Schwingfestigkeit von Schraube‐Mutter‐Verbindungen

High cycle fatigue of bolted connections Extensive tests regarding the influences on the fatigue of bolt‐nut‐connections of preloading with torsion, of preloading with yielding, of loading with superimposed bending and of the tested lot are processed. These influences are not yet known according to VDI 2230. New testing devices were designed for these tests, which allow a far less expensive operation and may easily be used for bolts of diameters up to M100 and testing frequencies up to 1000 Hz. The validity of fatigue resistance according to VDI 2230 is specified with respect to the test results. The determined influence of the tested lots is unexpectedly high. The manufacturing process of bolts should be improved to minimize this influence.     

Effect of organic dopants on electrodeposition and characteristics of polyaniline under the varying influence of H2SO4 and HClO4 electrolyte media

Electrodeposition of conducting polyaniline (Pani) was made under potentiostatic condition at pH 1.0 in different electrolyte media (H₂SO₄ and HClO₄) in the absence and presence of two organic dopants, disodium salts of naphthalene-1,5-disulphonic acid (NSA) and of catechol-3,5-disulphonic acid (CSA). The rate and yield of Pani deposition were dependent on the acid medium and the dopant employed. NSA in H₂SO₄ caused an increase in rate and yield but CSA decrease when compared to the rate and yield of H₂SO₄ alone. In HClO₄ medium, both the dopants showed a decrease. With regard to DC electrical conductivity, both the dopants exhibited an enhancement in H₂SO₄ medium but NSA a decline in HClO₄. Characterisation of the electrosynthesised polymer samples by various instrumental techniques (cyclic voltammetric: CV, FTIR, UV-Visible: UV-Vis, EPR, XRD, TGA and DTG methods) revealed that between the two acid media, H₂SO₄ was the better one. Further, it enlightened the role of two organic dopants in relation to the acid media. The advantageous role of NSA in H₂SO₄ had origin on its molecular characteristics such as non-polarity, larger π-electron cloud etc., while CSA could not perform such a role because of its easily oxidisable hydroxyl groups. In HClO₄, however, both the dopants could play only an unfavourable role owing to its greater polarity and oxidizing power than H₂SO₄.     

塔河油田特殊钻井条件下的录井技术

该文阐述了定向井、水平井和欠平衡钻井技术对传统录井方法的影响:钻时偏大、失真,岩屑细、代表性差,荧光常达12级、无意义,全烃值一般在5%以上,难以有效划分油气层;指出在特殊钻井条件下掌握设计指导思想,卡准重要层位是录井工作的关键,重点要参考组分分析数据、定量荧光分析数据和综合录井其它信息才能准确识别油气层。     

Prediction of foam growth and its nucleation in free and limited expansion

The influence volume approach (IVA) is often utilized for modeling the mass transfer process dictating bubble growth dynamics in physical foaming. However, the assumed concentration profile in the IVA method is only valid when the changes in dissolved gas concentration are small (less than 5%). In addition, the validity of the IVA method is difficult to justify in chemical foaming applications because of the difficulties involved in defining the dissolved gas concentration profile.In the present work, we define two distinct stages of bubble growth for physical foaming. These two stages are termed as free and limited expansion and are controlled by the bubble nucleation rate. Bubble nucleation is assumed to occur only in the free expansion stage. In this stage, the bubble pressure drops substantially from an initially high pressure in the supersaturated state while the dissolved gas concentration changes very little. The second stage of our two-stage mass transfer model is termed the limited expansion stage and accounts for bubble growth in the late stages of foam evolution, when the pressure changes become small. However, in the limited stage of bubble growth the dissolved gas concentration drops significantly, as the available dissolved gas is depleted. To summarize our two-stage mass transfer model of foam expansion, the pressure difference between the bubble phase and the liquid phase is the primary mechanism for driving mass transfer in the early (free) stages of foam growth and the concentration difference is the driver for bubble growth in the late (limited) stages of growth. The first stage can be regarded as the nucleation stage and it is relatively short; while the second stage can be regarded as the bubble growth stage and is much longer. Most of the bubble volume expansion takes place in the second stage.The concentration gradient at the bubble edge, which is often ignored in other models, is analyzed in detail in this paper. The details of our novel mass transfer model are also presented.     

重油隧道窑的红外温度测量

在分析重油隧道窑工况的基础上，分析了窑内烟气、燃烧物发射率、窑墙效应、环境温度对红外测温的影响以及热电偶测温的缺点，采取了相应的措施。利用中国发现专科实现了传感器输出信号的一致性。给出了传感器在重滑隧道窑现场使用２．５年后的复校数据。最后，估算出了用红外温度计替代热电偶测窑温产生的经济效益。     

Research on the measure method of complaint theme influence on online social network

Consumer complaints on online social network quickly become online groups complaints through many people’s aggregation and looking on, interaction and word-of-mouth communication. Therefore, assessing and managing online complain influence has become a new problem for enterprise to listen to and manage online group complaints. This paper analyzed the complaint information feature of consumer group on online social network, from three-dimensional perspective of complaint text’s quality, transmission timeliness and user interaction degree. We built the influence measure model of online complaint theme based on entropy weight model by monitoring and analyzing real-time the static and dynamic properties of complaint information, explored the measure method of complaint theme influence, employed empirical method to verify the validity and provided scientific decision-making tools and methods for enterprise listening to and managing online group complains.     

影响丙烯聚合釜正常运行和检修周期的因素及应对方法

在高分子化工生产当中,聚合釜是主要的反应、合成设备,聚合釜的正常运行使用和检修周期在很大程度上反应了生产工艺水平和设备管理维护水平。以间歇式液相本体法生产聚丙烯为例,对在该装置工艺条件下,影响聚合釜的运行情况及检修周期的几个主要因素进行初步的总结和分析,并提出相应的应对方法,以排除问题和不安全因素,提高聚合釜运行水平和正常使用周期。     

火驱燃烧前缘位置预测与影响因素研究

及时掌握火驱过程中火线的位置,有助于进行生产调控,通过调研现场预测火线位置的方法,得出一套针对不同特征油藏的适用方法:红外照相法适用于浅层油藏;用测温元件直接测试法适用于观察井和生产井密集的油藏;生产动态和物质平衡相结合的方法适用于均质性好且井网形式规范的油藏;示踪剂监测和生产动态相结合的方法适用于非均质性严重或井网形式不规范的油藏;压降试井法由于计算复杂,有待进一步研究。最后指出应在前期地质筛选的基础上,做到"少注气、多采油",并结合生产动态分析加强对油井的管理,引导燃烧前缘均匀稳定的推进。     

应力时效对P110套管螺纹参数的影响

在Φ339.7mmP110高强套管研制开发中发现,螺纹加工完成后因应力时效引起管体端头直径的变化,导致螺纹参数随之变化。通过对调质处理并矫直的套管几何尺寸及螺纹参数的测量试验,测试出随时间推移钢管几何尺寸、螺纹参数的变化量,分析其变化趋势及程度。通过应力时效对钢管形体作用的机理分析,提出确保套管螺纹参数稳定的控制措施。     

一种新型铁路天窗分析与探讨

利用列车运行图,采用模拟分析的方法,分析计算了双线自动闭塞线路上V型天窗和X型天窗的在空间域上列车运行线集,由此得出了开设X型天窗比V型天窗使列车正常运行所要受的约束条件多。在此基础上提出了V—X混合型天窗,经计算表明,该维修天窗性能优于V型和X型天窗。