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以碳电极为基体的聚氯乙烯膜铋离子选择电极的研制与应用 总被引:1,自引:1,他引:1
铋是得乐、胃必治等胃药的主要成分,其含量测定方法有用中国药典法、吸光光度法、等离子体发射光谱法等。本文利用铋离子可与碘离子形成稳定的配合物,且该配合物又能与胺类物质生成沉淀,报道了以六碘合铋配离子与曲马多缔合物为电活性物的涂碳式聚氯乙烯膜铋离子选择电极,并用此电极以标准曲线法对枸橼酸铋钾胶囊进行了测定,此法简便,结果与药典法相符。 相似文献
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盐酸莱克多巴胺是人工合成的β2-肾上腺素兴奋剂,它可加快畜禽生长速度,降低酮体脂肪含量,提高瘦肉率,俗称"瘦肉精"。由于盐酸莱克多巴胺存在组织残留问题,对人体健康产生不利影响,我国相关部门已明文禁止莱克多巴胺用于动物养殖。目前国内有关动物组织中莱克多巴胺的检测方法主要 相似文献
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用固体石蜡山梨酸碳糊电极电位法测定食品中山梨酸 总被引:1,自引:0,他引:1
制备了一种以山梨酸根与乙基紫形成的缔合物为电活性物的固体石蜡山梨酸碳糊电极,并对其性能做了测定。结果显示该电极对山梨酸有较好的能斯特响应。山梨酸的线性范围为2.2×10-5~1.0×10-1mol.L-1,检出限为1.6×10-5mol.L-1。该电极用于食品中山梨酸根的测定,结果与分光光度法结果相符。 相似文献
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炭材料具有比表面积大、孔径可调、取材广泛等优点,以其为载体负载金属活性组分制备硅氢加成催化剂极具发展前景.我们详细总结了近20年不同炭材料如活性炭、石墨与石墨烯、碳纳米管、富勒烯、卡宾等在硅氢加成反应中负载金属催化剂的制备方法、催化性能以及可能的催化机理,并对有望应用到该反应的新型炭材料载体进行了对比与展望.认为未来硅氢加成炭负载型催化剂的研究可聚焦于(1)探寻新型双金属活性组分以进一步提高催化活性;(2)研发更具优势的金属配体,明晰配体与载体、配体与金属之间的相互作用关系以提高催化选择性与稳定性;(3)结合科学可靠的催化机理研究,以期研发出更符合可持续发展要求的炭负载型硅氢加成金属催化剂,可使硅氢加成反应基本实现原子经济性. 相似文献
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We develop a new calibration method in lab by measuring the absolute spectral irradiance responsivity of Sun photometer sun channel. The absolute power responsivity of Sun photometer is obtained when a white laser double monochromator system serve as a source, and a standard transfer detector calibrated against cryogenic absolute radiometer is assembled to measure the absolute power of laser beam. The effective area of aperture is measured through laser raster scanning method, and the relative spectral irradiance responsivity of the corresponding channel is obtained by using tungsten-halogen lamps double monoehromator system. On the basis of the above results, the top of the atmosphere responsive constants V0 (500, 675, and 870 nm) are obtained by integration with extraterrestrial solar spectral irradiance data. Comparing the calibration results with that of CIMEL, France in November 2011, the relative differences are 4.38%, 2.23%, and 2.45%, respectively. The calibration uncertainty reaches to 2.048×10^-2, which shows a remarkable consistency with the Langley plot method. Further, our scheme can overcome the limits of space and atmospheric conditions which are only available at a high-altitude calibration site in particular date. The advantages lie in not only shortening the experiment period but also being of high precision. This new scheme definitely plays an important role in supporting the current and future sun photometry calibration activities which are significant to earth observation. 相似文献