硫酸铵-氯化亚锡-孔雀绿体系浮选分离铂

研究了在盐酸介质中硫酸铵存在下氯化亚锡—孔雀绿—水体系浮选分离铂的方法。在最佳实验条件下，铂的浮选率可达100．0％，并与常见贱金属完全分离。     

Long-chain fatty ammonium quaternaries in papermaking

A series of long-chain quaternary ammonium halogen esters (UKK-chemicals), quaternary dimethyl tallow epoxypropyl ammonium halogens (EPK1), quaternary ditallow methyl epoxypropyl ammonium halogens (EPK2), and EPK2 oligomers (EPK2P) were synthesized. At acidic, neutral, or slightly basic conditions, EPK1-, EPK2-, EPK2P-, and UKK-chemicals operate as cationic chemicals. They can be used, for example, as stock sizings, surface sizings, or fixatives. Stock sizing, surface sizing, and fixative experiments indicate that EPK1-, EPK2-, EPK2P-, and UKK-chemicals function at least as well as or better than the corresponding synthetic chemicals used in papermaking.     

油气田开发中的CO2腐蚀及防护技术

综述了二氧化碳均匀腐蚀和局部腐蚀的机理，分析了二氧化碳腐蚀的各种影响因素，并对二氧化碳腐蚀的防护技术进行了概括，着重介绍了缓蚀剂防护技术研究进展，并提出了研究CO2腐蚀及其缓蚀剂应注意的几个问题。     

Preparation of Ultra—fine Aluminum Nitride in Thermal Plasma

Ultra-fine aluminum nitride has been synthesized by the evaporation of aluminum powder at atmospheric-pressure nitrogen plasma in a hot-wall reactor.The average size of aluminum nitride particle is 0.11μm measured by scanning electric mirror(SEM),and the purity is at least over90% evaluated by X-Ray diffraction(XRD).The conversion of Al powder to aluminum nitride is strongly depended on the injection of NH3.Typical experimental parameters such as the feed rate of raw material,the flow rate of ammonia and the position of injecting aluminum powder into the reactor are given.     

十六烷基辛基二甲基溴化铵和十六烷基癸基二甲基溴化铵的合成

合成了十六烷基辛基二甲基溴化铵和十六烷基癸基二甲基溴化铵两个新型杀生剂。用元素定量分析和红外光谱核磁共振谱等方法进行分析和结构鉴定。评定了两个化合物对硫酸盐还原菌的杀生作用。结果表明，两个化合物有很好的杀生效果。     

P／MCs新型复合材料制备、结构及阻尼性能

采用特殊的渗流法所制备的新型Ｐ／ＭＣｓ复合材料，由高分子聚合物与蜂窝状铝架组成，它具有优异的阻尼性能，并简述了结构对阻尼的影响     

SiCp/2024复合材料的氢脆敏感性研究

在浸泡、阴极极化、阴极极化同时迭加拉伸变形、添加As₂O₃毒化剂等常见致氢条件下,通过慢应变速率拉伸试验研究了SiC_p/2024复合材料的力学性能,考察了断口形貌.测定了该材料在按几种常用充氢条件充氢后的氢含量.发现虽然强烈阴极极化使材料力学性能下降,但其原因在于阴极极化引起的碱性腐蚀,与氢脆无关.获得了不同于前人研究的新结论:在本文试验条件下SiC_p/2024材料不发生氢脆,也不发生不可逆氢损伤,其原因与该材料难以充入氢有关.     

Pyrolysis-field ionization mass spectrometry of modified bagasse fractions

The fractions obtained from bagasse after activation with 17.5% NaOH, alternative alkylation with quarternary ammonium groups and extraction with 80% ethanol, water and 5% NaOH, were analyzed using pyrolysis-field ionization mass spectrometry (Py-FIMS). The proposed degradation products from lignin were mostly symmetric fragments containing two aromatic rings while the compounds formed from polysaccharides were the result of dehydration reactions. From the temperature-resolved Py-FIMS it could be seen that ethanol-lignin starts to degrade at temperatures lower than 180°C before the degradation of the hemicellulose fraction. The lignin markers are eliminated from hemicellulose fractions before the polysaccharide gasification starts. The quarternary ammonium groups are cleaved from the fractions at temperatures lower than 200°C.     

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本文采用流动模拟实验方法,以渗透率损害率为评价气层损害的定量标准,对以川东石炭系为主的完井液损害程度及滤失深度进行了试验研究,并对地层损害进行了预测。