机械合金化过程中Fe70B30粉末晶粒尺寸和微观应变的研究

用Ｘ射线和电镜研究了Ｆｅ＿（７０）Ｂ＿（３０）粉末经不同时间高能球磨后晶粒尺寸和微观应力的变化。在机械合金化过程中，粉末的Ｘ射线衍射谱的宽度随球磨时间的增加逐渐加宽，这是晶粒细化和内部微观应力共同作用的结果。Ｘ射线衍射结果表明：随着机械合金化的进行，粉末的晶粒尺寸逐渐减小，球磨初期晶粒尺寸下降较快，经１５ｈ球磨，晶粒尺寸为２５ｎｍ，机械合金化进行到一定时间后晶粒尺寸下降缓慢，８０ｈ球磨后晶粒尺寸可达５ｎｍ。在机械合金化过程中球磨所造成的微观应变不大，球磨初期粉末的内应力随球磨时间增加而增加，当粉末粒子尺寸很小时，随球磨的进行粉末中的微观应变显著下降。     

Electrical/electronic effects of titanium and iron impurities in EFG and FZ solar cell silicon: SPV/EBIC analysis

In this paper results on surface photovoltage (SPV) and electron beam induced conductivity (EBIC) studies of edge-defined film-fed growth (EFG) and floating zone (FZ) silicon solar cell materials (both p-type) are presented. A systematic comparison based on minority carrier diffusion length and carrier recombination is made between: (i) samples contaminated with Ti and/or Fe, (ii) samples gettered by phosphorous diffusion, and (iii) as-received samples. Deep level transient spectroscopy (DLTS) measurements, together with the iron-boron (FeB) pairing kinetics [1] have successfully been used to detect the presence of Fe in the samples. Even though this process is effective in revealing Fe impurities in p-type FZ silicon it is evidently not suitable for Fe identification in p-type EFG silicon. Ti, like Fe, is found to be a prominent lifetime-limiting metallic impurity in both EFG and FZ silicon. Phosphorous diffusion is proven to be an effective external gettering technique for fast-diffusing impurities such as Fe, but not for Ti.     

胜利油区放射性同位素测井的粒径选择

根据胜利油区的地层渗透率、孔隙度，在２７个低渗透油田和４６个中、高渗透油田的放射性同位素测井中进行了粒径为１００～３００μｍ、３００～６００μｍ、６００～９００μｍ放射性同位素１３１Ｂａ微球粒径选择实验，确定了放射性同位素１３１Ｂａ微球的选择原则。当油藏渗透率Ｋ＜１００×１０－３μｍ２、孔隙度＜２０％时，放射性同位素粒径为１００～３００μｍ；当油藏渗透率Ｋ＞１００×１０－３μｍ２、孔隙度＞２０％时，放射性同位素粒径为３００～６００μｍ或６００～９００μｍ。在此基础上得到胜利油区选用同位素粒径明细表，对于指导施工，提高放射性测井资料的可靠性具有重要意义。     

On the applied stress dependence of the subgrain size

The present work studies the collection of experimental data from which Raj and Pharr (Mater. Sci. Eng., 81 (1986) 217) deduced a universal empirical dependence of the subgrain size on the applied stress. In accord with their result and some theoretical predictions the normalized subgrain size d_s/b was ssumed to be proportional to G/σ (G is the shear modulus, b the Burgers vector length, σ the applied stress). The evaluated factor of proportionality K₁, having the value within the interval from 0.76 to 180 in the inspected data sets, was discussed from the point of view of various factors which can influence the experimental data.     

鼓风引射式燃气燃烧器的计算

提出鼓风式射式燃气燃烧器的基本计算公式与计算结果，并进行结构尺寸与工况分析，确定各种因素对其的影响程度。     

高速钢高温形变诱发析出的研究

本文探讨了高速钢在高温形变过程中碳化物析出的行为及奥氏体组织状态对析出的影响。用透射电镜和扫描电镜分析了不同热处理状态奥氏体的组织结构,分析了高温形变过程中碳化物析出的部位,颗粒尺寸及形态。试验表明, 碳化物主要在奥氏体的缺陷处呈点状和点列状析出,大小为20mμ。处于回复状态的奥氏体缺陷诱发碳化物析出,析出碳化物钉札缺陷阻止再结晶进行。当再结晶驱动力较大时,由于动态再结晶充分发展,使缺陷大量消除,碳化物析出显著地减少。     

How Meta-Analysis Increases Statistical Power.

One of the most frequently cited reasons for conducting a meta-analysis is the increase in statistical power that it affords a reviewer. This article demonstrates that fixed-effects meta-analysis increases statistical power by reducing the standard error of the weighted average effect size (T?.) and, in so doing, shrinks the confidence interval around T?.. Small confidence intervals make it more likely for reviewers to detect nonzero population effects, thereby increasing statistical power. Smaller confidence intervals also represent increased precision of the estimated population effect size. Computational examples are provided for 3 effect-size indices: d (standardized mean difference), Pearson's r, and odds ratios. Random-effects meta-analyses also may show increased statistical power and a smaller standard error of the weighted average effect size. However, the authors demonstrate that increasing the number of studies in a random-effects meta-analysis does not always increase statistical power. (PsycINFO Database Record (c) 2010 APA, all rights reserved)     

Influence of Billet Size on Flow, Solidification and Solute Transport in Continuous Casting

ListofSymbol　　B———Buoyancy ,m·s- 2 ;　　c———Concentrationofsoluteelement ;　　Cμ———Turbulentconstant;　　D———Diffusivityofsoluteelement ,m2 ·s- 1 ;　　fl,fs———Liquidandsolidfraction ;　　fμ———Turbulentcoefficient ;　　h———Enthalpy ,J·kg- 1 ;　　k———Turbulentkineticenergy ,m2 ·s- 2 ;　　kp———Equilibriumpartitioncoefficient;　　Kp———Permeabilityofmushyzone ,m2 ;　　K0 ———Permeabilitycoefficient;　　p———Pressure ,Pa ;　　Pr———Prandtlnumber ;…     

套管钻井用套管外表面磨损后剩余强度分析

在分析讨论套管钻井管柱磨损形态的基础上,结合API5C5实物试验尺寸要求,通过有限元计算分析方法,对钻井套管完钻后含有外表面磨损缺陷的套管柱的极限剩余抗挤强度和极限剩余抗拉强度进行了研究,分别获得了均匀磨损和偏磨条件下,套管钻井套管柱外表面磨损缺陷的临界长度尺寸数值,以及不同破坏失效准则条件下的剩余抗挤强度和剩余抗拉强度的计算方程,为套管钻井中套管柱的设计、计算奠定了理论基础。     

Sorption of Acid Green 25 on chitosan: Influence of experimental parameters on uptake kinetics and sorption isotherms

Acid Green 25, which is a diazoic dye bearing two sulfonic groups, is efficiently sorbed on chitosan. The protonation of chitosan may explain the electrostatic attraction of this anionic dye and that its optimum pH is close to 3. Preliminary protonation of amine groups (obtained by contact with a sulfuric acid solution) reduced the variation of solution pH following sorbent addition but significantly reduced sorption performance: the maximum sorption capacity of raw chitosan, 525 mg dye/g (0.84 mmol dye/g), was halved by acidic preconditioning. The acidic conditioning also reduced the kinetic rate—the time necessary to reach equilibrium increased up to threefold depending on the experimental conditions. The size of sorbent particles influenced sorption kinetics and equilibrium because of resistance to intraparticle diffusion, but the sorption appeared to occur not only at the surface of the sorbent but also in the intraparticle network of the polymer. © 2003 Wiley Periodicals, Inc. J Appl Polym Sci 90: 1073–1080, 2003