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101.
The short term (∼100 h) oxidation behaviour of the 9%Cr steel P91 was studied at 650 °C in N2-O2-H2O gas mixtures containing a relatively low oxygen level of 1%. The oxidation kinetics were measured thermogravimetrically and the oxide scale growth mechanisms were studied using H218O-tracer with subsequent analyses of oxide scale composition and tracer distribution by MCs+-SIMS depth profiling. The corrosion products were additionally characterised by light optical microscopy, SEM-EDX and XRD. It was found that the transition from protective, Cr-rich oxide formation into non-protective mixed oxide scales is governed by the ratio H2O(g)/O2 ratio rather than the absolute level of H2O(g). The results of the tracer studies in combination with the data obtained from experiments involving in situ gas changes clearly illustrated that under the prevailing conditions the penetration of water vapour molecules triggers the enhanced oxidation and sustains the high growth rates of the poorly protective Fe-rich oxide scale formed in atmospheres with high H2O(g)/O2 ratios. The experimental observations can be explained if one assumes the scale growth to be governed by a competitive adsorption of oxygen and water vapour molecules on external and internal surfaces of the oxide scales in combination with the formation of a volatile Fe-hydroxide during transient oxidation. The formation of the non-protective Fe-rich oxide scales is suppressed in atmospheres with low H2O(g)/O2 -ratios, and the healing of any such scale is promoted. 相似文献
102.
采用高分子网络微区沉淀法制备纳米镁铝尖晶石(MgAl2O4)粉体,并采用TGA/DTA、XRD和TEM等分析测试技术对前驱体的热分解和所制得粉体的物相组成、形貌及颗粒尺寸进行表征,结果表明所制得的MgAl2O4粉体颗粒粒径小,结晶良好,成分单一且粒径大小均匀。而实验过程中工艺参数的改变会对生成粉体的粒径和形貌产生一定的影响,进而即研究了各种工艺参数的改变对该方法制备纳米MgAl2O4粉体的影响。 相似文献
103.
New inverse method for identification of constitutive parameters 总被引:1,自引:1,他引:1
A new inverse method by coupling iSIGHT and ABAQUS was proposed to determine the constitutive parameters of Al2O3sf/LY12 composite deforming at elevated temperature. It combined the merits of the f'mite element simulation and optimization technique. The direct model was simulated with finite element code ABAQUS. The inverse problem associated with the identification of the constitutive parameters was expressed as a least square optimization problem. The direct simulation and the parameters optimization were implemented in iSIGHT integrated environment. The aim was to match the output of the direct simulation with the experiment data. The capability of the proposed inverse method was demonstrated through the identification of constitutive parameters of Al2O3sf/LY12 composite. The proposed new inverse method is also applicable to other parameters identification which is hardly determined through experiments or direct analytical method. 相似文献
104.
105.
通用电子手册数据库录入软件的关键技术 总被引:1,自引:0,他引:1
文章主要讨论了关于通用电子手册数据库录入软件的组成和功能,较为详细地讨论了实际开发中几个关键技术的解决方案.实际设计完成了通用电子手册数据库录入软件模块,并应用于实际工作中,运行良好. 相似文献
106.
大型钛合金压气机盘超塑性等温锻造模具结构及工艺参数实验研究 总被引:3,自引:0,他引:3
通过超塑拉伸和压缩试验,用金属铅进行模拟实验,探讨了大型TC11合金压气机盘超塑性等温锻造的工艺参数,模具结构,锻坯形状尺寸及润滑剂的选择、并讨论了其模具材料及加热方式的选择。 相似文献
107.
磁性纤维随机混合媒质等效电磁参数的计算 总被引:1,自引:0,他引:1
为计及强散射偶极子间的相互作用,引入参量εh和μh,利用广义多重散射理论及MATLAB计算机软件对在2 GHz~18 GHz频率下的体积占空比为8%的铁纤维随机混合媒质等效磁导率的实验值进行曲线的拟合,导出了耦合系数εh和μh,并在此基础上,对体积占空比分别为30%和20%的铁纤维随机混合媒质等效磁导率进行了计算,计算结果与实验吻合良好. 相似文献
108.
109.
Sand casting process and directional solidification technique combining thermal-rate treatment(TRT) were used. The influence of process parameters on TRT was investigated according to the values of impact toughness. At the same time, the mechanism of TRT was discussed. The results showed that TRT can improve the impact toughness of this alloy, while the hardness is basically constant. The time of heat preservation should not be more than 5min. Different forms of cooling intensification additive have different effects among which the zinc ingot solidified in graphite mold is the best one that can improve impact toughness of samples by more than 80%. With increasing the cooling temperature, the value of α(Al) crystal lattice constant increases. The element Sb has negative effect on TRT. 相似文献
110.