排序方式: 共有89条查询结果,搜索用时 250 毫秒
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在表面活性剂辅助的水热条件下合成出尺寸均一的Gd2O3∶Eu3+纳米棒, 对其结构和荧光性质进行了表征, 并对其生长机理进行了初步讨论. XRD结果表明, 水热前驱体样品为六方晶相的Gd(OH)3, 经过灼烧之后样品为立方相的Gd2O3. TEM照片表明, 所得样品为直径60 nm、长度约600 nm的纳米棒. 荧光光谱表明, 在波长为254 nm 的紫外光激发下, Gd2O3∶Eu3+纳米棒产生了不同于前驱体的特征红光发射, 对应于Eu3+ 的5D0-7F2跃迁, 表明Gd2O3是红色发光材料的良好基质. 相似文献
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研究了退化弱(k1,k2)拟正则映射的正则性.利用Holder不等式、Sobolev空间的空间分析方法,以及内插定理等工具,给出了退化弱(k1,k2)拟正则映射事实上为退化(k1,k2)拟正则映射的一个充分条件,其结果对非退化情形也成立. 相似文献
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采用水热法合成了Fe3O4@SiO2@YF3:Eu3+磁-光双功能复合粒子,对其结构和性能进行了表征.XRD分析表明:Fe3O4表面包覆上了结晶良好的正交晶系的YF3.TEM照片表明:复合粒子为球形,构成核的Fe3O4颗粒的尺寸在200~350 nm之间,Fe3O4@SiO2@YF3:Eu3+核壳结构复合粒子的尺寸约为230~380 nm,与包覆前的Fe3O4相比较,包覆后,颗粒尺寸增大,并且YF3:Eu3+是以棒状结构连接在Fe3O4球型颗粒的表面.磁性和荧光光谱分析表明:该复合颗粒同时具有良好的发光性和磁性,使其在生物医学领域具有潜在的应用. 相似文献
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The spherical Y2O3∶Eu3+ luminescent particles with size of 0.5~3 μm and smooth surface were synthesized by hydrothermal method. The resulted Y2O3∶Eu3+ precursors and the calcined particles were characterized by differential thermal analysis (DTA) and thermogravimetric (TG) analysis, X-ray diffraction (XRD), Fourier-transform IR spectroscopy (FTIR), scanning electron microscopy (SEM) and photoluminescence spectra (PL). FTIR, TG-DTA, XRD measurements show that the precursors are crystal with hydroxyl and carbonate group, and the pure cubic yttria is obtained after annealing above 700 ℃. The SEM images indicate that the Y2O3∶Eu3+ particles are in spherical shape and with smooth surface. PL analysis shows that the particles present characteristic red emission of Eu3+. 相似文献
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球形Gd2O3∶Eu纳米发光材料的制备 总被引:1,自引:0,他引:1
Spherical nanometer Gd2O3∶Eu luminescent materials were prepared by homogeneous precipitation method, and the properties were studied also. TG, FTIR and XRD analysis showed that the precursor was carbonate, the cubic Gd2O3was obtained after calcination. TEM photographs indicated that the samples were spherical and well dispersed with nanometer and submicrometer size of 200~300 nm which is the nanoparticles’ aggregate. The mechanics of agglomerating growth is also discussed. ED photograph showed that the particle was crystalline. The PL analysis exhibited that CTB band of nanometer Gd2O3∶Eu was of 17 nm red shift to bulk materials, and the emission peak was broadened due to the surface and interface effect of nanocrystals. 相似文献
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近红外光谱检测技术在害虫检测中的应用 总被引:3,自引:0,他引:3
近红外光谱是20 世纪80 年代以来发展最快、最引人注目的光谱分析技术。以其快速、无损伤、操作简单、稳定性好、效率高等特点,在仓储害虫检测、种子害虫侵染检测和林草害虫危害检测中的应用已成为一个活跃的研究领域。而近红外光谱技术在我国害虫检测中的研究和应用则较少,处于刚刚起步阶段。因此,文章介绍了利用近红外光谱技术检测的基本原理, 综述了国内外利用近红外光谱技术检测农林业害虫的应用情况,并对近红外检测技术在害虫检测上的应用进行了展望,以期推动近红外光谱技术在我国害虫检测科技和生产中的应用。 相似文献
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