TIG熔敷堆焊快速成形视觉传感系统的研究

对于TIG熔敷堆焊快速成形视觉传感系统进行了一定的研究；通过对TIG熔敷堆焊快速成形的原理的分析．介绍了选择CCD作为TIG熔敷堆焊快速成形视觉传感器的动能；从光学理论得出视觉系统的标定方法；从实验结果来看视觉传感系统所得到的图像能够清晰反映出TIG熔敷堆焊的焊接轨迹。     

Interfacial reactions of liquid Sn and Sn-3.5Ag solders with Ag thick films

The interfacial reactions of liquid Sn and Sn-3.5Ag solders with Ag thick films are investigated in the temperature range from 250–325 °C, and the morphology of intermetallic compounds formed after such soldering reactions is observed. In kinetics analysis of the growths of intermetallic compounds, it was found that both Sn/Ag and Sn-3.5Ag/Ag reactions were interfacial-controlled, and the growth rates for both cases were similar. The rate of Ag dissolution into liquid solder attendant on the formation of interfacial intermetallic compounds after Sn/Ag reaction was about four times higher than that after Sn-3.5Ag/Ag reaction, as evidenced by experimental results.     

从彩印漂定液废水中回收银和制备纳米银粉技术的研究

研究了用过氧化氢还原法、沉淀 -还原法和次亚磷酸钠还原法从彩印漂定液废水中回收Ag和制备纳米银粉技术 .比较了 3种还原方法与银粉纯度和回收率的关系 ,研究了各还原方法的反应条件对银粉粒径的影响。实验结果表明 ,采用过氧化氢还原法 ,得到的银粉纯度高 ( 93% ) ,回收率 >92 % ,银粉粒径 <1 0 0nm ,是一种较好的回收方法。     

Ag-Pd-5Ru-Gd四元系部分相图的700℃等温截面

在Ag Pd Gd ,Ag Pd Ru ,Ag Ru Gd和Pd Ru Gd三元系合金相图的基础上 ,采用X射线衍射 ,差热分析、扫描电镜和显微金相分析等方法研究了Ag Pd Ru Gd(x(Ru) =5 % ,x(Gd) <2 5 % )四元系相图的 70 0℃等温截面。结果表明 :该截面上包含有 2个单相区 ,即Pd(Ag)和Pd3 Gd ;4个两相区 ,即Pd(Ag) (Ru) ,Pd(Ag) Pd3 Gd ,(Ru) Ag51Gd14 ,(Ru) Pd3 Gd ;3个三相区 ,即Pd(Ag) Pd3 Gd (Ru) ,Pd(Ag) Ag51Gd14 (Ru) ,Pd3 Gd Ag51Gd14 (Ru) ;1个四相区 ,即Pd(Ag) Pd3 Gd Ag51Gd14 (Ru)。未发现新的四元中间相     

乐红铅锌矿床综合找矿模型的建立及重要性

通过对云南乐红铅锌矿已知矿床的地质、地球物理、地球化学特征的研究,构建了地质—地球物理—地球化学的综合找矿模型。该模型的建立,对Pb、Zn金属成矿带预测、地球物理、地球化学异常评价及解释具有重要的意义,并能较好地指导区域找矿及勘查工作。     

微量稀土对SnAgCu无铅钎料力学及润湿性能的影响

对真空条件下制备的Sn2．5Ag0．7CuxRE钎料合金的力学及润湿性能进行了研究。结果表明：当RE添加量为0．1％（质量分数）时，钎料合金具有较大的铺展面积、较小的润湿角和较高的拉伸强度、伸长率，可满足微电子连接的需要。     

工艺参数对合成ZnO／Ag纳米复合抗菌剂产率的影响

通过正交实验，研究了反应温度、反应时间、反应物配比对ZnO／Ag纳米复合抗菌剂合成产率的影响规律。获得了高产率合成ZnO／Ag纳米复合抗菌剂的优选工艺条件：反应温度为10～25℃，ZnSO4与NH4HCO3的摩尔比为1：2-2．5，ZnSO4与NH4HCO3的反应时间为2．5～3h，AgNO3与NH4HCO3的摩尔比为1：1．5～2，反应时间为0．5h，ZnO／Ag的产率超过98％。XRD、TEM和SAED结果表明：ZnO／Ag纳米复合抗菌剂为具有纤锌矿结构的ZnO和立方结构的Ag组成。粒径为15～25nm，分散性较好。     

熔剂对高频熔覆耐磨覆层工艺性能的影响

采用高频感应加热可以在低碳钢表面熔覆一层耐磨材料，熔剂对覆层与基体的结合、覆层表面成形、脱渣性等工艺性能起着决定性的作用。本文探讨了熔剂对高频熔覆工艺性能的影响。在Fe基Cr13Ni2B合金粉末中加入适量的焊剂431、硼酐及氟化物，可以有效地去除粉料表面的氧化物，降低其熔点，促进粉料与基体的结合．形成一层脱渣容易、表面成形美观且与基体形成牢固冶金结合的耐磨覆层，覆层厚度可以达到2．5mm。     

四川盆地含膏盐红层特征及坝基工程地质问题(Ⅱ)

本文探讨了四川盆地含膏盐红层类岩溶作用引起的坝基工程地质问题,首先是地下水化学成分的改变及其对水工结构混凝土的腐蚀作用及坝基渗漏问题,然后确定了表征类岩溶作用强度的类岩溶强度因子(k).最后,通过类岩溶岩体Vp与主要岩体工程力学指标,诸如:允许承载力fak、抗剪(断)摩擦系数f(f')、变形模量(E0)的回归关系,探讨了类岩溶作用对坝基岩体弱化的作用.     

Activatable NIR-II Lanthanides-Polymetallic Oxomolybdate Hybrid Nanosensors for Monitoring Chemotherapy Induced Enteritis

Chemotherapy-induced enteritis is one of the side effects associated with cancer therapy, which significantly affects the treatment effect, but there is no effective clinical detection method that can early diagnose its occurrence and progression. Here, a series of second near-infrared window (NIR-II) hybrid nanosensors are designed that consisted of lanthanide nanoparticles and β-Mo2C-derived polymetallic oxomolybdate nanoclusters (Ln@POM). Based on the high sensitivity of POM to reactive oxygen species (ROS) closely related to chemotherapy-induced enteritis, the NIR-II luminescence intensity and lifetime of Ln@POM (Ln: Yb³⁺, Nd³⁺, Ho³⁺, Tm³⁺, Er³⁺) show excellent responsiveness to H₂O₂ and HClO with the detection limit down to 0.15 and 0.14 µm , respectively. Utilizing Nd@POM as a ROS-activated NIR-II nanosensor, the chemotherapeutic enteritis is successfully detected within 7 h after induction of chemotherapy drugs, which is significantly earlier than the gold standard method (immunohistochemistry, 24 h). These results demonstrate that the designed hybrid nanosensors are promising optical tools for the early diagnosis of ROS-related diseases.