimetry - The increasing need of the modern era of technology for better ways to increase the heat transfer performance of thermal systems has made nanoliquids... 相似文献
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The MP2 method in combination with the aug-cc-pVXZ (X = D and T) basis set has been carried out to examine the complexes between O3 and isostructure species of CO2, CS2 and SCO. Two, two and four minima have been located on the potential energy surfaces of O3–CO2, O3–CS2 and O3–SCO complexes, respectively. The results reveal that the stabilization of complexes should be in the order O3–CS2 > O3–SCO > O3–CO2. 相似文献
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Water activity measurements by isopiestic method have been carried out on the aqueous solutions of alanine + tri-potassium citrate (K3Cit) over a range of temperatures at atmospheric pressure. From these measurements, values of the vapor pressure of solutions were determined. The effect of temperature on the vapor–liquid equilibrium of alanine + K3Cit + H2O systems has been studied. The experimental water activities have been correlated successfully with the segment-based local composition Wilson and NRTL models. The agreement between the correlations and the experimental data is good. 相似文献
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Ultrashort laser pulse interaction with the surface of silicon wafer in air and water environments is investigated. Ti:sapphire laser with 40 femtosecond laser pulses at 790 nm and 10 Hz repetition rate was used. The ablation threshold of the silicon surface in the air was determined to be about 0.28 J cm?2. The surface morphology was studied by using scanning electron microscope images. The size of the regular ripples formed in the air environment is a little smaller than the laser wavelength. Due to the nonlinear interaction and self-focusing before the target, the ripples size reduced to nearly a half of the laser wavelength in the water. Moreover, the spikes’ structure formation and their diameter in air and water were studied. Two regimes for spike formation in water are proposed that can explain the anomalous decrease of the spikes’ diameter in higher fluence. During the interaction of single linearly polarized femtosecond laser pulse with the surface, an irregular ripple formation that called circular ripple is observed. This structure which is a result of radiation pressure implies to the surface by the end of the pulse. A new physical model for interpretation of the circular ripples formation based on the ponderomotive force of an ultrashort pulse laser is proposed which can predict the size of the circular ripples. The calculated results are in accordance with our experimental findings. 相似文献