甘肃武威盆地页岩气“武页1井”成膜低固相冲洗液的应用

“武页1井”是甘肃省地质调查院实施的一口页岩气基础地质条件调查井,主要目的是为了查明页岩层段的分布。地层岩性主要为泥岩、砂岩、页岩、碳质板岩、灰岩。浅层倾角大、胶结性差、破碎、井壁强度低。现场采用成膜低固相冲洗液体系,解决了地层破碎、坍塌掉块和水敏性钻探施工难题,体系具有护壁性、抑制性和胶结性。使用中取得了较好的效果,保证了该项目的顺利施工。     

小入射角下海浪后向散射系数不对称性和各向异性分析验证

基于北京遥测技术研究所机载波谱仪实测数据以及ECMWF提供的风场数据,分析了不同风速条件下小入射角海浪平均后向散射系数不对称性与各向异性随入射角的变化特性,并对导致这一现象的原因进行了初步分析。结果表明:小入射角下,海浪平均后向散射系数随入射角增大呈现递减趋势并在18°时达到某一稳定值,之后基本维持不变;海浪后向散射系数不对称性与各向异性均随入射角增大呈现递增趋势,同样在18°增大至某一稳定值,之后基本维持不变;低风速条件下,海浪不对称性和各向异性与风速有关,且风速越大不对称性与各向异性越明显。     

Research of in-situ hydraulic test method by using double packer equipment

Double packer equipment for hydraulic test can be used to measure pressure of test zone directly, and it is frequently used to perform many kinds of hydraulic tests and take groundwater sample from borehole. The test method of this equipment mainly includes the test design, implementation, interpretation and synthetic analysis. By adopting the double packer equipment for hydraulic test, the parameter distribution of rock permeability along borehole can be acquired, as well as the connectivity, water conductivity and water bearing capacity of the disclosed structure and the chemical characteristics of the deep groundwater. It is a necessary method for the research and evaluation of the complex hypotonicity terrace site selection under geological conditions. This method is not only suitable for the geological disposal of high level radioactive waste, but also can be used in the site selection of underground facilities such as storage of petroleum and carbon dioxide. Meanwhile, it has a good application prospect in other hydrogeological investigation fields.     

Formation of low permeability reservoirs and gas accumulation process in the Daniudi Gas Field,Northeast Ordos Basin,China

The Daniudi Gas Field is a typical large-scale coal-generated wet gas field located in the northeastern Ordos Basin that contains multiple Upper Paleozoic gas-bearing layers and considerable reserves of gas. Based on integrated analysis of reservoir petrology, carbonate cement C–O isotope, geochemistry of source rocks and HC gas and numerical basin modeling, a comprehensive study focusing on the formation of low permeability reservoirs and gas generation process uncovers a different gas accumulation scene in Daniudi Gas Field. The gas accumulation discovered was controlled by the reservoir permeability reduction and gas generation process, and can be divided into two distinct stages by the low permeability reservoir formation time: before the low permeability reservoir formation, the less matured gas was driven by buoyancy, migrated laterally towards NE and then accumulated in NE favorable traps during Late Triassic to early Early Cretaceous; after the low permeability reservoir formation, highly matured gas was driven by excessive pressure, migrated vertically and accumulated in-situ or near the gas-generating centers during early to late Early Cretaceous. The coupling relationship between reservoir diagenetic evolution and gas generation process controlled on gas accumulation of the Daniudi Gas Field. This study will aid in understanding the gas accumulation process and planning further E&D of the Upper Paleozoic super-imposed gas layers in the whole Ordos Basin and other similar super-imposed low permeability gas layer basins.     

Development of Prebored Screw Pile Method and Evaluation of Its Bearing Characteristics

The pile-driving method produces considerable noise and vibrations. Hence, an auger-drilled pile method was developed as a low-noise and -vibration substitute. However, this method does not guarantee the bearing capacity of the pile unless some amount of pile-driving is performed. Therefore, the noise and vibration problems cannot be completely solved. In this study, a prebored screw pile method is proposed to solve these problems. In this method, piles are constructed by the rotary penetration of a screw pile into a prebored hole filled with some cement milk and whose diameter is smaller than that of the screw pile. To determine the shape of the screw pile, laboratory tests with model screw piles were conducted. Also, field load tests were conducted on an actual screw pile fabricated based on the laboratory test result and on a smooth-surfaced pile. In addition, the behavior of the screw pile was estimated by using three-dimensional finite element analysis. The results of the field load test and the numerical simulation showed that the ultimate bearing capacity and the unit skin friction of the screw pile are very superior to those of the smooth-surfaced pile and the cement milk is an important factor in the prebored screw pile method.     

四川平武银厂金矿勘探复杂地层钻进技术

四川平武银厂金矿区钻探施工中遇到漏失、缩径、岩心破碎、易孔斜和钻孔事故频发等施工难题,施工难度极大。本文结合地层特点,通过采用绳索取心液动锤、高密度低失水泥浆体系、跟管钻进等工艺技术措施,提高了钻进效率和施工质量,大幅度减少了孔内事故的发生,为顺利完成钻孔施工任务奠定了坚实的基础。     

围压和孔隙结构对不同粒级砂岩孔隙度渗透率的影响实验研究

孔隙度和渗透率是储层评价的两个重要参数.岩石毛管压力曲线和核磁共振T2谱图是描述储层微观结构特征的重要参数.通过测量不同压力条件下岩心样品的孔隙度和渗透率,得到了孔隙度和渗透率随压力的变化情况.实验结果表明：孔隙度和渗透率随着压力的增加而降低,并且与压力服从对数函数变化规律.不同孔隙度渗透率区间的砂岩样品,孔隙度和渗透率随着压力变化的趋势不同.通过测量不同粒级砂岩样品的毛管压力曲线和核磁共振T2谱图,证实了孔隙结构对孔隙度和渗透率的影响,微观孔隙结构是决定渗透性好坏的关键因素.     

印度尼西亚苏门答腊岛Woyla金矿流体包裹体研究及矿床成因分析

印度尼西亚Woyla金矿床位于西苏门答腊地体北段,为一中型规模的金矿床。本文通过对含矿石英脉开展详细的流体包裹体显微测温、成分分析,结合石英的H-O同位素和黄铁矿的S同位素特征分析,结果如下：其中,流体包裹体研究结果表明,含金石英脉中的石英主要发育气液两相包裹体,包裹体均一温度变化范围为152～324℃,集中在200～280℃。盐度为(0.88～6.16)wt%NaCleqv,集中在(1.00～3.00)wt%NaCleqv,成矿流体密度为0.70～0.94g/cm3,平均为0.82g/cm3。成矿压力为9.63～25.84MPa,平均值为18.37 MPa。成矿深度为0.96～2.58km,平均为1.86km,以上显示Woyla矿床成矿流体具有中低温低盐度和浅成的特征。包裹体气、液相成分测定显示气相成分以H2、N2、CO 、CO2、CH4和H2O为主;液相成分中阳离子以Na+、K+和Ca2+为主,阴离子以富SO42-和Cl-为特征,成矿流体属Cl--SO42--Ca2+-K+型。氢氧同位素测定显示成矿流体δ18DV-SMOW=-78.3‰～-92.4‰,δ18OH2O=-3.0‰～-5.5‰,主要来自大气降水,可能有少量岩浆水参与。黄铁矿硫同位素组成为-0.21‰～1.22‰,平均值为0.34‰,说明成矿物质的S具有深源岩浆硫的特征。结合矿床地质特征和成矿流体研究,首次提出Woyla金矿床属典型的低硫型浅成低温热液型金矿床。     

Petrophysical characterisation of tight sandstone gas reservoirs using nuclear magnetic resonance: a case study of the upper Paleozoic strata in the Kangning area,eastern margin of the Ordos Basin,China

Residual and movable porosity are significant parameters for characterising petrophysical properties, especially in tight reservoirs. Eight tight sandstone samples from the upper Paleozoic gas-bearing strata in the Kangning area, from the eastern margin of the Ordos Basin, were analysed using nuclear magnetic resonance (NMR), scanning electron microscopy (SEM), petrography, and porosity and permeability tests. The lithology and pore types were identified and classified using petrography and SEM. The residual and movable porosity were obtained with NMR. In addition, NMR was used to visualise pore structure and pore size distribution. The results suggest that the upper Paleozoic sandstones in the study area mainly comprise feldspathic litharenite and litharenite. The sandstone porosity and permeability are low, with means of 5.9% and 0.549 mD, respectively. Four pore types exist in the tight sandstones: residual primary pores, grain dissolution pores, micropores (clay-dominated) and microfractures. The T₂ spectra under water-saturated conditions correlate with pore size and can be used to distinguish small and large pores based on the transverse relaxation time cutoff value of 10 ms, which corresponds to a pore diameter of 0.232 μm. Small pores account for 72% of the pores in the tight sandstones. The continuous bimodal T₂ spectra suggest good connectivity between small and large pores, despite the low porosity and permeability. In this study, the movable porosity of the major tight sandstone gas reservoirs is higher than the residual porosity, which confirms the effective evaluation of movable porosity to tight sandstone reservoirs, based on NMR experiments.     

季节性低温胁迫下陇东黄土高原油污土壤环境因子对耐冷混合菌场地生态修复的响应

为了揭示季节性低温胁迫下陇东黄土高原油污土壤环境因子对耐冷混合菌场地生态修复的响应机制,利用自主筛选构建的耐冷石油降解混合菌在甘肃省庆阳市庆城县马岭镇长庆油田陇东油泥处理站开展了为期7个月的场地修复实验,采用常规方法测定了不同季节土壤理化特性、酶活性和微生物群落特性等环境指标。结果表明：（1）在季节性低温胁迫下（9-11月）M2组（耐冷混合菌处理组）月平均降解率明显增加（P<0.01）,JZJ+M1组（金盏菊联合常温混合菌处理组）和M2组累计TPH降解率分别为15.37%±3.51%和28.64%±4.12%。（2）M2组土壤脱氢酶和多酚氧化酶在低温季节（LT）活性最高,且温度和处理存在显著交互作用（P<0.01）。在土壤营养元素方面,无论何种处理方式（JZJ+M1和M2）二者含量均为RT（常温季节）高于LT（P<0.05）,同时明显高于CK组（P<0.05）。（3）M2组土壤微生物群落Shannon-Wiener指数和均匀度指数在LT高于RT（P<0.05）。（4）NMDS和Pearson相关性分析结果显示,M2组在低温季节具有较高TPH降解率主要与土壤多酚氧化酶、脱氢酶、单月TPH降解率（μ2）和Shannon-Wiener指数有关,且均呈极显著正相关关系。通过分析环境因子的季节响应,优化场地修复在低温环境的降解条件、加速低温期石油烃降解速率,以期为陇东地区低温耐冷混合菌场地生态修复技术的推广应用提供参考和基础数据资料。