Effects of Refractories on the Total Oxygen Content and Inclusions in the IF Steel

The effects of refractories of quarz-corundum consisting of 45 mass% quartz and 55 mass% corundum,fused corundum and fused magnesia on the total axygen content(TOC) and the composition of inclusions in intersitital free(IF) steel were studied,3 mass% microsilica was added into the three refractories as binder.The refractories were shaped as lining of the graphite crucible by castable method IF steel was placed in the crucibles,then they were heated at 1600℃ for 90min and 45min respectively.Oxygen contents of the steel samples were obtained by axygen determinator.Inclusions were analyzed by SEM and EDS.The results show that the TOC of steel increase with ncrease of Index of Oxygen Potetial (IOP) of the refractories.The steel sample coped with MgO refractories having the lowest IOP has the lowest TOC.     

b型流感嗜血杆菌多糖结合疫苗的研制

［摘 要］目的 研制b型流感嗜血杆菌（Hib）结合疫苗并考察其稳定性。方法 用溴化氰活化提纯Hib荚膜多糖抗原，通过己二酰肼（ADH）与破伤风类毒素（TT）蛋白共价结合，制备b型流感嗜血杆菌结合物，并考察放置在2～8℃及室温9个月和37℃　3个月后的稳定性。结果 用本工艺提取的多糖，合成的多糖衍生物，多糖蛋白结合物的化学组成及结构特性均达到了国外同类产品的质控要求。结合物在2～8℃及室温放置9个月后基本无降解。结论 为临床评价Hib结合疫苗的安全性和保护效果及确定效期提供了实验基础。     

基于B/S的资料信息管理系统的设计和实现

该文介绍了基于B/S资料信息管理系统的设计和开发,重点阐述了资料信息管理系统的开发设计的难点和要点,同时提供了部分数据库表信息和代码。     

基于Web网的高校安全管理系统的设计与开发

为了解决高校安全保卫工作办公方式落后、管理水平低下等问题,开发了一套基于Web网的高校安全管理系统。介绍了系统设计和架构框图,并对系统功能做了进一步的实现,最后展示了运行效果。     

实时物流递送路径规划与模拟

近些年来,顾客需求不断多样化、企业竞争更加激烈、全球制造的概念不断发展,不仅我国政府也将物流视为新的经济热点,而且已经引起了全球各个国家的重视。从政府到企业,从中央到地方,都开始物流战略的规划与实施,并且开始物流信息系统的建设。该文以物流路径规划系统为研究对象,介绍了一些著名的最优路径规划算法。在深入分析节约算法的基础上,提出并实现了配合Dijkstra算法的节约里程表算法,开发了以本文算法为核心的实时物流路径规划与模拟系统。     

基于PHP和Ajax技术的在线网页闹铃的设计与实现

该文简单介绍了B/S网络应用开发架构,详细阐述了网页闹铃功能设计,并对原理进行了详细的讲解,对功能做了进一步的实现,展示了运行效果。     

Adhesive bonding of stainless steel water tubing

The use of an adhesive to bond stainless steel water tubing, allowing stainless steel fittings to be employed, is considered and compared with the more conventional use of compression or capillary copper fittings together with a soft solder. Tests carried out to determine environmental effects on adhesively bonded stainless steel tubing suitable for domestic water supply, and the strengths of these joints, are described. It has been found that acrylic anaerobic adhesives are suitable for bonding tubing carrying cold water, the joints attaining superior strength to the copper-soldered ones; a reasonable degree of flexing can also be tolerated. It would appear that certain selected adhesives may also be used in joints carrying hot water.     

Production of finely ground natural graphite particles with high electrical conductivity by controlling the grinding atmosphere

Natural graphite particles with high crystallinity sieved to obtain a particle size range of under 63 μm were ground with a ball mill, under various well-controlled grinding atmospheres such as N₂, O₂, He, H₂, and vacuum. The ratio, X_dif50/X_st50, i.e. between the 50 wt.% Stokes diameter and the 50 wt.% laser diffraction diameter, of the ground particles, was used as an index of the flakiness of the particles. The specific resistance of films composed of the ground graphite particles was systematically measured. The rate of reduction in the size of the particles by grinding was slow under an O₂-rich atmosphere such as 100% O₂ and dry air. On the other hand, it was relatively fast in vacuum, or under an N₂ or He atmosphere, and a gas mixture of 99% N₂ and 1% O₂. The rate of size reduction by grinding under a H₂ atmosphere was intermediate. In our experimental conditions, the flakiness of the ground particles increased with the decrease in the particles’ sizes. The electrical conductivity of the ground particles, however, tended to decrease with the decrease in their sizes. Under the condition that the Stokes diameter of the ground particles remains constant, the electrical conductivity of films made from the ground particles increases with the increase in the flakiness of the particles. It was finally determined from our systematic grinding experiments that small flaky particles, which had a size, X_st of ∼1 μm, with a high electrical conductivity can be produced by grinding in a gas mixture of 99% N₂ and 1% O₂. In this case, the flaky shape of the ground particles was visually confirmed by scanning electron microscopy.     

304 Stainless steel oxidation in sulfate and sulfate+ bicarbonate solutions

The electrochemical characterization of 304 stainless steel in 0.1–0.5m Na2SO4 and Na2SO4 + NaHCO3 aqueous solutions at pH8 was done in combination with SEM surface analysis. Passivation of the surface film without any pitting events is observed for the current–potential and current–time experiments, and no anodic current spikes, which are associated with depassivation events, are distinguishable above the background current level. However, SEM pictures of an electrode surface polarized at potentials above 0.4V show microscopic pit nucleation. Even when the metal may be regarded as passive from a current–time or current–potential characteristics, passivity is not stable and localized film breakdown can still occur. The events are ascribed to pit nucleation at the active inclusion sites. The pits do not grow even into the metastable state but die through repassivation by metal salt precipitation immediately after birth. The effect is ascribed to the solubility of metal salts with the electrolyte produced by dissolution in the nucleation sites. The results show that pit nucleation and pit growth are two distinct processes. The importance of solution composition and the protective effect of bicarbonate ions is also discussed.     

碳中和背景下的钢化联产发展趋势

本工作针对钢铁行业副产的煤气、余热、钢渣及钢化联产现状进行了分析，论述了碳中和背景下钢化联产绿色低碳技术的发展趋势，展望了未来无碳炼钢的新型钢厂从“以化固碳”转变为“以氢代碳”的新模式，并提出了加快钢化联产新技术应用建议和举措，以期建立以钢铁行业为龙头，耦合化工行业的新型工业可持续发展生态链，支撑我国“双碳”目标的实现。