双酚A型不饱和树脂在氯碱工业防腐蚀中的应用

本文针对氯碱工业特殊的防腐蚀要求，简要介绍了以双酚A型不饱和树脂为基体制作玻璃钢衬层和玻璃磷片涂层的配方、施工工艺及应注意的问题。     

亚麻籽胶对糯米淀粉凝胶冻融稳定性影响

为了解亚麻籽胶对糯米淀粉凝胶冻融稳定性的影响,利用差示扫描量热仪、X-射线衍射、傅里叶变换红外光谱仪和扫描电镜测定添加不同比例亚麻籽胶的糯米淀粉凝胶经过7次冻融循环后的热力学特性、结晶性、分子结构和微观结构。结果显示,亚麻籽胶能显著降低糯米淀粉凝胶的析水率;淀粉凝胶熔融焓/糊化焓降低显示糯米淀粉凝胶老化受抑制;随着亚麻籽胶添加量增大糯米淀粉凝胶相对结晶度降低,显示亚麻籽胶抑制了淀粉凝胶的重结晶;亚麻籽胶使淀粉凝胶羟基伸缩振动峰发生较大的位移,增强分子间氢键作用力,而没有生成新的基团;添加亚麻籽胶的淀粉凝胶微观结构表面光滑平整,凹洞较小,基质较紧密。说明亚麻籽胶能提高糯米淀粉凝胶的冻融稳定性。     

防腐蚀新技术在氯碱工业中的应用

介绍了应用于氯碱工业中的防腐蚀新技术：玻璃鳞片涂层和衬里、耐腐蚀玻璃钢、耐酸耐温砖(空心)／法奥里特复合衬里、不停车带压堵漏等。     

LED封装用导电银胶的制备及性能研究

通过研究树脂体系、固化剂及片状银粉对导电银胶体系力学性能、导电性能及耐候性能的影响,制备出可常温储存的导电银胶。结果表明,银粉质量含量75%,环氧树脂(EP)与聚酰胺酰亚胺树脂(PAI)质量比为80/20,二氨基二苯甲烷/二氨基二苯醚质量比为60/40,所配制的导电银胶的性能能够达到技术指标。样品经封装企业进行上线测试,能够满足应用要求。     

低温固化银浆导电性能的研究

对不同条件下制备的片状银粉与不同种类树脂体制备的银浆导电性能进行比较,讨论了表面分散剂、表面处理、球磨时间、树脂种类、固化温度等对低温固化银浆电性能的影响,对影响导电性能的因素与导电机理进行了探讨。     

Ni元素对原位自生TiCp/Fe复合材料组织和性能影响的研究

探讨了Ni元素对TiCp/Fe复合材料组织结构、力学性能及有害相的作用.结果表明,Ni元素对抑制TiCp/Fe复合材料中的石墨有害相有明显的作用,可以显著减少,甚至完全消除TiCp/Fe复合材料中的片状石墨有害相.同时,在Ni元素合金化作用下,TiC增强相数量增多,珠光体片层间距变小,这有效提高了TiCp/Fe复合材料的力学性能.     

Superior Mechanical and Magnetic Performance of Highly Anisotropic Sendust-Flake Composites Freeze Cast in a Uniform Magnetic Field

Despite extensive research, the manufacture in the bulk of high-performance flake-based magnetic composites with a highly aligned, nacre-like structure remains challenging. Many challenges can be overcome by freeze casting in an externally applied, uniform magnetic field, which causes both the flakes and the composite walls of the cellular solid to align parallel to the B-field lines. When appropriately sized, the flakes experience a second alignment parallel to the freezing direction because of a shear flow that occurs due to both the volumetric expansion of the ice phase and mold contraction during the directional solidification. The resulting orthotropic structure of the freeze-cast magnetic composite is reflected in orthotropic mechanical and magnetic properties of the material. The magnetic composites manufactured by magnetic-field assisted freeze casting outperform by a factor of 2–4 in terms of stiffness, strength, and toughness materials that are processed in the absence of a magnetic field and do not exhibit a monodomain architecture. Because of the highly aligned microstructure, it is possible to compact the initially lamellar composite with 90% porosity to at least 80% strain. The results presented in this study illustrate the tremendous potential for magnetic freeze casting of magnetic composites for use in power conversion.     

不同品种亚麻籽营养成分分析与品质综合评价

目的:研究不同品种亚麻籽综合营养品质的差异.方法:以来源于6个产地的12个品种亚麻籽为研究对象,以α-亚麻酸等8个营养成分作为品质评价指标,利用主成分分析法和隶属函数法对12个品种亚麻籽进行品质综合评价,同时利用聚类分析法将其归类.结果:对8个指标进行主成分分析,从中提取出3个主成分,累计贡献率达到87.608％,可较...     

Effects of germination on tocopherol,secoisolarlciresinol diglucoside,cyanogenic glycosides and antioxidant activities in flaxseed (Linum usitatissimum L.)

The changes in chemical composition and antioxidant activities of brown and golden flaxseeds (Linum usitatissimum L.) during 5-day germination were investigated. Flaxseeds germinated in a dark and closed incubator at the temperature of 25 °C. With noticeable reduction in fat content, germinated flaxseeds were determined higher percentage of linolenic acid. The total phenolic content and antioxidant activities increased with germination time. The highest amount of secoisolarlciresinol diglucoside (SDG) was found in 2-day germinated brown and golden flaxseeds, which increased 1.04-fold and 1.09-fold, respectively, and germinated flaxseed oil was found rich in SDG. Intriguingly, germination increased the α-tocopherol content from 0 to 4.58 mg per 100 g and 0 to 7.83 mg per 100 g in brown and golden flaxseeds while γ-tocopherol decreased. Germination process also reduced the total content of cyanogenic glucosides, the content of linustatin, neolinustatin and lotaustralin decreased significantly, but caused an increase in the content of linamarin. Therefore, germination can be utilised as an effective method to improve the nutritional value of flaxseed.