镁合金表面喷铝防腐蚀层的微观组织分析

在AZ91D镁合金表面热喷铝，用以提高其表面的耐腐蚀性能。采用SEM，EPMA等方法对AZ91D表面喷铝扩散层的组织进行了仔细的观察与分析，发现在防腐蚀层上有大量的Mg17Al12相存在，且呈决状及非连续片状分布。经显微硬度测定，喷铝层硬度较镁合金基体高；腐蚀后这种相凸出于基体，比镁合金基体有较好的耐腐蚀性能。     

残留奥氏体对1500MPa级新型低碳Mn-Si-Cr系合金钢冲击韧度的影响

15 0 0MPa级无碳化物贝氏体 马氏体复相钢的第一类回火脆性开始温度高于 36 0℃。实验表明 ,这并非由于贝氏体 马氏体复相韧化 ,而是与无碳化物贝氏体中的膜状残留奥氏体有关。无碳化物贝氏体中机械稳定性较高的残留奥氏体可能是导致无碳化物贝氏体 马氏体复相钢第一类回火脆性开始温度升高的直接原因。     

Cold Gelation of β-lactoglobulin in the Presence of Iron

ABSTRACT: To protect and transport iron, we investigated the trapping properties of a network formed from β-lactoglobulin. We studied the influence of different parameters—pH, iron, and protein concentrations—on gel properties (optical and mechanical properties, WHC, and microstructure). For all conditions tested, the results show the formation of a cold gel in the presence of iron. The mechanical properties reveal that the elastic behavior and the strength of rupture increase with higher protein concentrations and decrease with higher iron concentrations. The water-holding capacity is high for low iron concentrations. The microstructure shows that, at low iron/protein ratios, a homogeneous filamentous network is obtained whereas, at high iron/protein ratios, more random aggregated particles are present.     

Recovery retardation in equal channel angular pressed Al–Zr alloy during friction stir welding

The effect of Zr on reduction of hardness and microstructure in an FS weld of equal channel angular-pressed Al alloy was investigated. Zr addition to Al suppressed dynamic recovery in the thermomechanically affected zone and enabled retention of the high hardness of the ECA-pressed material throughout the weld.     

Al-Cu-Fe系初生准晶相凝固过程的电子显微分析

采用包括金相（OM），粉末X射线衍射（XRD），扫描电子显微镜（SEM）观察和透射电子显微（TEM）分析等方法，研究了铸态Al592.Cu36.8Fe3.0Si1.0合金（700℃保温2．5h后水淬）的显微组织及相组成。发现铸锭中存在4种相：准晶I相，τ3相（或φ相），θ－Al2Cu相和η－AlCu相，凝固过程可描述为：初生晶是准晶Ⅰ相；在保温过程中发生包晶或共晶反应（L＋i→τ3(或φ）或L→τ3（或φ）＋i)形成的τ3相（或φ相），呈微畴结构；而剩余液体水淬形成θ－Al2Cu相和η－AlCu 相。     

Recent developments of high-performance NEOMAX magnets

For further improvement in achieving extremely high magnetic properties of Nd- Fe- B sintered magnets, extensive investigation has been done to densify the magnet up to the theoretical value, to increase the volume fraction of the Nd ₂Fe₁₄B matrix phase, and to achieve a high degree of alignment. By controlling chemical composition and the amount of constituent phases,improving particle size distribution, and adopting the isostatic pressing method to get better alignment of fine particles, we have succeeded in obtaining a high-performance magnet having residual flux density (B_r) of 1.495 T (14.95 kG), maximum energy product [(BH)_max] of 431 kj/m³ (54.2 MGOe), and intrinsic coercivity (iH_c) of 845 kA/m (10.62 kOe).     

施加复合电磁搅拌对A357合金微观组织的影响

在半固态加工技术中，电磁搅拌是最早应用于制备非枝晶浆料的方法之一，同时也是半固态触变压铸技术最早获得工业应用的重要技术基础之一。采用自行开发的电磁搅拌器，研究了多种不同电磁搅拌方式在不同工艺条件下，单独施加或复合施加对A357合金微观组织的影响。试验结果表明：单一施加旋转感应电磁搅拌时，浆料径向组织很不均匀；单一施加无芯感应电磁搅拌。当搅拌电流较小时，径向组织也不均匀，增大电流，浆料质量有明显改善；采用（旋转感应＋无芯感应）复合电磁场进行复合电磁搅拌时，可在电流较小时获得满意的浆料质量。     

Development of ultra light magnesium-lithium alloys

Magnesium-lithium alloys are among the lowest density metallic materials. Addition of lithium, with a relative density of 0·53, in magnesium reduces the density of the alloy significantly. Furthermore, addition of nearly 11 wt.% lithium converts hexagonal close packed structure of pure magnesium to a body centered cubic lattice, markedly improving formability of the alloy. The development of these alloys, however, had been hampered due to the high reactivity of lithium and magnesium in the molten state and also, due to poor creep resistance and instability of mechanical properties at room temperature. In an attempt to indigenize these ultra light alloys for possible applications in Indian satellite programme, detailed research work was initiated in DMRL. The difficulties associated with producing sound cast ingots have been overcome by controlling melting and casting parameters of these alloys. Extensive work has been done on structure-property correlation of alloys with varying lithium content and minor alloying additions. Based on these work, advanced magnesium-lithium alloys have been developed with improved tensile properties, room temperature stability and creep resistance. Wrought products (plates/sheets) of magnesium-lithium alloy have been supplied to ISAC, Bangalore and are being used in their INSAT-2 programme. This paper describes the systematic studies carried out in the laboratory to indigenize these ultra light alloys.     

Non-contact methods of measuring moisture concentration in external layers of building partitions II—Monitoring of the water vapour condensation on porous surfaces

This paper present the results of the investigation into a potential application of laser radiation for the detection of phase transition processes occurring on the surface layers of porous materials. An attempt was made to discuss in the approximation equations, the relationships between coefficients of the reflected light, the temperature and humidity of the surrounding environment. Laser light reflected from the porous surface carries information about the roughness of the structure. The presence of water microdrop on the surface of the porous material, as a result of condensation and thus a phase transition, leads to the phase displacement of individual rays, which is represented by different images. Therefore, a comprehensive analysis of the reflected light parameters allows a dynamic study of the phase transition phenomena without mechanical intervention.     

平面Z-型软磁铁氧体频率特性的研究

研究分析了Co2Z材料显微结构与磁性能的关系,在普通铁氧体工艺中引入预磁化处理方法,并适当控制二次再结晶现象,成功地研制出高性能的Co2Z型宽频材料,Z-型铁氧体材料的共振频率可达1.8GHz以上,截止频率在1GHz附近,起始磁导率在8-13之间,介电常数相对较低(ε'<30)。