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51.
Nanosized lead zirconate titanate (PZT) powder with Zr:Ti ratio in the morphotropic phase boundary region was synthesized by homogeneous precipitation of metal ions. The powder precipitated at 90°C and at pH 6.7 resulted single-phase perovskite lead zirconate titanate powder when calcined at 550°C and above for 4 hours in air. The solution pH and the precipitation temperature strongly affect the composition of the calcined powder. The results obtained by structural characterization of homogeneously precipitated powder were compared with that obtained from the conventional precipitation method using ammonia in terms of crystallization, homogeneity, and microstructure. The homogeneously precipitated powder showed smaller particle size, minimum agglomeration and uniform shape on calcination and annealing. Powdered samples that precipitated by homogeneous precipitation crystallized directly to perovskite PZT, without any intermediate pyrochlore phase formation. In contrast, the NH3 precipitated powder converted to perovskite PZT via metastable pyrochlore and it showed phase segregation upon annealing at higher temperatures. The reaction kinetics has been studied by X-ray diffraction, differential thermal analysis, and differential scanning calorimetry. 相似文献
52.
STUDY ON PHASE PERCEPTION IN SPEECH 总被引:4,自引:0,他引:4
Tong Ming Bian Zhengzhong Li Xiaohui Dai Qijun Chen Yanpu 《电子科学学刊(英文版)》2003,20(5):387-392
The perceptual effect of the phase information in speech has been studied by auditory subjective tests. On the condition that the phase spectrum in speech is changed while amplitude spectrum is unchanged, the tests show that: (1) If the envelop of the reconstructed speech signal is unchanged, there is indistinctive auditory perception between the original speech and the reconstructed speech; (2) The auditory perception effect of the reconstructed speech mainly lies on the amplitude of the derivative of the additive phase; (3) td is the maximum relative time shift between different frequency components of the reconstructed speech signal. The speech quality is excellent while td <10ms; good while 10ms< td <20ms; common while 20ms< td <35ms, and poor while td >35ms. 相似文献
53.
D. Mangelinck P. Gas T. Badche E. Taing F. Nemouchi C. Perrin-Pellegrino M. Vuaroqueaux S. Niel P. Fornara J. M. Mirabel L. Fares P. H. Albarede 《Microelectronic Engineering》2003,70(2-4):220-225
The formation of Ti silicides has been examined in flash memories with 0.25 μm linewidth by X-ray diffraction, scanning electron microscopy, and transmission electron microscopy. It has been observed that, after the first rapid thermal process and the selective metal etch, there is no silicide on the source and on a majority of drain contacts while C49-TiSi2 is found on the gate. A pre-amorphisation implant increases drastically the formation of C49-TiSi2 in the drain zone while modifications of annealing conditions have little impact. These results indicate that the formation of C49-TiSi2 is most likely controlled by nucleation and that this nucleation is sensitive to both the width and the length of the reaction zone. The formation of a Ti rich silicide may play an important role in this nucleation by decreasing the driving force for the formation of C49-TiSi2. Curiously enough, the formation of C49-TiSi2 appears thus as a major concern for the salicide process in flash memories. 相似文献
54.
A type of CO2 sensor based on oxygen concentration cell was designed as following: Cell I: Pt | Au, O2,CO2|Na2CO3(Au)|NKBA(Au)|YSZ|O2, CO2|Pt or Cell Ⅱ: Pt|Au, O2, CO2|K2CO3(Au)|NKBA(Au)|YSZ|O2, CO2|Pt.(Na,K-β/β″-Al2O3 is named by NKBA). The sensor signal is consistent with the Nernstian slope within the region ofphase equilibrium for Na, K-β/β"-Al2O3 material. The relationship between CO2 sensor voltage response and phaseequilibrium of solid electrolyte Na, K-β/β-Al2O3 is discussed in this paper. 相似文献
55.
添加剂及硫元素对ZL108合金中铁相形态的影响 总被引:7,自引:1,他引:6
在含铁为12%的ZL108合金中,加入5%的以锰、铬、稀土为基本成分的添加剂时,合金中针状、片状的铁相变为团球状、块状及梅花状。单独加硫时,铁相呈短杆状。先加入3%的添加剂再加硫,则铁相变为非常细小的团球状、块状,根据GB3508-83的规定,铁相形态可达一级 相似文献
56.
在BSO晶体中同时掺入Ce和Eu离子,生长了Ce:Eu:BSO晶体,对晶体的二波耦合和四波混频性能了测试。结果表明,Ce和Eu离子对晶体的光折变效应起到了增强的作用。 相似文献
57.
58.
单元系T—p相图的数学结构 总被引:1,自引:0,他引:1
作者以化学元素的稳定单质为基准,推演出了任意物质M_i(相态Ω)的热力学生成活度{相态Ω)的函数形式:?D_Ω数值的大小体现着相态Ω的热力学相对稳定性.根据集合论原理沿D(稳定性)座标取极大值的方法把物理性质互不连续的各个异相态连结在一起,建立了单元系在T-p面上的优势分布方程(PSDE):■作者以H_2O为实例,计算了T-p相图,与实验相图基本一致. 相似文献
59.
本文进一步探讨了有关双反馈晶振低噪声性能的问题,着重分析了石英谐振器静电容C_0对双反馈晶振电路Q倍增固子、石英谐振器Q值及净噪特性的影响。为验证上述C_0的影响,也对不同C_0的石英谱振器的相噪特性进行了测量并得到了与分析一致的结果。 相似文献
60.